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National Repository of Grey Literature

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	3D Construction View of Differential Pumping Chamber with Detector Board of Environmental Scanning Electron Microscope Neděla, Vilém This paper deals with construction of the differential pumping chamber with a detector board for adaptation of the scanning electron microscope (SEM) to the environmental scanning electron microscope (ESEM). ESEM allows work at higher pressure in some parts of the microscope. It focuses especially on the 3D construction view of the differential pumping chamber together with the detector board of the differential pumping chamber and it comments reasons of necessity of the assembly of these parts into the environmental scanning electron microscope. Detailed record
	Signal Detection by Scintillation Detector from Organic and Inorganic Specimens in Environmental SEM Neděla, Vilém This article deals with the principle of the function and the example of practical application of a scintillation detector in Environmental scanning electron microscopy. Exploitation of this detector is demonstrated on the case of observation of organic and inorganic specimens, while it deals simultaneously with related problems. Detailed record
	Differentially Pumped Chamber in ESEM-VEGA and its Application in the Study of Water-Containing Samples Neděla, Vilém Detailed record
	Měření a nastavování vlhkosti v Environmnetálním rastrovacím elektronovém mikroskopu Autrata, Rudolf ; Jirák, Josef ; Neděla, Vilém ; Špinka, J. When we are detecting signal electrons with an ionization detector in ESEM, the most advantageous is to use, with respect to the effectiveness of ionization, environment of water vapours in the specimen chamber. The most suitable are saturated water vapours (relative humidity of 100%). This environment is also advantageous for observation of specimens containing water. At pumping of the specimen chamber to the working pressure (typically around 1000 Pa), in the case of wet specimens, evaporation of specimen can occur, or on the contrary, condensation of water on them. It means, that in some cases the specimen will not remain in the original state. That is why we try to adjust and optimize the pumping procedure and pumping of water vapors to minimize deformation of the observed specimens Detailed record

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