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Production process optimization
Hejzlar, Aleš ; Vacek, Jan (referee) ; Fiala, Alois (advisor)
This diploma thesis deals with the production process optimization. The cutting operation and the lathe-turning issue is described in this thesis. In the practical part the production process is analyzed, the designed experiment (DOE) is suggested and evaluated. In the end of the practical part there is the evaluation of the machined material in the light of microstructure. On the basis of the partial findings the enclosures are done and the recommendations leading to the production optimization are suggested.
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Production process optimization
Drábková, Veronika ; Jankových, Róbert (referee) ; Fiala, Alois (advisor)
This master´s thesis is aimed at the strategy and implementation of DOE (planned experiment) and QFD (quality function deployment) in business. There are described about these methods. It deals with their use for a given problem. The last section provides a possible procedure in the enterprise.
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Obtaining and complex charaterization of Aronia spp. extracts
Seidlová, Kateřina ; Zemanová, Jana (referee) ; Veselá, Mária (advisor)
Aronia (Aronia melanocarpa) is a berry fruit with distinctive sensory characteristics and health-promoting properties. Polyphenols are the main bioactive compounds found in aronia including natural pigments – anthocyanins. Bioactive compounds are usually obtained from natural materials by extraction, in this work, two methods of extraction were compared – maceration and PHWE. Based on the total phenolic content, maceration was chosen as a more suitable method and then was optimized with statistical model – Design of Experiment. Optimal conditions were set to temperature of 30 °C, extraction agent 50 % ethanol, solid-solvent ratio 10 g per 50 ml and time of extraction for 30 minutes. Extract obtained under these conditions was characterised by total phenolic content – 1441 ± 90 mg/100 g DW, total anthocyanin content 943 ± 8 mg/100 g DW and antioxidation activity by ABTS 24,78 ± 0,09 molTE/g. In total of 25 volatile compounds were indentified in the optimal extract with content > 0,5 %. Major part created aldehydes and esters, with the main compounds being benzaldehyde (32,25 %) and methyl hexanoate (21,37 %).
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Machining of bio-composite materials
Obid, Daniel ; Slaný, Martin (referee) ; Zouhar, Jan (advisor)
This diploma thesis is focused on machining of composite materials mainly from natural fibers. The first part describes the production of composite materials and the methods used for their machining. The practical part of the work is devoted to the study of the influence of tool choice and cutting conditions on the cutting process and the quality of machined surfaces. The measured data are analysed using regression analysis.
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Obtaining and complex charaterization of Plectranthus spp. extracts
Boboková, Alexandra ; Saláková, Alena (referee) ; Vítová, Eva (advisor)
Plectranthus amboinicus is a herb that was found to have a lot of bioactive compounds, most of them are polyfenolic compounds. Extraction is neccesary to obtain bioactive compounds and to use them subsequently in food or cosmetic industry. Three methods of extraxtion – maceraction, PHWE and PFE, were used in this study. The best yield of extracted polyfenols was observed by maceration. Maceration was, in the next step, optimized using mathematical statistical method of planned experiment (DOE). The optimal conditions found for extraction were: temperature 60 °C, solvent 40% ethanol, time 90 minutes, solid-solvent ratio 1:10. Total phenolic compunds content in this extract was 0,18 ± 0,05 mgGAE·ml-1, which means 1,83 ± 0,53 mgGAE·g-1 of plant. The antioxidant activity was 148,69 ± 26,92 gTEACml-1. Percentage of radical scavenging activity ABTS•+ was 30,03 ± 5,44 %. Further, 27 of volatile aroma compounds were identified in optimal extract, the most important were: -selinene (16,67 %), trans--bergamotene (14,22 %), caryophyllene (14,11 %), 3-carene (8,22 %), -copaene (7,55 %), -terpinene (6,28 %), humulene (5,87 %), cadina-1(10)-4-diene (5,19 %).
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Foaming of fermentation residues during a vacuum evaporation
Knob, Jan ; Brummer, Vladimír (referee) ; Vondra, Marek (advisor)
The diploma thesis deals with the processing of digestate, which is the remaining material after biogas production. It aims to experimentally prove how chosen operational parameters of antifoaming agents influence digestate foaming associated with the vacuum evaporating technology. Based on the research of available antifoamers and the issue of digestate foaming itself, it was observed how three selected antifoamers (i.e. rapeseed oil, silicone antifoamer Erbslöh Schaum-ex and oleic acid), together with the decrease in the pH factor of the evaporating digestate, influence the final foam production. For the purposes of the research, an apparatus simulating the vacuum evaporating process was set up in which the heated sample was brought to boil by gradual pressure decrease. The process of foaming was observed in a transparent cylinder of a testing culumn. The essential part of the experimental activity is represented by a planned experiment which by means of a DoE (Design of experiments) method proved rapeseed oil to be very efficient. In contrast, other antifoamers, as well as the influence of the pH factor decrease, manifested themselves as insignificant factors, while the oleic acid even supported the foaming. The supplementary measurements led to a more detailed research of the effects of rapeseed oil and to the construction of a mathematical model describing how the concentration of rapeseed oil undermines the amount of generated foam. The main contribution of the thesis is firstly the evidence that rapeseed oil plays an important part in the reduction process of digestate foaming and secondly the determination of minimum substance concentration leading to the foaming reduction of a particular sample which is considered efficient enough to enable functioning of a vacuum evaporator. The thesis has also experimentally demonstrated the influence of some polymer organic flocculants which have been proved to support the foaming.
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Design of experiment on a washer extractor
Těthal, Josef ; Šomplák, Radovan (referee) ; Kuba, Pavel (advisor)
This bachelor thesis deals in the first part with research regarding the laundry process and introduction to design of experiments. The next part, which is the output of this work, describes an experiment made. The experiment defines the impact of rinsing temperature and spin speeds on consequential humidity of the laundry.
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Operational safety of mobile robots in indoor environment
Vojta, Jakub ; Věchet, Stanislav (referee) ; Krejsa, Jiří (advisor)
During cooperation with the Bender Robotics company a need for operational safety assessment of an autonomous mobile robot (AMR) emerged. Operational safety evaluation is a step towards mass production of the studied robot. Market entry of a product requires a string of various actions and safety assessment is one of them. For risk identification and severity rating were used legal requirements, best practice given by standards, FMEA method, experiment and RIPRAN method. Threats, possible scenarios and risks analysis is systematically discussed through all areas of operation of the robot, from design and construction to control software. All the steps are described in logical order. Starting with information research, going on with series of analysis and ending with suggestions for increased operational safety of autonomous mobile robots.
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Design of Experiment
Holec, Tomáš ; Popela, Pavel (referee) ; Bednář, Josef (advisor)
In this thesis, the design of experiment is studied. Firstly, a theoretic background in mathematical statistics necessary for understanding is built (chapter 2). The design of experiment is then presented in chapters 3 and 4. Chapter 3 is divided into several subchapters in which its brief history is provided as well as its complex theoretic description (basic principles, steps for planning, etc.). Chapter 4 deals with particular types of the design of experiment (Factorial experiments or Response surface design). Simple examples are provided to illustrate the theory in chapters 3 and 4. Last part of the thesis is strictly practical and focuses on an application of the theory for particular data sets and its evaluation (chapter 5).
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