Original title:
Ensolisation-silylation reaction study of selected steroids
Authors:
Hehenberger, A. ; Kotas, Petr ; Tříska, Jan Document type: Papers Conference/Event: CECE 2014, Brno (CZ), 2014-11-20 / 2014-11-22
Year:
2014
Language:
eng Abstract:
For the purposes of trace analysis of 1,4-androstadiene-3,17-dione (ADD), 1,4-androstadiene-3-one-17β-ol (Boldenone) and 17-β-estradiol in water, waste water, soil and for the further phytosterols transformation studies the enolisation-silylation reaction was studied using MSTFA and BSTFA with different catalysts as derivatization reagents. The different reaction conditions and stability of the products was also studied using GC-MS technique.
Keywords:
Enolisation-silylation; steroid hormones applications Project no.: ED1.1.00/02.0073, LH13045 (CEP) Funding provider: GA MŠk, GA MŠk Host item entry: CECE 2014. 11th International Interdisciplinary Meeting on Bioanalysis, ISBN 978-80-904959-2-0
Rights: This work is protected under the Copyright Act No. 121/2000 Coll.