Národní úložiště šedé literatury Nalezeno 16 záznamů.  1 - 10další  přejít na záznam: Hledání trvalo 0.01 vteřin. 
MICROSTRUCTURE AND COMPOSITION OF FINE PARTICLES RELEASED BY CAR BRAKING
Švábenská, Eva ; Roupcová, Pavla ; Pizúrová, Naděžda ; Schneeweiss, Oldřich
Vehicular traffic is connected with large volume of fine particles released during brake processes of cars. Our research is focused on the phase, structure and chemical analysis of the fine particles taken from some car brake parts by their services. The information on structure and phase composition was obtained by X-Ray Powder Diffraction, Mossbauer Spectroscopy, scanning electron microscopy with EDX and transmission electron microscopy. The results of the wear debris analysis are compared with original brake materials components. Most of recognized particles are based mainly on iron oxides. Wear brake particles are discussed in the relation to the potential risk to the environment and human health.
MICROSTRUCTURE AND COMPOSITION OF FINE PARTICLES RELEASED BY CAR BRAKING
Švábenská, Eva ; Roupcová, Pavla ; Pizúrová, Naděžda ; Schneeweiss, Oldřich
Vehicular traffic is connected with large volume of fine particles released during brake processes of cars. Our research is focused on the phase, structure and chemical analysis of the fine particles taken from some car brake parts by their services. The information on structure and phase composition was obtained by X-Ray Powder Diffraction, Mossbauer Spectroscopy, scanning electron microscopy with EDX and transmission electron microscopy. The results of the wear debris analysis are compared with original brake materials components. Most of recognized particles are based mainly on iron oxides. Wear brake particles are discussed in the relation to the potential risk to the environment and human health.
HIGH - TEMPERATURE CREEP BEHAVIOUR OF CAST COBALT-BASE SUPERALLOYS
Dvořák, Jiří ; Král, Petr ; Kvapilová, Marie ; Hrbáček, Karel ; Sklenička, Václav
Two cast and heat-treated NbC and TaC – strengthened cobalt superalloys have been developed for a precision casting of spinner discs for glass wool industry. In this work constant load creep tests in tension were carried out in argon atmosphere at three testing temperature 900, 950 and 1000 °C and at the initial applied stresses ranged from 40 to 200 MPa. All the tests were continued until the final fracture. The results of creep testing were combined with microstructural and fractographic examinations by means of light and scanning electron microscopy. A mutual comparison of creep characteristics of the investigated superalloys under comparable creep loading conditions showed that NbC-strengthened superalloy exhibited longer creep life than TaC-strengthened one. Further, it was found that carbide precipitation is the primary strengthening mechanism in both cobalt-base superalloys under investigation and the amount, morphology\nand type of carbides have the decisive effect on the creep properties including creep damage and fracture processes. By contrast, NbC-superalloy exhibited a more brittle character of creep fracture mode than TaCstrengthened superalloy. This study was initiated to investigate in more details creep deformation processes and the effect of the creep microstructure and damage evolution on both investigated superalloys. The different behaviour and properties of studied superalloys were explained based on the received results of this study.
Quantum-mechanical study of magnetic properties of superalloy nanocomposite phase Fe2AlTi
Slávik, Anton ; Miháliková, Ivana ; Friák, Martin ; Všianská, Monika ; Šob, Mojmír
The L21-structure Fe2AlTi intermetallic compound is one of the two phases identified in Fe-Al-Ti superalloy nanocomposites. Experimental data related to low-temperature magnetic properties of this Heusler compound indicate that magnetic moment is about 0.1 Bohr magneton per formula unit. In contrast, previous quantum-mechanical calculations predicted Fe2AlTi to have much higher magnetic moment, 0.9 Bohr magneton per formula unit. In order to solve this discrepancy between the theory and experiment we have performed a series of quantum-mechanical fix-spin-moment calculations and compared our results with those for non-magnetic state. It turns out that the total energy of the non-magnetic state is only by 10.73 meV/atom higher than that of the magnetic state. When applying Boltzmann statistics to this very small energy difference we predict that the non-magnetic state appears at non-zero temperatures with significant probabilities (for instance, 22.36 % at T = 100 K) and reduces the overall magnetic moment. As another mechanism lowering the magnetization we studied selected shape deformations, in particular trigonal shearing. Fe2AlTi exhibits a compression-tension asymmetry with respect to these strains and, for example, the strain 0.08 destabilizes the spin-polarized state, leaving the non-magnetic state as the only stable one.
First-principles study of interface energies in Fe-Al-based superalloy nanocomposites
Miháliková, Ivana ; Slávik, Anton ; Friák, Martin ; Všianská, Monika ; Koutná, N. ; Holec, David ; Šob, Mojmír
Fe-Al-based nanocomposites with a superalloy-type of microstructure constitute a very promising class of materials. They possess a great potential as an alternative to the currently used steel grades in high temperature applications. Intermetallics-containing nanocomposites, such as those with the Fe3Al compound being one of the phases, may open a way towards future automotive and energy-conversion technologies with lower fuel consumption and reduced environmental impact. We employ quantum-mechanical calculations to analyze relations between ordering tendencies of Al atoms in the disordered Fe-18.75at.%Al phase on one hand and thermodynamic, structural and magnetic properties of Fe-Al-based nanocomposites on the other. When comparing supercells modeling disordered Fe-Al phase with different atomic distribution of atoms we find out that the supercell without 1st and 2nd nearest neighbor Al-Al pairs has a lower energy than that mimicking a perfect disorder (a special quasi-random structure, SQS). Further, coherent interfaces with (001), (110) and (1-10) crystallographic orientations between Fe3Al compound and SQS Fe-Al phase have higher energies than those exhibiting atomic distribution without 1st and 2nd nearest neighbor Al-Al pairs.
Fatigue crack initiation and growth in 316L steel in torsional cyclic loading
Karol, Michal ; Chlupová, Alice ; Mazánová, Veronika ; Kruml, Tomáš
Fatigue crack initiation and growth study in 316L austenitic stainless steel was made in cyclic\ntorsion. The experiments on hollow cylindrical specimens were performed at room temperature using fully reversed shear strain controlled cycles. The specimens used were polished mechanically and electrolytically to enable surface damage and crack propagation observation using optical light microscope, SEM. It was found that high density of extrusions and intrusions are formed on the specimen surface due to cyclic loading. TEM observations revealed that dislocation arrangement in well-known ladder-like structure is responsible for the localization of cyclic plastic deformation and for the origin of surface roughness in which the fatigue crack nucleate. The path of fatigue cracks leading to failure was observed, too. The crack path\nwas found to be dependent upon the applied shear strain amplitude.
Effect of the load eccentricity on fracture behaviour of cementitious materials subjected to the modified compact tension test
Seitl, Stanislav ; Ríos, J. D. ; Cifuentes, H. ; Veselý, V.
Fracture properties of quasi-brittle cementitious composites are typically determined from the load–displacement response recorded during a fracture test by using the work-of-fracture method or possibly other relevant fracture models. Our contribution is focused on a set of experimental tests which are used to study the fracture behaviour on notched dog-bone-shaped specimens made of cementitious materials. These specimens are subjected to modified compact tension (ModCT) test under a specific range of eccentricity of the tensile load. This type of test generates a stress state in the specimen ligament which combines a direct tension with a defined level of bending due to eccentricity of the tensile load. Several values of relative notch length are also considered. While the crack propagates, a variety of stress states, resulting in variations in the crack-tip stress and deformation constraint, appears in the ligament zone because of the changes in the eccentricity of the applied load, which influences the fracture behaviour of the investigated specimens. The K-calibration, T-stress, CMOD and COD curves for ModCT specimens are introduced and variations of these curves with varying load eccentricity are discussed.
Quantum-mechanical study of tensorial elastic and high-temperature thermodynamic properties of grain boundary states in superalloy-phase Ni3Al
Friák, Martin ; Všianská, Monika ; Holec, D. ; Šob, Mojmír
Grain boundaries (GBs), the most important defects in solids and their properties are crucial for many materials properties including (in-)stability. Quantum-mechanical methods can reliably compute properties of GBs and we use them to analyze (tensorial) anisotropic elastic properties of interface states associated with GBs in one of the most important intermetallic compounds for industrial applications, Ni3Al. Selecting the Sigma 5(210) GBs as a case study because of its significant extra volume, we address the mechanical stability of the GB interface states by checking elasticity-based Born stability criteria. One critically important elastic constant, C 55, is found nearly three times smaller at the GB compared with the bulk, contributing thus to the reduction of the mechanical stability of Ni3Al polycrystals. Next, comparing properties of Sigma 5(210) GB state which is fully relaxed with those of a Sigma 5(210) GB state when the supercell dimensions are kept equal to those in the bulk we conclude that lateral relaxations have only marginal impact on the studied properties. Having the complete elastic tensor of Sigma 5(210) GB states we combine Green's-function based homogenization techniques and an approximative approach to the Debye model to compare thermodynamic properties of a perfect Ni3Al bulk and the Sigma 5(210) GB states. In particular, significant reduction of the melting temperature (to 79-81% of the bulk value) is predicted for nanometer-size grains.
Estimation of Anisotropy of Creep Properties in Al and Mg Alloys by Means of Small Punch Test
Dobeš, Ferdinand ; Dymáček, Petr
Small punch test was used to determine the properties of light alloys and composites in various directions. Three different materials were studied:\n(i) magnesium alloy WE54 prepared by a powder metallurgical route with final hot extrusion,\n(ii) aluminium alloy reinforced with 20 vol. % of Saffil fibres with planar orientation, and\n(iii) Al-Al4C3 composite prepared by mechanical alloying and subjected to equal channel angularpressing as a final step.\nSmall punch tests were performed under constant force at elevated temperatures. The observed orientation dependence of creep properties is strongly material dependent. The results confirm the feasibility of the small punch test for determination of anisotropy of mechanical properties.
Lifetime Assessment of Particulate Ceramic Composite with Residual Stresses
Náhlík, Luboš ; Majer, Zdeněk ; Štegnerová, Kateřina ; Hutař, Pavel
A micro-crack propagation in particulate ceramic based composite was studied using finite element method (FEM). Subcritical crack growth (SCG) was numerically simulated under complex load conditions (mechanical loading and loading by internal residual stresses). The effect of residual stresses on the crack propagation was studied. Two-dimensional computational model of particulate ceramic composite with material properties corresponding to low temperature co-fired ceramics (LTCC) was developed. The results indicate that the presence of residual stresses significantly reduces values of stress intensity factor in the vicinity of composite surface and the direction of residual stresses around the particles contributes to the micro-crack deflection from the particles. The time to failure of the composite under mechanical loading was determined. Results obtained contribute to a better understanding of the role of residual stresses during micro-crack propagation in ceramic particulate composites.

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