|
|
Methods of Preparation and Characterization of Experimental Field-Emission Cathodes
Knápek, Alexandr ; Luňáček, Jiří (referee) ; Lazar, Josef (referee) ; Grmela, Lubomír (advisor)
Téma doktorské práce se zabývá přípravou a popisem katod na bázi autoemise, jenž představují kvalitní a levný elektronový zdroj pro zařízení pracující s fokusovaným elektronovým svazkem. Pro přípravu kompozitní autoemisní katody byla využita elektrochemická metoda výroby. Kompozitní struktura katody zlepšuje proudovou stabilitu ve srovnání s čistě autoemisními katodami na bázi wolframu. Na základě charakterizace katody, jenž byla nově provedena metodou šumové spektroskopie, byla implementována technologická zlepšení stávající výroby. Metoda šumové spektroskopie je založena na analýze emisního proudu v časové a kmitočtové rovině, ale především poskytuje informace o nosiči náboje, o jeho pohyblivosti a dále o životnosti katody. Výsledky experimentální části byly rozšířeny teoretickými simulacemi, vedoucími k návrhu metodiky charakterizace vylepšené autoemisní katody.
|
|
|
Noise, Transport and Structural Properties of High Energy Radiation Detectors Based on CdTe
Šik, Ondřej ; Lazar, Josef (referee) ; Navrátil, Vladislav (referee) ; Grmela, Lubomír (advisor)
Poptávka ze strany vesmírného výzkumu, zdravotnictví a bezpečnostního průmyslu způsobila v posledních letech zvýšený zájem o vývoj materiálů pro detekci a zobrazování vysokoenergetického záření. CdTe a jeho slitina CdZnTe. jsou polovodiče umožnují detekci záření o energiích v rozsahu 10 keV až 500 keV. Šířka zakázaného pásma u CdTe / CdZnTe je 1.46 -1.6 eV, což umožňuje produkci krystalů o vysoké rezistivitě (10^10-10^11 cm), která je dostačující pro použití CdTe / CdZnTe při pokojové teplotě. V mé práci byly zkoumány detektory CdTe/CdZnTe v různých stádiích jejich poruchovosti. Byly použity velmi kvalitní spektroskopické detektory, materiál s nižší rezistivitou a výraznou polarizací, detektory s asymetrií elektrických parametrů kontaktů a teplotně degenerované vzorky. Z výsledků analýzy nízkofrekvenčního šumu je patrný obecný závěr, že zvýšená koncentrace defektů způsobí změnu povahy původně monotónního spektra typu 1/f na spektrum s výrazným vlivem generačně-rekombinačních procesů. Další výrazná vlastnost degenerovaných detektorů a detektorů nižší kvality je nárůst spektrální hustoty šumu typu 1/f se vzrůstajícím napájecím napětí se směrnicí výrazně vyšší než 2. Strukturální a chemické analýzy poukázaly, že teplotní generace detektorů způsobuje difuzi kovu použitého při kontaktování a stopových prvků hlouběji do objemu krystalu. Část mé práce je věnována modifikaci povrchu svazkem argonových iontů a jejímu vlivu na chemické složení a morfologii povrchu.
|
|
|
Spatial Division of Optical Beams
Hampl, Martin ; Lazar, Josef (referee) ; Vlček, Čestmír (referee) ; Wilfert, Otakar (advisor)
The dissertation thesis deals with a free space optical links, especially is focused directly to the transmission optical beams. The influence of environmental conditions like atmospheric turbulence, buildings movement and vibration is described. As a possibility to reduce these undesirable influences, the generation of the transmission beam by the help of the two-mode optical fiber is proposed. A possibility to drive the shape of the resulting transmission beam by means of the change of power ration of individual modes in fiber is described. The coherence features of the proposed beam are analyzed considering the possibility to reduce the influence of atmospheric turbulence. In the thesis there are introduced beam quality parameters that enable to evaluate the quality of the optical beam for the free space optical link. These parameters give the relationship between the shape of the optical beam and the power balance of the optical link and the statistical evaluation of the optical link.
|
|
|
Low level measurement
Roubal, Zdeněk ; Lazar, Josef (referee) ; Sládek, Petr (referee) ; Steinbauer, Miloslav (advisor)
The doctoral thesis presents methods for low-level measurements, which are exemplified by the general measurement of air ion concentration. Within the first section, the author progressively identifies certain critical effects influencing the concentration of air ions, and these effects are to be considered in evaluating the uncertainty of the measured concentrations. Thus, the thesis aims to provide a systematic description of the procedures and requirements related to low-level measurements; the proposed description then involves a discussion of the process reliability requirements, namely the factors of repeatability, elimination of errors, and definition and describability of measurement uncertainties. Such methodology facilitates, among other activities, the long-term monitoring of air ion concentration in extreme environments, including caves or spaces characterized by high temperatures and humidity. The use of common methods for determining the air ion mobility spectrum is accompanied by a number of disturbing effects, such as spurious fluctuation in the concentration of air ions in time. The experimental section of the thesis describes the testing of different configurations of the measuring device (a collecting electrode and a polarization capacitor); at this stage, we seek the most advantageous distribution of the electrostatic field in the sensor – a Gerdien tube. The systematic suppression of the influence of spurious fluctuations in air ion concentration during the measurement of saturation characteristics is carried out with the least-squares numerical method (as a supporting element), a hybrid technique to describe and evaluate the experimental model. In the second part of the thesis, the methodology of low-level measurement is complemented with procedures for the measurement of freezing potential. This latter domain, as an overall experimental approach applicable during phase changes of the sample, has hitherto not been sufficiently characterized from the metrological perspective, in an up-to-date manner; several subregions of the said domain remain somewhat obscured and deserve significantly more attention. In the given context, this thesis systematically considers a problem where comparable measurement results produced by multiple authors are not available. The measuring methodology proposed herein was utilized in applied research to facilitate the fabrication of an apparatus for the experimental measurement of freezing potential in pre-defined samples; the obtained results then lead us to conclusions with respect to the evaluation of effects that cause differences in the measured data, and the results can be further compared with those obtained by other researchers investigating the given segment of the problem.
|
|
|
Polarization Imperfections of Light in Interferometry
Kučera, Petr ; Lazar, Josef (referee) ; Mohr, Fridemann (referee) ; Wilfert, Otakar (advisor)
Disertační práce pojednává o polarizačních nedokonalostech optických komponentů, které jsou využívány ke kontrole a k transformaci polarizačního stavu světla. Získané teoretické výsledky jsou pak využity ve vybraných aplikacích, jež ke své činnosti využívají právě polarizace světla. Konkrétně se jedná o zařízení měřící vibrace oscilujících objektů, dále o interferenční měření dvojlomu v transparentních materiálech a konečně, o vybraná témata z optické kvantové komunikace.
|
|
|
Local optical and electrical characteristics of optoelectronic devices
Škarvada, Pavel ; Hrabovský, Miroslav (referee) ; Lazar, Josef (referee) ; Tománek, Pavel (advisor)
Solar energy conversion, miniaturization of semiconductor devices and associated lifetime, reliability and efficiency of devices are the basic premise of this work. This work is focused on the study of optoelectronic devices especially solar cells and its nondestructive diagnostic. Solar cells are advantageous for study mainly because the pn junction is located near the surface and contains a lot of inhomogeneities. It has been difficult until recently to investigate their local physical (electrical and optical) parameters due to the size of inhomogeneities. Behavior of inhomogeneities can be well understood with knowledge of its local properties. Establishment of measurement workplace, that satisfies requirements for measurement of local emission and optically induced current measurement, allows us detection and localization of inhomogeneities with spatial resolution more or less 100 nm. The core of thesis is characterization of imperfection using nondestructive techniques in the macroscopic region but primarily in microscopic region using scanning probe microscopy. Integral parts of the work are characterization techniques for photoelectrical devices, microscopic techniques and data processing. Scanning near-field optical microscope is used for the purpose of microscopic characterization such as topography, local optical, photoelectrical and electrooptical properties of structures in high spatial resolution. Locally induced current technique, current voltage characteristics, emission from reversed bias pn junction measurement including its thermal dependence are used for samples investigation in macroscopical region. It is possible to localize defects and structure inhomogeneity using mentioned techniques. Localised defects are consequently analyzed for composition and measured using electron microscopy. Specific outputs of work are classification of photoelectric devices defects and specification of nondestructive characterization techniques used for defect detection. Experimental characterization techniques are described together with defects measurement procedures. The key output is the catalog of serious defects which was detected. Particular defects of samples are shown including describe of its properties and physical meaning.
|
|
|
Degradation of GaAs Solar Cells
Papež, Nikola ; Pinčík,, Emil (referee) ; Lazar, Josef (referee) ; Sobola, Dinara (advisor)
Solární články na bázi arsenidu gallia patří mezi nejvýkonější typ dostupných solárních článků vůbec. Jejich výhodou je výborná odolnost vůči tepelnému a ionizujícímu záření, a proto se využívají zejména v náročných podmínkách. Tato disertační práce popisuje stav GaAs fotovoltaických článku vystavených vůči tepelnému namáhání, vysokému ochlazování, gama záření a ozáření širokospektrálním laserem. Vzorky byly zkoumány před, po a i během těchto procesů pomocí několika analytických a charakterizačních metod. Měření bylo zaměřeno na charakterizaci povrchu, optických a elektrických vlastností. Byly objeveny limity a nové chování tohoto typu článků, které jsou ovlivněny i tenkými ochrannými a antireflexními vrstvami.
|
|
|
Analysis of an Electromagnetic Wave on the Boundary between Electromagnetic Materials
Kadlec, Radim ; Lazar, Josef (referee) ; Macháč, Jan (referee) ; Kroutilová, Eva (advisor)
The proposed dissertation thesis contains an analysis of conditions on the boundary between layers having varied electromagnetic properties. The research is performed using consistent theoretical derivation of analytical formulas, and the underlying problem is considered also in view of multiple boundaries including the effect of the propagation of electromagnetic waves having different instantaneous speed. The author presents a survey and formulation of the basic characteristics of methods used for electromagnetic wave propagation analysis; in this respect, special emphasis is placed on radial models. The processing of the topic involved the designing and verification (using a set of different, layered planar materials) of algorithms to analyze the electromagnetic field components. The algorithm was assembled to enable simple evaluation of all components of the electromagnetic field in relation to the speed of the wave propagation in a heterogeneous environment. The proposed algorithms are compared by means of different numerical methods for the modelling of electromagnetic waves on the boundary between materials; moreover, electromagnetic field components in common points of the model were also subject to comparison. When in conjunction with tools facilitating the analysis of material response to the source of a continuous signal, the algorithms constitute a supplementary instrument for the design of a layered material. Such design enables the realization of, for example, recoilless plane, recoilless transition between different types of environment, and filters for both optical and radio frequencies.
|
|
|
Method of Atmospheric Transmission Media Characteristics Determination in Optical Spectrum
Hudcová, Lucie ; Lazar, Josef (referee) ; Vlček, Čestmír (referee) ; Wilfert, Otakar (advisor)
This dissertation is focused on the determination of turbulent atmospheric transmission media properties. The concept of new method for turbulent attenuation designation is presented – the method of available power. This method comes from laser beam intensity profile analysis. The next point of this work is relative variance of optical intensity study. On the basis of experimental measurements relative variance of optical intensity is non-uniformly distributed in laser beam intensity profile. This non uniform distribution is subordinated to angular coefficient of intensity profile curve. Due to this information we can determine optimal laser beam shape to minimize influence of turbulent atmosphere.
|
|
|
Advanced Interferometric Methods of Coordinates Measurement
Holá, Miroslava ; Klapetek,, Petr (referee) ; Mrňa, Libor (referee) ; Lazar, Josef (advisor)
This thesis addresses particular topics in the field of the length metrology for nanometrology. Nanometrology deals with dimensional measurements of micro- and nanostructures with a high spatial resolution. It typically combines a microscope imaging with a precise coordinate measurement, usually capable of nanometre resolution using the state-of-art laser interferometry techniques. The development in this field is driven, among others, by emerging advanced nanotechnologies that demand to push further the capabilities and limits of the interferometric techniques to make the nanometre-level dimensional measurement of nanostructures possible. The principal limitations of current systems are the environmental conditions and especially the fluctuations in the refractive index of air. The theoretical part of this thesis aim at analysis of individual parts of laser interferometer. I oriented myself on the study of their advantages/disadvantages and further also the possibilities of their industrial applications. The second part of the thesis presents my work that focused on the influence of the refractive index of air (RIA) on the measurement uncertainty. I experimentally demonstrated an interferometric system with a self-cancellation RIA fluctuations: a transparent photodetector is used for the measurement of the standing wave along the axis of a passive resonator, where the resonator also serves as a reference for the laser wavelength stabilisation. Another optical arrangement, based on a setup of several Michelson interferometers, represents a combination of an interferometer and a refractometer into a single system. This setup was used to study the behaviour of the ambient airflow with respect to the optical path difference and physical separation of the interferometer’s and refractometer’s path. Based on the experimental results I proposed new arrangements for shape measuring interferometers, which combine length interferometry and a tracking refractometer for the direct compensation of RIA fluctuations with geometrically adjacent optical beams. The results indicate an improvement in RIA fluctuation induced uncertainty by a factor of 100. Third part describes the design and implementation of interferometric systems for specific applications. For the industrial environment I developed a compact interferometric displacement gauge which is designed to allow nanometre level measurement using a simplified interferometer construction. For coordinate measurement of the position of the sample up to six degrees of freedom, I realised a compact modular interferometric system, which represents a unique setup together with a stabilised laser source. To measure the position of the sample in an electron beam writer chamber, I designed and implemented a differential interferometer that works in the near infrared domain and uses a new detection method developed for this system. In the fourth part I describe the realisation of a high-speed interferometer with a differential arrangement, which allows evaluation of high-cycle fatigue in material engineering. This method of studying high-cycle fatigue should be beneficial for both the basic research and the engineering practice.
|
guest ::
RSS feed.