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Problems of Drug Residues Determination in Waste Waters
Lisá, Hana ; Márová, Ivana (referee) ; Hajšlová, Jana (referee) ; Kráčmar, Stanislav (referee) ; Vávrová, Milada (advisor)
The PhD thesis deals with determination of sulfonamides and tetracyclines in waste waters. Sulphonamides and tetracyclines are widely used in human and veterinary medicine. They are biologically active compounds and block biological processes in waste water treatment plants. These substances can influence microorganisms in the environment. Sulphonamides and tetracyclines induce resistance in low concentrations. These substances penetrate into the environment from industrial production, use in households, hospitals, veterinary clinics and fish farms. Tetracyclines and sulphonamides were determined in waste water from waste water treatment plants in Brno. Optimalization of extraction of these compounds was performed by solid phase extraction. Sulphonamides and tetracyclines were determined by liquid chromatography coupled with diode array detector or coupled with mass spectrometry. Optimalized method was used for determination tetracyclines and sulphonamides in waste water from waste water treatment plants in Brno in years 2007 – 2010.
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Removal of micropolutants in drinking water treatment
Hambálková, Kateřina ; Vávrová, Milada (referee) ; Dolejš, Petr (advisor)
Intrusion of pharmaceuticals into surface and drinking water is nowadays a problem, that is solved all over the world. This diploma thesis is focused on the removal of pharmaceuticals from water by coagulation. The efficiency of two coagulant agents - chitosan and ferric sulphate was compared. For comparison was used adsorption on a granular-activated-carbon. Efficiency of removal was investigated by UV-VIS spectrophotometer and HPLC.
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Study of the availability of antibiotics in soil
Hroncová, Michala ; Landová, Pavlína (referee) ; Řezáčová, Veronika (advisor)
The diploma thesis is focused on the determination of tetracyclines, sulfonamides and fluoroquinolones from soil. Antibiotics such as tetracycline, chlortetracycline, oxytetracycline. ciprofloxacin, trimethoprim, sulfamethaxazole and sulfadiazin were selected due to frequent use in veterinary medicine. Due to the fact that the soil is a complex matrix and contains many components that can interfere with the detection signal of analytes, it was necessary to use the MAX column in the SPE method, which removes fulvic aned humic acid from analytes and the HLB column Final analysis of the analytes was performed by liquid chromatography with mass detesction (LC-MS). The method was also used for real soil samples, which were delivered from ÚKZUS.
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Study of the availability of antibiotics in soil
Hroncová, Michala ; Landová, Pavlína (referee) ; Řezáčová, Veronika (advisor)
The diploma thesis is focused on the determination of tetracyclines, sulfonamides and fluoroquinolones from soil. Antibiotics such as tetracycline, chlortetracycline, oxytetracycline. ciprofloxacin, trimethoprim, sulfamethaxazole and sulfadiazin were selected due to frequent use in veterinary medicine. Due to the fact that the soil is a complex matrix and contains many components that can interfere with the detection signal of analytes, it was necessary to use the MAX column in the SPE method, which removes fulvic aned humic acid from analytes and the HLB column Final analysis of the analytes was performed by liquid chromatography with mass detesction (LC-MS). The method was also used for real soil samples, which were delivered from ÚKZUS.
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Problems of Drug Residues Determination in Waste Waters
Lisá, Hana ; Márová, Ivana (referee) ; Hajšlová, Jana (referee) ; Kráčmar, Stanislav (referee) ; Vávrová, Milada (advisor)
The PhD thesis deals with determination of sulfonamides and tetracyclines in waste waters. Sulphonamides and tetracyclines are widely used in human and veterinary medicine. They are biologically active compounds and block biological processes in waste water treatment plants. These substances can influence microorganisms in the environment. Sulphonamides and tetracyclines induce resistance in low concentrations. These substances penetrate into the environment from industrial production, use in households, hospitals, veterinary clinics and fish farms. Tetracyclines and sulphonamides were determined in waste water from waste water treatment plants in Brno. Optimalization of extraction of these compounds was performed by solid phase extraction. Sulphonamides and tetracyclines were determined by liquid chromatography coupled with diode array detector or coupled with mass spectrometry. Optimalized method was used for determination tetracyclines and sulphonamides in waste water from waste water treatment plants in Brno in years 2007 – 2010.
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Removal of micropolutants in drinking water treatment
Hambálková, Kateřina ; Vávrová, Milada (referee) ; Dolejš, Petr (advisor)
Intrusion of pharmaceuticals into surface and drinking water is nowadays a problem, that is solved all over the world. This diploma thesis is focused on the removal of pharmaceuticals from water by coagulation. The efficiency of two coagulant agents - chitosan and ferric sulphate was compared. For comparison was used adsorption on a granular-activated-carbon. Efficiency of removal was investigated by UV-VIS spectrophotometer and HPLC.
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