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Original title:
Determination of Composition and Anomeric Ratio in Mixtures of Fluorinated Ologosaccharides.
Authors: Červenková Šťastná, Lucie ; Kurfiřt, Martin ; Hamala, Vojtěch ; Karban, Jindřich
Document type: Papers
Conference/Event: Magnetic Moments in Central Europe 2019, Prague (CZ), 20190227
Year: 2019
Language: eng
Abstract: Plenthora of glycosylation reactions was performed and sophisticated NMR approach for characteriza-tion of the coressponding products was aplied. ID 19F and *H NMR were utilized for accurate derermina-tion of anomeric ratios and 2D NMR techniques as HSQC, HMBC and COSY were used to assign the signals of individual anomers. In some cases, spectrum simulation was necessary to obtain the desired parameters.
Keywords: 2D NMR techniques; deoxofluorinated oligosaccharides; glycosylation
Project no.: LM2015037 (CEP), GA17-18203S (CEP)
Funding provider: GA MŠk
Host item entry: Book of Abstracts, ISBN 978-80-86186-97-9
Rights: This work is protected under the Copyright Act No. 121/2000 Coll.
Institution: Institute of Chemical Process Fundamentals AS ČR (web)
Original record: http://hdl.handle.net/11104/0306362
Permalink: http://www.nusl.cz/ntk/nusl-409686
The record appears in these collections:
Research > Institutes ASCR > Institute of Chemical Process Fundamentals
Conference materials > Papers
Authors: Červenková Šťastná, Lucie ; Kurfiřt, Martin ; Hamala, Vojtěch ; Karban, Jindřich
Document type: Papers
Conference/Event: Magnetic Moments in Central Europe 2019, Prague (CZ), 20190227
Year: 2019
Language: eng
Abstract: Plenthora of glycosylation reactions was performed and sophisticated NMR approach for characteriza-tion of the coressponding products was aplied. ID 19F and *H NMR were utilized for accurate derermina-tion of anomeric ratios and 2D NMR techniques as HSQC, HMBC and COSY were used to assign the signals of individual anomers. In some cases, spectrum simulation was necessary to obtain the desired parameters.
Keywords: 2D NMR techniques; deoxofluorinated oligosaccharides; glycosylation
Project no.: LM2015037 (CEP), GA17-18203S (CEP)
Funding provider: GA MŠk
Host item entry: Book of Abstracts, ISBN 978-80-86186-97-9
Rights: This work is protected under the Copyright Act No. 121/2000 Coll.
Institution: Institute of Chemical Process Fundamentals AS ČR (web)
Original record: http://hdl.handle.net/11104/0306362
Permalink: http://www.nusl.cz/ntk/nusl-409686
The record appears in these collections:
Research > Institutes ASCR > Institute of Chemical Process Fundamentals
Conference materials > Papers
Record created 2020-02-12, last modified 2023-12-11
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