Original title:
Development of a tube nebulizer for microflow atmospheric pressure chemical ionization mass spectrometry
Authors:
Strmeň, Timotej ; Vrkoslav, Vladimír ; Pačes, Ondřej ; Cvačka, Josef Document type: Papers Conference/Event: International Students Conference ”Modern Analytical Chemistry” /13./, Prague (CZ), 20170921
Year:
2017
Language:
eng Abstract:
A novel nebulizer for microflow atmospheric pressure chemical ionization mass spectrometry was developed. It consisted of a tube with analyte-transporting fused silica capillary inside. The terminal part of the tube was resistively heated using a coiled resistance wire. Optimal nebulizer parameters and construction setup were investigated to fully demonstrate its versability. Corundum appeared to be a more suitable material than quartz for fabrication of the tube nebulizer. The lowest analyte flow rate investigated was 1.0 mul/min with an excellent signal stability reached.
Keywords:
mass spectrometry; micro-APCI; tube nebulizer Project no.: GA16-01639S (CEP) Funding provider: GA ČR Host item entry: Proceedings of the 13th International Students Conference ”Modern Analytical Chemistry”, ISBN 978-80-7444-052-6
Institution: Institute of Organic Chemistry and Biochemistry AS ČR
(web)
Document availability information: Fulltext is available at the institute of the Academy of Sciences. Original record: http://hdl.handle.net/11104/0274992