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The Technology Of Ceramic Packages
Skácel, Josef
This paper deals with the technology of ceramic packages. The first part is about ceramic in general. The next part is focused on used material Nabaltec and advantages of this type of technology i.e. ceramic powder pressing followed by the milling of the pressed ceramic and shows disadvantages of this technology step. The inspection was done by SEM pictures and shows the difference between sintered and unsintered ceramic. The last part is a simulation with 120mW power load and shows temperature distribution on the ceramic package compared with mold compound as the packaging material.
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Utilization of mica separated from washed kaolin
Vaculík, Josef ; Ptáček, Petr (referee) ; Opravil, Tomáš (advisor)
The Master’s Thesis aims to laboratory test the possibilities of utilization mica separate, which arises during the process of floating kaolin as a by-product together with sand. Mica and sand are then separated by flotation or vibration. The mica separate thus formed was subjected to analysis. XRD and heating microscopy methods were used for analysis. Subsequently, experiments with mica separation as a filler in composites based on epoxy resins were set up and performed. Furthermore, the separate was tested as a part of plasters and visual building elements. Last but not least, the separate was mixed into the ceramic, which was then subjected to firing in the selected mode. The diploma thesis provides a comprehensive overview of the above-mentioned possibilities of using mica separation, which is based on a sufficient amount of experimental data.
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RAKO, Jano Koehler and the way of the cross on Svatý Hostýn
Vacková, Veronika ; Czumalo, Vladimír (advisor) ; Šmied, Miroslav (referee)
The bachelor thesis will focus on the way of the cross on Svatý Hostýn made by RAKO company and designed by Jano Koehler. The author will present a mosaic art in general, the RAKO company and its influence on Czech art culture and Jano Koehler's personality and work. In the core part of thesis, the author will carry out with technological, formal and iconographic analysis of the individual stations of the way of the cross. Another works made in a ceramic mosaic created within a time before or after Svaty Hostyn cycle will be included in next chapters. Furthermore, the author will deal with the problematic of historical preservation and the previous experience with restoration works made up to now. An attachment of visuals will be a part of thesis. Key words Way of the cross, Svatý Hostýn, Jano Koehler, RAKO, Emil Sommerschuh, mosaic, ceramic, catholic modern art
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Thermophysical and electrical properties of illite-based ceramics
Csáki, Štefan ; Dobroň, Patrik (advisor)
CSÁKI, Štefan: Thermophysical and electrical properties of illite-based ceramics. [Doctoral thesis]. Constantine the Philosopher University in Nitra. Faculty of Natural Sciences. Charles University. Faculty of Mathematics and Physics. Supervisor: prof. RNDr. Libor Vozár, CSc. (Constantine the Philosopher University in Nitra), doc. Ing. Patrik Dobroň, PhD. (Charles University). Nitra & Prague, 2018. 107 p. Illitic clays are of special importance in the ceramic industry. Therefore, a deep knowledge of the thermophysical processes, as well as the electric properties, is of special importance. The illitic clay originated in Northeastern Hungary was used in this thesis. The reactions, occurring during firing, were studied using thermal analyses (Differential thermal analysis, Thermogravimetry, Thermodilatometry) and special attention was paid to the measurement of the electrical conductivity (both DC and AC). Up to 250 řC, where the removal of the physically bond water (PBW) takes place, the dominant charge carriers were the H+ and OH- ions. After the PBW was removed, Na+ and K+ ions became the dominant charge carriers. During dehydroxylation (450 - 750 řC) H+ and OH- ions were freed from the illite structure, which supported the electrical conduction in the samples. At ~ 970 řC glassy phase appeared...
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Diagnostic Methods Suitable for Monitoring of Drying Process of Brick Product
Sarvaš, Ondřej ; Sokolář, Radomír (referee) ; Nevřivová, Lenka (advisor)
This work deals with the study of diagnostic methods suitable for monitoring of the drying process of brick raw materials. Based on the extensive literature search, several parameters are selected, which are appropriate to monitoring during drying. In addition, a methodology for measuring these selected parameters is proposed. In the experimental part, the use of all described methods is gradually verified on the brick raw material with and without shortening additive (also known as grog). Was carried out: measurement of the surface temperature in the climatic chamber, determination of humidity distribution in the sample, determination of moisture diffusivity, determination of tensile strength, determination of ultrasonic wave velocity and determination of dynamic E-modulus of elasticity. Results of experiments and the gained experiences show, that at least two of the above-mentioned monitoring methods are very appropriate and beneficial – determination of moisture diffusivity and determination of tensile strength. In the work was described in detail the procedure of determination of moisture diffusivity of material. The dependence of moisture diffusivity on the moisture content of the dried material, has been described. Also, differences between raw material with grog and without grog has been described. As part of the practical verification of the experiment designed to determine the tensile strength at different humidity levels of test samples. A new shape of the test specimens and a new device were designed to allow them to be attached to a hydraulic press. The results of this work show that the tensile strength of the ceramic green bodies is primarily dependent on the moisture content of the material. The type of raw material almost does not affect the tensile strength.
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Thermophysical and electrical properties of illite-based ceramics
Csáki, Štefan ; Dobroň, Patrik (advisor) ; Koštial, Pavol (referee) ; Labaš, Vladimír (referee)
CSÁKI, Štefan: Thermophysical and electrical properties of illite-based ceramics. [Doctoral thesis]. Constantine the Philosopher University in Nitra. Faculty of Natural Sciences. Charles University. Faculty of Mathematics and Physics. Supervisor: prof. RNDr. Libor Vozár, CSc. (Constantine the Philosopher University in Nitra), doc. Ing. Patrik Dobroň, PhD. (Charles University). Nitra & Prague, 2018. 107 p. Illitic clays are of special importance in the ceramic industry. Therefore, a deep knowledge of the thermophysical processes, as well as the electric properties, is of special importance. The illitic clay originated in Northeastern Hungary was used in this thesis. The reactions, occurring during firing, were studied using thermal analyses (Differential thermal analysis, Thermogravimetry, Thermodilatometry) and special attention was paid to the measurement of the electrical conductivity (both DC and AC). Up to 250 řC, where the removal of the physically bond water (PBW) takes place, the dominant charge carriers were the H+ and OH- ions. After the PBW was removed, Na+ and K+ ions became the dominant charge carriers. During dehydroxylation (450 - 750 řC) H+ and OH- ions were freed from the illite structure, which supported the electrical conduction in the samples. At ~ 970 řC glassy phase appeared...
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Stará Kouřim- the revision of the selected sections from the archeological excavasion made by M. Šolle.
Dvořáček, Daniel ; Štefan, Ivo (advisor) ; Varadzin, Ladislav (referee)
This thesis deals with the revision of archaeological research at Stará Kou im. This locality was excavated between 1948 and 1957 by M. Šolle. Sixty years after the end of the Stará Kou im research, some conclusions need to be reinterpreted. The paper was mainly focused on the revision of the middle fortifications research and brought new, unpublished results. Key words: early middle age, hillfort, fortification, revision, ceramic, Old Kou im.
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Behaviour of the Interface of Low Toughness Materials
Halasová, Martina ; Pabst, Willi (referee) ; Tatarko, Peter (referee) ; Fintová, Stanislava (referee) ; Chlup, Zdeněk (advisor)
The work is focused on evaluation of factors influencing behaviour of interface in low toughness ceramic materials reinforced with fibres. The main aim was to characterise processing effects influencing the quality of fibre-matrix interface, with respect to final behaviour of composites at various loading type. The partial goal was to map the possibility of influencing the composite material by choice of matrix material, eventually by change of its processing, leading to change of interfacial properties without need of modification of reinforcement surface. The materials used in studied composites as a matrix were based on thermal transformation of polymer precursors, thus, the resulting materials were characterised in partially as well as in fully pyrolyzed state. Behaviour of interface in cpomposite materials was first evaluated from the global behaviour (i.e., change of mechanical properties) and in chosen representative composites also from the point of local changes in close surrounding of the interface (i.e., microstructure, chemical processes, fracture-mechanic processes, etc.) due to thermal exposition. In experiment were used particularly composite materials prepared by pyrolysis of polysiloxane resins reinforced by basalt fibres or Nextel™720 fibres. With respect to thermal resistance of the reinforcement, the basalt reinforced composites contained only partially pyrolyzed matrix (i.e., to temperature of 800°C), and in composites with Nextel™720 reinforcement was the matrix in form of fully pyrolyzed polymer into ceramic (SiOC). At partial pyrolysis of polysiloxane resin occurs rapid change of behaviour at temperature of 600°C. It was demonstrated, that around this temperature the formed interface with basalt fibre exhibits optimum adhesion/strength, allowing to reach sufficient level of composite strength at acceptable fracture toughness. Above temperature of 750°C occur significant difusion processes in the area of the interface and formation of new crystalline phases in the fibre, what deteriorates the fibre strength, and on the contrary, strengthen the interface cohesion, what leads to degradation of properties of the whole composite. At composite materials determined for high temperatures, reinforced by Nextel™720 fibres, was detected significant resistivity against oxidation caused especially by fully pyrolyzed matrix. As similarly important factor was observed the formation of mullite interphase in surface area of the fibre. Volume changes caused by formation of the interphase, difusional transport of the matter and thermal exposition led to formation of thermally and stress-induced micro-cracks, weakening interfacial surrounding in matrix as well as in fibre. This mechanism in contrast to amplifying chemical bond between fibre and matrix led to preserving of the composite properties also at high temperatures up to 1500°C. The work also dealed with effects of loading rate, where in contrast to static loading were observed different failure mechanisms. Realized research led to description and explanation of the influence of the fibre-matrix interface by change of matrix material processing parameters, which allow processing of economically advantageous and thermally stable composite.
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Determination of acoustic properties of brick body
Hladík, Lukáš ; Skotal, Zbyněk (referee) ; Sokolář, Radomír (advisor)
Bachelor thesis deals with the possibility of increasing the index of the air soundless the wall brick forms. The theoretical part summarizes the present knowledge in the field of acoustic properties of the ceramic shard and also the theory and methodology of the appraisal the index of the air soundless of building materials. Then there is the possibility of using ultrasound for indirect appraisal of the index the air soundless of a brick shard described both in the theoretical part in the form of a research of existing sources and in the practical part.
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