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Soil hydrogels based on the principle of controlled release
Macuráková, Viktória ; Smilková, Marcela (referee) ; Kratochvílová, Romana (advisor)
This bachelor thesis is focused on soil hydrogels, which operate on the principle of controlled release. The aim of the research was on the release of substances, and the practical use of hydrogels in agricultural practice. At work, we focused on the effect of humic substances and the quantities of the substances of the fertilizer NPK of hydrogel. Querying this data will use a variety of methods such as pH-metry, conductometry, spectrophotometry and chromatography and knowledge not only of the analysis but also the macromolecular chemistry. Experiment it was found that the content of sodium lignohumate does not affect the rate of release of potassium and phosphorus into the soil. Hydrogel which is located above the quantity of NPK fertilizer and a certain number of lignohumate released from its structures much larger amounts of ions such as Hydrogel without fertilizer NPK with approximately the same amount of lignohumate
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Humic substances as transport medium for plant nutrition
Vlková, Markéta ; Solná, Irena (referee) ; Klučáková, Martina (advisor)
This bachelor thesis treats about humic matters and their application in agriculture by means of hydrogels transport medium. It studies progressive releasing of substances, which could be used as more common nutrition for plants, prepared from superabsorbent polymers. Research was implemented in collaboration with industrial partners. The substances are synthetically made of sodium Lignohumate and mixture of industrial fertilizer called NPK. Released substances were characterized by using some methods. First, there were measured qualities, which didn’t specify released compounds, like swelling, conductivity, pH and absorption of hydrogels with different wavelengths. More details came with methods ICP-OES and ion chromatography. Hydrogels which contained both mixtures of matters written up, were studied in water solution for 5 weeks and every week all characterization were measured. From the results we can see that both of the mixtures decrease ability of hydrogel’s swelling, mainly NPK. Measuring of absorption showed that the most of the substances released from sodium Lignohumate were from hydrogels without NPK. By other measuring, we noticed realizing of potassium and phosphorus elements. The most of them were from hydrogels containing NPK. By measuring ion chromatography, we found chloride, phosphoric, sulfuric and nitric ions in solution.
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Problems of humic matters as precursor of trihalomethanes (THMs) in water
Jelínková, Zuzana ; Dolejš, Petr (referee) ; Doležalová Weissmannová, Helena (advisor)
The bachelor’s thesis deals with qualities of humic matters, their origins, structures and occurrence in aquatic environment. There are suitable methods for determination of humic substances and processes used for their removing from water. The thesis describes disinfection of water and related origin of trihalomethanes. The aim of the experimental part of the thesis is to coagulate model humic water on the laboratory mixing column including suggestion of optimal dose of selected coagulation agent and comparison of effectivity of floccules separation by membrane filtration and centrifugation. Effectivity of the removal of humic matters was determined by measuring water absorbance at wavelengths 245 nm in a silica cuvette with optical 1 cm trajectory and at 387 nm in a glass cuvette with optical 5 cm trajectory. For evaluation of quality suspension concentration of residual iron of coagulation agent in water was determined.
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Interactions of soil organic matter with pollutants studied by microcalorimetric techniques
Macuráková, Viktória ; Sedláček, Petr (referee) ; Smilek, Jiří (advisor)
This diploma thesis dealt with the study of interactions of soil organic matter, specifically humic acids with a pollutant, where the surfactant Septonex was used. Humic acids were isolated from two different soils in the work, namely black earth and cambium. The theoretical part describes the formation of humic acids as such, their possible interactions with substances and the characterization of surfactants. The experimental part is devoted to the characteristics of humic acids using elemental analysis, thermogravimetry and then the most important part of the thesis, namely the monitoring of interactions using isothermal titration calorimetry. The experiment showed that the sample of isolated black earth at the surfactant concentration of 0,075 moldm3 had the best interaction with the surfactant.
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Interactions of soil organic matter with pollutants studied by microcalorimetric techniques
Macuráková, Viktória ; Sedláček, Petr (referee) ; Smilek, Jiří (advisor)
This diploma thesis dealt with the study of interactions of soil organic matter, specifically humic acids with a pollutant, where the surfactant Septonex was used. Humic acids were isolated from two different soils in the work, namely black earth and cambium. The theoretical part describes the formation of humic acids as such, their possible interactions with substances and the characterization of surfactants. The experimental part is devoted to the characteristics of humic acids using elemental analysis, thermogravimetry and then the most important part of the thesis, namely the monitoring of interactions using isothermal titration calorimetry. The experiment showed that the sample of isolated black earth at the surfactant concentration of 0,075 moldm3 had the best interaction with the surfactant.
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Soil hydrogels based on the principle of controlled release
Macuráková, Viktória ; Smilková, Marcela (referee) ; Kratochvílová, Romana (advisor)
This bachelor thesis is focused on soil hydrogels, which operate on the principle of controlled release. The aim of the research was on the release of substances, and the practical use of hydrogels in agricultural practice. At work, we focused on the effect of humic substances and the quantities of the substances of the fertilizer NPK of hydrogel. Querying this data will use a variety of methods such as pH-metry, conductometry, spectrophotometry and chromatography and knowledge not only of the analysis but also the macromolecular chemistry. Experiment it was found that the content of sodium lignohumate does not affect the rate of release of potassium and phosphorus into the soil. Hydrogel which is located above the quantity of NPK fertilizer and a certain number of lignohumate released from its structures much larger amounts of ions such as Hydrogel without fertilizer NPK with approximately the same amount of lignohumate
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Humic substances as transport medium for plant nutrition
Vlková, Markéta ; Solná, Irena (referee) ; Klučáková, Martina (advisor)
This bachelor thesis treats about humic matters and their application in agriculture by means of hydrogels transport medium. It studies progressive releasing of substances, which could be used as more common nutrition for plants, prepared from superabsorbent polymers. Research was implemented in collaboration with industrial partners. The substances are synthetically made of sodium Lignohumate and mixture of industrial fertilizer called NPK. Released substances were characterized by using some methods. First, there were measured qualities, which didn’t specify released compounds, like swelling, conductivity, pH and absorption of hydrogels with different wavelengths. More details came with methods ICP-OES and ion chromatography. Hydrogels which contained both mixtures of matters written up, were studied in water solution for 5 weeks and every week all characterization were measured. From the results we can see that both of the mixtures decrease ability of hydrogel’s swelling, mainly NPK. Measuring of absorption showed that the most of the substances released from sodium Lignohumate were from hydrogels without NPK. By other measuring, we noticed realizing of potassium and phosphorus elements. The most of them were from hydrogels containing NPK. By measuring ion chromatography, we found chloride, phosphoric, sulfuric and nitric ions in solution.
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|
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Problems of humic matters as precursor of trihalomethanes (THMs) in water
Jelínková, Zuzana ; Dolejš, Petr (referee) ; Doležalová Weissmannová, Helena (advisor)
The bachelor’s thesis deals with qualities of humic matters, their origins, structures and occurrence in aquatic environment. There are suitable methods for determination of humic substances and processes used for their removing from water. The thesis describes disinfection of water and related origin of trihalomethanes. The aim of the experimental part of the thesis is to coagulate model humic water on the laboratory mixing column including suggestion of optimal dose of selected coagulation agent and comparison of effectivity of floccules separation by membrane filtration and centrifugation. Effectivity of the removal of humic matters was determined by measuring water absorbance at wavelengths 245 nm in a silica cuvette with optical 1 cm trajectory and at 387 nm in a glass cuvette with optical 5 cm trajectory. For evaluation of quality suspension concentration of residual iron of coagulation agent in water was determined.
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