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Functional TiO2 layers on fiber structures
Bečár, Tomáš ; Chladil, Ladislav (referee) ; Bača, Petr (advisor)
This thesis deals with the formation of functional layers on fibrous structures. The aim of the thesis is to deposit a titanium dioxide film on glass fibres for its use as an additive in lead acid batteries. The work includes a survey of methods of titanium dioxide deposition on glass substrate, a review of measuring and recording equipment and a structural analysis of the materials used. As a result of the work, experiments of titanium dioxide deposition on filter paper and glass fibers will be developed along with their analysis. The evaluation of the analyses will be followed by a proposal for the use of these functional layers in possible applications.
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Preparation and characterization of nanostructured III-V semiconductor materials
Maniš, Jaroslav ; Kostelník,, Petr (referee) ; Hospodková,, Alice (referee) ; Šikola, Tomáš (advisor)
Předkládaná dizertační práce se zabývá výrobou a analýzou gallium nitridových (GaN) nanostruktur ve třech odlišných formách. V prvním případě byl zkoumám trojdimenzionální GaN ve formě nanokrystalů rostených na grafenu. Nanokrystaly byly připraveny s využitím techniky droplet epitaxy, která mimo jiné umožňuje růst nanostruktur za nízké teploty substrátu (T = 200°C). Studium se zaměřovalo jak na charakterizaci kvality připravených nanokrystalů, tak na statistický popis růstu. V dalším kroku byly připravené struktury využity pro výrobu fotodektoru citlivého na ultrafialové světlo. Výroba fotodektoru a jeho úspěšné použití slouží jako základ pro navazující výzkum. Ve druhém případě byly studovány dvoudimenzionální GaN nanostruktury, které byly rovněž připraveny za nízké teploty křemíkového substrátu. Následná analýza se soustředila na popis krystalové struktury a prvkovou analýzu, neboť byly takovéto struktury pozorovány vůbec poprvé. Další rozvoj možností přípravy těchto nanostruktur je předmětem navazujícího výzkumu. Ve třetím případě byly zkoumány jednodimenzionální GaN nanodráty připravené na safírovém substrátu. Účelem tohoto projektu bylo získání datasetu pro ověření teoretického modelu, který popisuje růst horizontálních nanodrátů. Na základě sběru a analýzy dat se podařilo modelovat růstovou dynamiku GaN nanodrátů, která byly v souladu s teoretickým modelem.
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New Areas of the Ultrasonic Application in Microelectronics Technology
Buršík, Martin ; Pietriková, Alena (referee) ; Králová,, Iva (referee) ; Szendiuch, Ivan (advisor)
Doctoral thesis deals with the deposition of special thixotropic materials for microelectronic technology. The aim of the work is the development of the new method optimizing the dosing process in order to achieve a print resolution of better than 100 microns. The work includes the development of a special dispensing head (UZD) using the influence of ultrasonic energy. These results demonstrate the possibility of a newly developed method that is able to print thixotropic materials with a resolution of 65 microns. Compared to other methods achieves these results with the commonly used materials for thick film technology with particle size up to 5 microns.
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The oxygen modification of the graphene structures for biosensors
Mikerásek, Vojtěch ; Bartošík, Miroslav (referee) ; Mach, Jindřich (advisor)
The bachelor thesis deals with the modification of CVD graphene by oxygen atoms. The theoretical part describe the structure of graphene oxide and its physical properties. Methods of production of this material and its use in biosensors are also described. The practical part describes the preparation of monolayer graphene on a silicon wafer. The main attention was paid to the oxidation of graphene by atomic oxygen and its modification in oxygen plasma. The samples were measured during process of oxidation at individual time intervals using XPS.
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Effect of Organic Additives on Electrochemical Processes Influencing Zn-Air Battery parameters
Smejkal, Jan ; Čech, Ondřej (referee) ; Chladil, Ladislav (advisor)
The diploma thesis is focused on the study of the influence of selected organic additives on the properties and morphology of zinc deposit on the negative electrode when used in zinc-air accumulators. Organic additives have been selected based on the study of literature and previously done experiments. The deposition was made on the tin plate electrodes in a solution of 6 mol/l KOH saturated with ZnO with added additives. All chosen additives were studied with a focus on the morphology of zinc deposit and with regard to their ability to suppress dendritic growth. Zinc morphology was studied by using a Tescan Vega 3 electron microscope and a Rigaku MiniFlex HR 600 X-ray diffractometer.
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Deposition of inhaled particles in a model of child lungs
Čederle, Jakub ; Pokorný, Jan (referee) ; Lízal, František (advisor)
This thesis presents a summary of research of deposition of inhaled particles in children’s respiratory system which was mainly conducted on realistic model of children's lungs. Experimental part introduces BUT model representing airways of 5-years-old child which served for measurements of regional deposition. Bachelor's thesis furthermore sums up basic knowledge of respiratory system and points out anatomical and physiological differences between children and adults in given field. There are described basic deposition mechanisms and their impact on aerosol therapy as well.
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Measurement and analysis of deposition of fibers from mineral wool in respiratory system
Hájek, Ondřej ; Elcner, Jakub (referee) ; Lízal, František (advisor)
This master thesis deals with inhalation of fine particles and fibres into human lungs. This is a scientific field where computer modelling is used to describe the movement of fibres and their deposition in the lungs. However, the results of these simulations must be verified experimentally. The prediction of fibres behaviour is important from a toxicology point of view where it is important to know deposition hot-spots and places where fibres could possibly cause problems. The review of the state-of-the-art is focused on the deposition of particles in human lungs followed with a chapter on fibre as a type of particle, and occupational exposure limits set by different world associations. The last theoretical chapter describes human lungs and its diseases which can evolve when limits for occupational exposure are not met. The experimental chapter consists of a description of the used experimental setup and results from an experiment together with a comparison of results with other similar experiments.
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Deposition of Molecular Magnets on „2D“ Materials
Vavrečková, Šárka ; Musálek, Tomáš (referee) ; Hrubý, Jakub (advisor)
This thesis deals with deposition of single-molecule magnets on 2D materials and studies their behavior on surfaces. Theoretical part contains information about properties of single-molecule magnets, deposition methods and also information about chosen 2D materials – graphene and molybdenum disulfide. Further, the physical principles of the selected characterization methods (atomic force microscopy, Raman spectroscopy, X-ray photoelectron spectroscopy and electron paramagnetic resonance) are described. In the experimental part graphene and molybdenum disulfide were exfoliated. Afterwards, depositions of single-molecule magnets from solution and by thermal sublimation were made. After that, samples were analyzed using the mentioned methods and results were discussed.
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