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Preparation and properties of porous zinc material
Ryšťák, Jaroslav ; Fintová, Stanislava (referee) ; Doležal, Pavel (advisor)
Bachelor thesis is focused on preparation of bulk material prepared from zinc powder by cold pressing followed by sintering. Topic of the work includes characterization of prepared material depending on the choice of the compaction process conditions. Bulk material is characterized by physical-mechanical tests, structure and porosity. Thesis solving and focuses on study and control of processes during bulk material preparation and description of the processes from physically-chemical point of view of the structure creation and final material properties.
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Electrochemical etching of silicon
Vrzal, Pavel ; Voborný, Stanislav (referee) ; Šamořil, Tomáš (advisor)
The electrochemical etching is very used technique for semiconductor materials modification. Different structures which find applications in many fields (biotechnology, nanotechnology or electronics) can be prepared by this technique. The task of bachelor’s thesis was preparation of porous silicon using electrochemical etching. At first, a study dedicated to porous Si was carried out. Experimental part of this work deals with a design of etching cell which was used for preparation of porous silicon by electrochemical etching. In addition, the porous Si was prepared by metal assisted chemical etching. Subsequently, created structures were analyzed by scanning electron microscopy. Photoluminescence properties of porous silicon were studied as well.
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Advanced ceramics for tissue engineering
Vojtíšek, Jan ; Koplík, Jan (referee) ; Bartoníčková, Eva (advisor)
This bachelor´s thesis deals issues of ceramics materials suitable for tissue engineering. An artificial substitute for human tissue can be divided to several generations. This include inert, bioactive and bioresobable materials. Resorbable substitutions are prepared from materials, which could substitute host tissue, for example hydroxyapatite. HA can be prepared in different ways (dry and wet way). To better application in medicine, ceramics foams prepared by in situ foaming or replication technique are using. Experimental part of this paper deals preparing of hydroxyapatite powder and process optimization. Samples was characterized by IR and Raman spectrometry, XRD analysis and particle size was studied by SEM. Ceramics foams was prepared by in situ foaming from Al2O3, HA and composites (in ratio 50 – 50, 75 – 25, 90 – 10). Porosity was evaluated by stereomicroscope, density and level of sintering was studied by SEM microscopy.
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The study of the effect of burning process on the properties of lime
Urban, Karel ; Bureš,, Jaroslav (referee) ; Dvořák, Karel (advisor)
At the institute of technology of building materials and components at the fakulty of civil engineering in Brno was initiated research deal with study of the effect of limestone on the progress of decarbonization. This work is an introductory study into this problems. It focuses on describing the genesis and diagenesis of limestones, their crystallography, texture and requirements for burning. Further describes the extraction and treatment of limestones before burning. In very burning is focused on its mechanism and the used furnace systems. In the experimental part is focused on the analysis of samples of limestones of various world sites in terms of petrology, geological origin, chemical composition, the content of insoluble residues, density and porosity, and analysis of formed limes, burned at 900 °C in terms of density, CO2 content and crystal size.
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Latex Modified Cement Composites
Kunc, Michal ; Rovnaníková, Pavla (referee) ; Kuřitka, Ivo (referee) ; Havlica, Jaromír (advisor)
The subject of dissertation is a study of physic-mechanical properties and development of self-leveling polymer-cement composite of the ternary binder system PC-CAC-CS modified with chemical additives and polymeric substances. The dissertation systematically describes a four-step optimalization of the composite considering its key properties. Experimental part has been focused on monitoring the impact of composite components on selected final properties. Basic physico-mechanical, structural properties and its relations (compressive strength, porosity, flow abilities, setting times) have been analyzed for deeper understanding of the effects of individual composite components. Methods which quantify the existence of the newly formed hydration product – ettringite (XRD, SEM with EDS, calorimetry, dilatometry) has been chosen as additional study methods on selected combinations. A working prototype of self-leveling polymer-cement composite was successfully developed based on systematic process and using of testing procedures and measuring methods.
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Possibilities of evaluation durability of the surface layer of concrete structures
Blažek, Michal ; Žalud, Oldřich (referee) ; Vymazal, Tomáš (advisor)
The thesis is focused on possibilities of durability evaluation of surface layer of concrete structures. The durability of concrete surface layer usually determines the durability of the structure as a unit. It has to be determined in what environment the structure is situated and what influences it has to face, to set the durability of the structure. There is a several normative prescription to set the resistance of the structure. There is formulated a summary of the most widely used and known prescriptions in the theoretical part of the thesis. It is a lot of effort to estimate the durability of the concrete by estimation of permeability of the concrete surface layer recently. Thus these methods are also formulated in the summary and there are compared the individual outputs of the tests. The permeability and pore structures of the concrete surface layer are crucial parameters for the durability of concrete structure. These parameters influence the construction properties of the concrete as well, thus the thesis is focused on relationship of the pore structure and the strength in press of the concrete.
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Development of method thermoporosimetry polymer powders
Urbánková, Radka ; Salajka,, Zdeněk (referee) ; Kratochvíla, Jan (advisor)
Thermoporosimetry is a technique to determine small pore sizes based on melting and crystallization point depression. The temperature shift was measured by Differential Scanning Calorimetry (DSC). Development of thermoporosimetry was carried out on silica with a well-characterized narrow pore size distribution. Several parameters were studied, which a have a direct influence on melting and crystallization point depression (for example: a quality of the solvent, filling the pores with the solvent, time and frequency of centrifuging, superfluous solvent removal conditions, etc.). The optimum conditions for the thermoporosimetry method were developed using high porosity silica. The optimized experimental conditions found for silica were applied to polypropylene powder with much lower porosity. Several polypropylene powders were synthesized using different polymerization catalysts and their porosity determined. Polymer powder morphology and structure was characterized by standard methods. Powder porosity obtained by thermoporometry, gas sorption, and BET methods was compared.
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Friction components produced by rapid prototyping
Pečenka, Tomáš ; Škaroupka, David (referee) ; Omasta, Milan (advisor)
The main aim of this bachelor thesis is to make an overview of use of additive technology for production of friction components. The first part is concerned on review of additive methods and type of materials. In the second section are situated applications of this technology for fabrication of friction components. The main goal of last part is research in area of tribology of parts manufactured by additive technology.
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Posouzení příčin podkorodování nátěrů a rychlosti napadení při anaerobních korozních reakcích
Fučíková, Jana
The present work is focused on the corrosion protection of steel structural materials. Provides a basic overview of coating system, and in detail is focusing on organic paint coating. It places emphasis on the quality of treatment of steel surfaces in the stage prior to coating in order, to maximize the elimination of defects subsequent coating systems and prolong their life. The work is experimental verification of assessing the corrosion resistance of powder coated steel parts of agricultural machinery. Part was subjected to the daily 20 test corrosion test in salt spray chamber under defined conditions (ČSN ISO 9227). In conclusion, the paper outlines one of the uses of laboratory findings in the area of technical expertise.
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Sensitivity framework-a tool for the constitutive modelling of double-porosity materials
Mašín, David
An original approach to constitutive modelling of double-porosity materials is presented in the paper. The approach is based on the parallel in the mechanical behaviour of these materials and sensitive clays. After summary of the framework for the behaviour of natural clays (Cotecchia a Chandler, 2000) a new simple constitutive model based on the Modified Cam-Clay model, which allows for modelling of the degradation of the intergranular porosity, is proposed. Finally, its application to the double-porosity materials is discussed.
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