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Manufacture of castings from electrical copper
Janský, Vojtěch ; Lána, Ivo (referee) ; Záděra, Antonín (advisor)
The goal of this thesis is to verify influence of conditions of metallurgical treatment, used foundry technology and conditions of solidification on electrical conductivity of pure copper castings. The experiment part observe differenec between alloy melting under normal pressure and in a vacuum and betwwen casting provided with chill, insulation and natural enviroment of mould.
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Dielectric properties of liquid insulators
Jahn, Michal ; Starý, Jiří (referee) ; Špinka, Jiří (advisor)
This master‘s thesis deals with measurement of liquid dielectric materials (insulators). Above all, it is the different kinds of clean and drinking water, but also transformer oils. There was done theoretical information retrieval about the given topic in this project and on the basis of theory there were realized the relevant measurements of selected properties of liquid dielectric, such as permittivity, capacitance, loss number, conductivity, but also temperature dependence of these parameters. The measurements were realized with the help of product manufactured at the faculty FEKT VUT and with the help of measuring system AGILENT 16452A. The measured results were evaluated, graphically processed and compared.
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Effects of soil management on soil quality near Šardičky village
Schneiderová, Šárka ; Doležal, Petr (referee) ; Kameníčková, Ivana (advisor)
This diploma thesis is focused on influence of reduced tillage technology of soil processing on it´s near-surface soil layer (0 to 10 cm). The research was carried out on agricultural land near Šardičky village, where company ZEMO spol. s r.o. provides long-term use of reduced tillage technology. In 2016 the soil quality in this site was evaluated by using physical and hydrophysical parameters, results are presented in the previous bachelor thesis "Selected hydrophysical parameters as indicators of soil quality.". In diploma thesis in addition chemical and other hydrophysical properties have been evaluated to provide a comprehensive assessment of soil quality. In 2016, poppy seed was grown on this site and spring barley was grown in 2017 and 2018. Grab samples and intact soil cores were taken during the vegetation period of the crop. After three years of experimental research, in which I participated, it is possible to assess the development of individual parameters and the influence of reduced tillage technology on near-surface soil layer. The theoretical part of the diploma thesis deals with the description of the reduced tillage technology and problematics of the determination of soil parameters, which are used for evaluation of the quality of the near-surface layer. The practical part deals with evaluation of these parameters according to various authors and describes the development of soil quality during years 2016, 2017 and 2018.
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Mechanical and Electrical Properties of Thin Metal Films Deposited by Vacuum Evaporation
W. F. Yahya, Doaa ; Kolařík, Vladimír (referee) ; Štencl,, Jiří (referee) ; Šandera, Josef (advisor)
Thin layers are widely used in many fields of technology and today we can say that they are found in all modern technologies. Thin layers can be created in two ways, namely by chemical or physical means. This work focuses on the latter method, more particularly a technology of thermal evaporation of thin layers in a vacuum. The work focuses on the process principles during and after the evaporation. Much of the work focuses on the development and design of experiments. These experiments illustrate some of the phenomena that take place on thin films produced by the aforementioned technology. Work helps to better understand processes during formation of thin layers and properties that influence the quality and stability of thin films. In conclusion we describe results of experiments and new developments in the field of thin films deposition using evaporation under vakuum are summarized.
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Electrical conduction of alternative electroinsulating liquids
Reňák, Ladislav ; Rozsívalová, Zdenka (referee) ; Frk, Martin (advisor)
This labor deals with features of alternative electrical insulating liquids and also petroleum-base liquids. It examines their usage in the electrotechnical industry. The practical part of the thesis deals with measurement of absorption charakteristics of biodegradable electrical insulating liquid MIDEL 7131 and the petroleum - based transformer oil TRAFO N. The results of the measurement are examined by the help of substitutional math function.
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Mechanical properties of gel polymer electrolytes
Bárta, Vladimír ; Vondrák, Jiří (referee) ; Sedlaříková, Marie (advisor)
This work deals with the measurement of electrical conductivity and mechanical properties of gel polymer electrolyte containing Lithium ion. Their preparation and performance depends on the concentration of nanoparticles Al2O3 contained therein. The theoretical part deals with the development of gel polymer electrolyte, their use and methods of measurement of electrical conductivity and mechanical properties. In the experimental part describes the preparation of gel electrolyte, the measurement of electrical conductivity, temperature dependence and the measurement of mechanical properties.
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Dielectric Properties of Thin Tantalum and Niobium Oxide Layers
Abuetwirat, Inas Faisel ; Chobola, Zdeněk (referee) ; Lelák, Jaroslav (referee) ; Liedermann, Karel (advisor)
Dielektrická relaxační spektroskopie je jednou z užitečných metod pro studium molekulární dynamiky materiálů. Díky nedávnému pokroku v přístrojové a měřicí technice je dnes možné získat dielektrické spektrum v širokém frekvenčním intervalu a pro velice rozdílné materiály. Cílem mé práce bylo studium dielektrických relaxačních spekter a vodivosti oxidů titanu, niobu, tantalu, lanthanu a hafnia pro katody pracující na principu studené emise. Cílem výzkumu bylo analyzovat frekvenční a teplotní chování těchto oxidů, včetně jejich vodivosti, v širokém frekvenčním a teplotním rozsahu, a pokusit se stanovit původ relaxačního mechanismu. Vzhledem k tomu, že původně zadaný rozsah oxidů byl dosti široký, soustředila se pozornost pouze na oxidy tantalu a niobu, rovněž s ohledem na jejich aplikace v elektrolytických kondenzátorech. Elektrické, tepelné a mechanické (při zpracování) vlastnosti oxidů tantalu a niobu jsou dnes již dobře prozkoumány. K dispozici je však jen málo poznatků o jejich dielektrických relaxačních mechanismech. Výsledky získané pro Ta2O5 ukazují existence relaxačního maxima, nacházejícího se v experimentálně dostupném teplotním a frekvenčním intervalu 187 K – 385 K a 1 Hz – 10 MHz. Frekvence ztrátového maxima se řídí Arrheniovým zákonem s aktivační energií 0.048 eV. Ve vodivostních spektrech vykazují tenké vrstvy Ta2O5 na nízkých frekvencích ustálenou hodnotu a při vysokých frekvencích monotónní nárůst, který závisí na teplotě. Pozorovanou vodivost lze popsat mocninnou funkcí s exponentem nepatrně větším než jedna (tzv. superlineární závislost). Výsledky získané pro Nb2O5 v podobné teplotní a frekvenční oblasti, 218 K – 373 K, 1 Hz – 1 MHz rovněž ukazují jedno relaxační maximum. Frekvence ztrátového maxima se opět řídí Arrheniovým zákonem s poněkud vyšší aktivační energií 0.055 eV. Niobové kondenzátory vykazují vodivostní mechanismus shodný s kondenzátory tantalovými.
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Gel aprotic electrolytes with tetraalkylamonium salts
Michalec, Juraj ; Veselkova, Iuliia (referee) ; Sedlaříková, Marie (advisor)
The essence of this graduate thesis is to summarize knowledge about the aprotic gel electrolytes. In the graduate thesis, there are explained methods for mensuration electrochemical properties of the aprotic gel electrolytes. In the theoretical part, I focus on the knowledge related to gel polymeric electrolytes, their history, properties, mechanisms and application. In the experimental part, I describe the preparation of the samples of the gel polymeric electrolytes, in which I evaluate their properties, electrical conductivity and potencial window.
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The influence of photochromic reaction on optoelectrical properties of organic semiconductors
Heinrichová, Patricie ; Weiter, Martin (referee) ; Vala, Martin (advisor)
This diploma thesis is focused on study of electric and optoelectric properties of conjugated polymers. The theoretical part describes the relationship between molecular structure of conjugated materials and their chosen macroscopic physical properties like absorption of visible and ultraviolet radiation, electrical conductivity and photoconductivity. This part also describes photochromism and its utilization for construction of light driven current switch. The experimental part studies this switch based on change of photochromic species dipole moment dispersed in conjugated conducting polymer. The active switching unit is represented by photochromic spiropyran 1’,3’-dihydro-1’,3’,3’-trimethyl-6-nitrospiro[2H-1-benzopyran-2,2’-(2H)-indol] which is dispersed in conjugated conducting polymer poly[2-methoxy-5-(3',7'-dimethyloctyloxy)-1,4-phenylene-vinylen]. The influence of the photochromic conversion on the polymer matrix was studied by absorption spectroscopy, current-voltage measurements and spectrally resolved steady state photoconductivity and transient photoconductivity.
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Gel polymer electrolytes with fire retardands
Veselkova, Iuliia ; Jahn, Michal (referee) ; Sedlaříková, Marie (advisor)
This graduate work deals with the study and preparation of gel polymer electrolytes with flame retardants for lithium-ion batteries. The theoretical part describes the types of electrolytes, their features, benefits, how they differ and where they are used in detail. The basis of this section is gel electrolytes with flame retardants, to measure their electrical and electrochemical properties. The experimental part deals with the preparation of samples of gel electrolytes with different percentages of flame retardant, where varied species of flame retardants and measuring their electrical conductivity and potential windows. Impedance spectroscopy, cyclic voltammetry and dynamic-analytical thermal analysis were selected as measuring methods.
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