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Accuracy of the determination of liquid viscosity
Zikmund, Ondřej ; Rozsívalová, Zdenka (referee) ; Frk, Martin (advisor)
This master thesis is focused on the rheological properties of liquids, especially on the viscosity and the standard uncertainty. It explains methods of the viscosity measurement and the calibration selected viscometers, the principle of the determination of standard uncertainty by indirect measurement of the viscosity and the density. The main object of this thesis was to create a specialized centre for viscosity measurement and to create a document which could be used by teaching of diagnostics.
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Effects of hyaluronan on properties of eye drops
Chromá, Kateřina ; Mravec, Filip (referee) ; Pekař, Miloslav (advisor)
Modifying eye drops using hyaluronan leads to an increased retention time on the eye surface. Long-lasting observations of the stability of two different eye drops, Opthalmo-Septonex and Visine Classic, after the addition of hyaluronan with varying concentration are presented in this work. The interactions of hyaluronan with the eye drops, or their components benzalkonium chloride and tetryzoline, are investigated by monitoring particle sizes and the charge of the molecules. Additionally, rheological examinations of the samples are done and the mucoadhesion index is determined by using the mucine method.
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Flow properties of coolants for metal cutting
Blašková, Daniela ; Poláček, Petr (referee) ; Bálková, Radka (advisor)
The flow properties of two types of operating and clean coolants (A and B) were measured, both used in metalworking. Four samples of both operating liquids were sampled from the process monthly (from the beginning to the end of its use). All liquids were measured at 25 °C with an oil emulsion content of 4%. In addition, flow curves of pure cooling emulsions with concentration of coolant 2, 4, 6 and 8% were measured at 30, 35, 40, 45 and 50 °C. Rheological measurement was performed at geometry of concentric cylinders. Microbial activity and content of additives (Thermogravimetry) was determined in operating liquid A. Both operating liquids exhibited non-Newtonian behavior. Viscosity increased with the shear rate (10–100 s-1) and impurity level. Although the amount of impurity was approximately the same in both liquids, viscosity varied. For pure liquids, the viscosity increased with increasing concentration and decreased with increasing temperature, except for liquid A with concentration of coolants 6 and 8%, which, depending on the temperature, exhibited both shear thinning, shear thickening and Newtonian behavior. The results shown that impurity level of operating liquids has only minor effect on viscosity and flow properties, but it had an effect on cooling effect. Impurities diluted operating liquids, partial decomposition of the oil component may occur, but in particular, microbial activity causes skin problems of staff. Recommended is to introduce a specific control test for the presence of bacteria.
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The effect of lubricant contamination and degradation on lubricating film behavior
Strnad, Jan ; Dzimko, Marián (referee) ; Omasta, Milan (advisor)
Lubrication contamination and degradation is one of the major causes of unexpected failure of tribological nodes. As a result, different levels of maintenance are introduced in practice, leading to a longer service life of the lubricated node. These systems often include sophisticated on-line diagnostic tools that can be used to evaluate a sample of a lubricant using certain variables such as viscosity, number of particles, humidity, dielectric constant, etc. Based on changes of these variables some systems can make corrective measures such as filtering or complete replacement of lubricant. Therefore, the aim of this experimental thesis is to determine the influence of lubrication contamination (solid particles, moisture) and degradation (oxidation) on the lubricating film behavior with respect to its limit bearing capacity. To examine the thickness of the lubricating film, friction and wear, an optical and MTM tribometer, in the ball-on-disc configuration, was used.
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Optimized manufacturing of aluminium castings by using lost wax technology
Talanda, Ivan ; Horenský, Jiří (referee) ; Horáček, Milan (advisor)
Aim of this diploma thesis is to choose new pattern wax for Fimes a.s. foundry. New wax should substitute old not fully satisfactory pattern wax which caused problems in technological process resulting in increased number of rejects. New pattern wax should eliminate current problems and help foundry with producing large, thin-walled, high-quality castings. Numbers of pattern waxes supplied by world’s leading wax manufacturers were subjected to laboratory tests and pilot study. This diploma thesis is part of project Alfa TA01010766: „Research and development of production technology large, thin and high quality castings of aluminium alloys “
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Investment casting waxes and measurements of their properties with regard to simulation software
Bochníček, Štěpán ; Mikulka, Vít (referee) ; Kosour, Vojtěch (advisor)
Today, the use of simulations is increasing in order to reduce cost and complexity of production and also to prevent product defects. For this purpose, we use simulation programs, such as ProCAST. This program is designed for simulation of casting parts. In my bachelor thesis I focused on the methods of casting lost wax, where the model is made of wax mixture. In each simulation we have to obtain and specify the properties of the material to casting. I described these properties and methods of measurement in this bachelor thesis.
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Dependence of quality parameters of malt on the temperature of mashing at sweet wort preparation
Zlámalová, Petra ; Sachambula, Lenka (referee) ; Mikulíková, Renata (advisor)
The Masters thesis deals with dependence of quality parameters of malt on the temperature of mashing at sweet wort preparation. The theoretical part focuses on the technology of malt production including description of ingredients, production parts, some kinds of malt and the quality parameters. There is also described the technology of sweet wort preparation and the methods of determination of the malt quality parameters in the sweet wort there. The experimental part focuses on determination of malt extract, viscosity, haze, colour, time of starch cleavage, pH, degree of fermentation and beta-glucans content. Based on temperature dependence of parameters, the individual samples were compared and the effects of temperature were discussed. The biggest extract of light and caramel malts was explored at 70 °C, of coloured malt at 50 °C. The lowest viscosity of light and coloured malts was explored at 65 °C, of caramel malt at 50 °C. The lowest haze of wort was at 65 °C. Ideal colour of all malts was at all mashing temperatures. Ideal pH of all malts was explored at 70 °C. Ideal time of starch cleavage was explored at 70-85 °C. The biggest achievable degree of fermentation and the hugest increase of beta-glucans content were explored at 65 °C.
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SnBi Solder Paste and Influence of Reactive Nanoparticles
Rychlý, Ivo ; Špinka, Jiří (referee) ; Starý, Jiří (advisor)
This work deals with effects of nanoparticles, mainly copper and silver, on properities of lead-free solder pastes. It describes basic tests done on solder pastes according to IPC-TM-650 standards. In practical section this work focuses on the preparation of Sn-Bi solder paste and the measuring of viscosity. After that different concentrations of silver copper alloy nanoparticles are added to the SnBi solder paste. These solder pastes are tested by the IPC standarts and mechanical and resistive tests are done on printed circuit boards where the effects of mixed in nanoparticles are observed.
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Study of adhesive penetration into the wood cell wall
Janová, Petra ; Krbila, Jaromír (referee) ; Vaněrek, Jan (advisor)
This labor is based on penetration of adhesive into a wood cell walls. It focuse on adhesives basicly used for construction purposes, especially on epoxy resins. The labor contains the use of methods for precise detection adhesive in wood and methodics for choice of adhesive and wood basically used for bonding. It describes the experimentally detected dependence of contact angle on viscosity epoxy resins.
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Durability test of magnetorheological fluid at high temperature
Grygárek, David ; Strecker, Zbyněk (referee) ; Roupec, Jakub (advisor)
This bachelor’s thesis is focused on behaviour of magnetorheological fluid during the durability test. In the first part are described basic properties of MR fluid and is defi-ned parameter LDE (Lifetime Dissipated Energy), which is used for prediction of durability of MR fluid. Primary part of thesis devote to realization of experiment, which measures a part of durability test at 70°C and monitoring the yield stress, vis-cosity and residual magnetism.
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