Národní úložiště šedé literatury Nalezeno 12 záznamů.  1 - 10další  přejít na záznam: Hledání trvalo 0.00 vteřin. 
Effect of casting conditions and heat treatment on high temperature low cycle fatigue performance of nickel superalloy Inconel 713LC
Šulák, Ivo ; Obrtlík, Karel ; Hrbáček, Karel
The present work is focused on the study of high temperature low cycle fatigue behaviour of Inconel 713LC produced by a vibratory investment casting (VIC) in as-cast conditions and in the condition after heat treatment (HT) consisting of hot isostatic pressing (HIP) followed by precipitation hardening. Low cycle fatigue tests were carried out on cylindrical specimens in symmetrical push-pull cycle under strain control with constant total strain amplitude and strain rate at 800 °C in air. Hardening/softening curves and fatigue life curves of both materials were assessed and compared with data of Inconel 713LC produced by a conventional investment casting (CIC). Cyclic hardening can be observed in the high amplitude domain while saturated stress response is apparent for low amplitude cycling for all material batches. Data presented in Basquin representation show an increase in fatigue life of both VIC batches compared to the CIC batch, however, no effect of HT on fatigue life of Inconel 713LC produced by VIC was observed. In contrast, the heat treated Inconel 713LC demonstrates slightly higher fatigue life in Coffin-Manson representation. The microstructure of both superalloys was studied by means of scanning electron microscopy (SEM). The microstructure of superalloy is characterized by dendritic grains with casting defects. It comprises the γ matrix, cubic γ´ precipitates, eutectics and carbides. The effect of the VIC and HT on fatigue performance and microstructure of Inconel 713LC is discussed.
Low cycle fatigue behaviour and fatigue crack initiation in MAR-M247 at 700 °c
Šulák, Ivo ; Obrtlík, Karel ; Hrbáček, K.
The second generation nickel-based superalloy MAR-M247 offersa satisfying combination of fatigue and creep properties and oxidation and corrosion resistance that arerequired for application at elevated temperatures in hostile environments. The microstructure consists mainly oftheface centred cubic γ matrix and ordered γ ́ strengthening precipitates (L12crystal structure). The present work focuses on low cycle fatigue (LCF) behaviour of polycrystalline nickel-based superalloy MAR-M247 at high temperature. LCF tests were conducted on cylindrical specimens in symmetrical push-pull cycle under strain control with constant total strain amplitude and strain rate at 700 °C in ambientair. Cyclic stress-strain curvesand fatigue life curves in the representation ofplastic strain amplitude vs. stress amplitude andstress amplitude vs. the number of cycles to failure, respectively,were plotted and compared with data obtained on Inconel 713LC. Special attention waspaid to the investigation of crack initiation in MAR-M247 during low cycle fatigue. Crack initiation sites were studied by means of scanning electron microscopy (SEM) in dual beam microscope TESCAN LYRA 3 XMU FESEM equipped with focus ion beam (FIB). Specimens’ surface observations revealed the formation of pronounced surface relief indicating localisation of plastic deformation.Observations in transmission electron microscope (TEM)confirmed localisation of cyclic plastic deformation in persistent slip bands along {111} slip planes. Fractographic analysis revealed fatigue crack initiation sites. Fatigue crack propagation in stage I was typical of smooth facets up to 500 μm long.
HIGH - TEMPERATURE CREEP BEHAVIOUR OF CAST COBALT-BASE SUPERALLOYS
Dvořák, Jiří ; Král, Petr ; Kvapilová, Marie ; Hrbáček, Karel ; Sklenička, Václav
Two cast and heat-treated NbC and TaC – strengthened cobalt superalloys have been developed for a precision casting of spinner discs for glass wool industry. In this work constant load creep tests in tension were carried out in argon atmosphere at three testing temperature 900, 950 and 1000 °C and at the initial applied stresses ranged from 40 to 200 MPa. All the tests were continued until the final fracture. The results of creep testing were combined with microstructural and fractographic examinations by means of light and scanning electron microscopy. A mutual comparison of creep characteristics of the investigated superalloys under comparable creep loading conditions showed that NbC-strengthened superalloy exhibited longer creep life than TaC-strengthened one. Further, it was found that carbide precipitation is the primary strengthening mechanism in both cobalt-base superalloys under investigation and the amount, morphology\nand type of carbides have the decisive effect on the creep properties including creep damage and fracture processes. By contrast, NbC-superalloy exhibited a more brittle character of creep fracture mode than TaCstrengthened superalloy. This study was initiated to investigate in more details creep deformation processes and the effect of the creep microstructure and damage evolution on both investigated superalloys. The different behaviour and properties of studied superalloys were explained based on the received results of this study.
LOW CYCLE FATIGUE BEHAVIOR AND FATIGUE CRACK INITIATION IN MAR-M247 AT 700 °C
Šulák, Ivo ; Obrtlík, Karel ; Hrbáček, K.
The second generation nickel-based superalloy MAR-M247 offers a satisfying combination of fatigue and creep properties and oxidation and corrosion resistance that are required for application at elevated temperatures in hostile environments. The microstructure consists mainly of the face centred cubic γ matrix and ordered γ´ strengthening precipitates (L12 crystal structure). The present work focuses on low cycle fatigue (LCF) behaviour of polycrystalline nickel-based superalloy MAR-M247 at high temperature. LCF tests were conducted on cylindrical specimens in a symmetrical push-pull cycle under strain control with constant total strain amplitude and strain rate at 700 °C in ambient air. Cyclic stress-strain curves and fatigue life curves in the representation of plastic strain amplitude vs. stress amplitude and stress amplitude vs. the number of cycles to failure, respectively, were plotted and compared with data obtained on Inconel 713LC. Special attention was paid to the investigation of crack initiation in MAR-M247 during low cycle fatigue. Crack initiation sites were studied by means of scanning electron microscopy (SEM) in dual beam microscope TESCAN LYRA 3 XMU FESEM equipped with focus ion beam (FIB). Specimens’ surface observations revealed the formation of pronounced surface relief indicating localisation of plastic deformation. Observations in transmission electron microscope (TEM) confirmed localisation of cyclic plastic deformation in persistent slip bands along {111} slip planes. Fractographic analysis revealed fatigue crack initiation sites. Fatigue crack propagation in stage I was typical of smooth facets up to 500 μm long.
Interaction of Creep and High Cycle Fatigue of IN 713LC Superalloy
Horník, V. ; Šmíd, Miroslav ; Hutař, Pavel ; Kunz, Ludvík ; Hrbáček, K.
The study deals with the interaction of creep and high cycle fatigue of cast polycrystalline nickel-based superalloy IN 713LC at high temperatures. Previous works indicated that creep lifetime of superalloy structures was un-affected or even slightly increased in the cases with superimposed vibrations. The reason for this behaviour was not well described up to now. Therefore, set of fatigue tests was conducted at high mean stresses level to observe this phenomenon. The mean stress was kept constant while the stress amplitudes were selected in order to measure wide range of conditions from pure creep to pure fatigue. Fractographic analysis by scanning electron microscopy (SEM) was done with the aim to identify governing damage mechanisms for particular test conditions as a preliminary evaluation of conducted tests.
EFFECT OF HIP ON LOW CYCLE FATIGUE OF MAR-M247 AT 900°C
Šulák, Ivo ; Obrtlík, Karel ; Škorík, Viktor ; Hrbáček, K.
Polycrystalline nickel-base superalloy MAR-M247 is used for high temperature applications requiring excellent combination of fatigue properties, creep resistance and surface stability. These superior high temperature characteristics derive from the microstructure which habitually consists of face centred cubic matrix γ and precipitate γ´ (L12 type ordered structure). In the present work, the high temperature low cycle fatigue behaviour of cast nickel-base superalloy MAR-M247 in as received condition and in hot isostatically pressed (HIP) condition was studied. The microstructure of the materials is characterized by dendritic grains, carbides and casting defects. Distribution and size of defects in both materials were studied. Isothermal low cycle fatigue (LCF) tests were performed on cylindrical specimens under total strain control at 900°C in air. Cyclic stress–strain response and fatigue life of both materials were assessed. Beneficial effects of HIP process on cyclic stress-strain and fatigue life curves are discussed.
Fatigue properties of nickel-base superalloy inconel 792-5A at 800°C
Šmíd, Miroslav ; Obrtlík, Karel ; Petrenec, Martin ; Polák, Jaroslav ; Hrbáček, K.
Smooth specimens were cyclically strained under strain control with constant strain amplitude and constant strain rate. Low cycle fatigue tests were conducted in servo-hydraulic pulsator MTS equipped with a three zone resistance furnace at temperature 800°C in air. Fracture surface was studied in SEM after fatigue test termination. Selected specimens were used to prepare foils for the transmission electron microscope (TEM) observation of microstructure and dislocation arrangement. They were used to obtain cyclic hardening/softening curves, cyclic stress-strain curve and fatigue life curves in the representation of stress amplitude, total strain amplitude and plastic strain amplitude versus number of cycles to fracture. Experimental points can be approximated with the Manson-Coffin law and the Basquin law. Fracture surface examinations revealed fatigue crack initiation sites.
Únavová životnost a únavový lom lité niklové superslitiny Inconel 792-5A při pokojové teplotě a při zvýšených teplotách
Šmíd, Miroslav ; Obrtlík, Karel ; Petrenec, Martin ; Polák, Jaroslav ; Hrbáček, K.
Cílem této práce je studium vlivu teploty na únavovou životnost a charakter únavového lomu lité polykrystalické superslitiny Inconel 792-5A. Pozorování povrchového reliéfu a lomových ploch pomocí SEM umožňuje objasnit mechanismy únavového poškozování v tomto materiálu užívaném na výrobu kritických částí plynových turbín. Křivky únavové životnosti byly získány pro všechny teploty. Experimentální body křivek životnosti vyhovují Mansonovu-Coffinovu a Basquinovu zákonu. Byl sledován povrchový reliéf pomocí SEM s důrazem na místa lokalizace cyklické plastické deformace. Komplexní informace o iniciaci únavových trhlin byly získány jak pozorováním povrchového reliéfu, tak lomové plochy. Bylo provedeno detailní studium morfologie lomových ploch při různých teplotách a různých amplitudách deformace a charakteristické lomové útvary. Mechanismy únavového porušování v závislosti na teplotě, amplitudě deformace a délce únavové trhliny jsou diskutovány.
Nízkocyklová únava superslitin Inconel 713LC a Inconel 792-5A při teplotách 500 A 700 °C
Petrenec, Martin ; Obrtlík, Karel ; Polák, Jaroslav ; Hrbáček, K. ; Kruml, Tomáš
Válcová zkušební tělesa litých polykrystalických niklových superslitin Inconel 713LC a Inconel 792-5A byla cyklicky zatěžována v režimu řízené deformace při teplotách 500 a 700 °C. Jsou dokumentovány strukturní charakteristiky obou materiálů včetně morfologie precipitátů gama´. Dislokační struktura ve vybraných vzorcích cyklovaných do lomu byla pozorována pomocí TEM s využitím techniky orientovaných fólií. Byly získány křivky cyklického zpevnění/změkčení, cyklické deformační křivky a křivky únavové životnosti. Průběh křivek cyklického zpevnění/změkčení závisí na teplotě a na amplitudě plastické deformace. Cyklické deformační křivky lze aproximovat mocninovou závislostí. Experimentální body křivek životnosti vyhovují Mansonovu-Coffinovu a Basquinovu zákonu. Charakteristiky cyklické napěťové odezvy a únavové životnosti stanovené při obou teplotách jsou porovnány a diskutovány v relaci ke strukturním parametrům a pozorovaným dislokačním strukturám studovaných superslitin.
Využití barevného leptání pro pozorování mikrostruktur Ni-superslitin
Konečná, R. ; Kunz, Ludvík ; Skočovský, P. ; Lukáš, Petr ; Hrbáček, K.
Bylo ukázáno, že metoda barevného leptání poskytuje cenné informace o gama/gama s čárkou mikrostruktuře Ni superslitin, o změnách mikrostruktury v průběhu exploatace materiálu a o malých defetech typu kavit a pórů.

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