|
|
Nanostructured surfaces for electrochemical detection
Dzuro, Matej ; Hrdý, Radim (referee) ; Drbohlavová, Jana (advisor)
This work deals with the preparation of gold nanostructures for future usage in electrochemical sensors and biosensors, methods for their characterization and production. The emphasis is focused on the template-based electrodeposition method of gold and on study of the effect of manufacturing conditions on physical properties, mainly electrical and topological of nanostructures. Thesis is focused also on overall function and sensitivity of the gold nanostructured electrode.
|
|
|
Optimization of electrochemical sensor for detection in microvolume
Gajdoš, Libor ; Pekárek, Jan (referee) ; Prášek, Jan (advisor)
This thesis describes optimization and modification of standard thick-film electrochemical sensor to be able to be used for detection in microvolumes. In the theoretical part, the thick film technology is described. The work is then focused on the wettability of surfaces followed by introduction to electrochemistry and electro-analytical methods. In the experimental part, screen-printing of various types of thick film pastes on ceramic substrates for determination of their wettability and the following modification of the sensors with thick-film paste and with Parylene vaporization can be found, as well as the basic electrochemical measurements in microvolume using the modified sensor. Finally the results are summarized in conclusion.
|
|
|
Electrochemical Characterization of Nanostructured Surfaces Modified by Substancies with Thiol Bound
Urbánková, Kateřina ; Kynclová, Hana (referee) ; Hrdý, Radim (advisor)
This master thesis deals with nanotechnology, nanoparticles and nanostructured surfaces, electrochemical methods, especially voltammetry, cyclic voltammetry, electrochemical impedance spectroscopy and contact angle measurement. One part is focused on electrodes primarily nanostructured and modified by substancies with thiol bound. Tutorial for preparation of gold nanostructured electrods is introduced in practical section including SEM photos of electrode surface. Nanostructured and bare gold electrodes were modified by 11-mercaptoundecanoic acid, streptavidin, glycine and biotin and measured by cyclic voltammetry, electrochemical impedance spectroscopy and contact angle.
|
|
|
Carbon materials for supercapacitors
Moncoľ, Maroš ; Macalík, Michal (referee) ; Dvořák, Petr (advisor)
This project deals with various carbon electrodes in order to achieve the maximal capacitance of supercapacitors. In a theoretical part of this work, is described physical substance of supercapacitors, energy storage principles and carbon based materials. In an experimental part, is described preparation of electrodes, results and evaluation of measurement.
|
|
|
Properties study of gel polymer electrolytes for lithium-ion batteries
Zítka, Jan ; Dvořák, Petr (referee) ; Musil, Michal (advisor)
The present work deals with the research and development of gel polymer electrolytes and their applications. Thesis talks about the mechanisms that take place in gel electro-lytes. It also discusses the electroanalytical methods used in assessing the gel electro-lytes. The main focus of the work is the preparation of gel polymer electrolytes and compared their properties using methods of impedance spectroscopy, cyclic voltam-metry and methods of measurement of transference numbers. KEYWORDS
|
|
| |
|
|
Influence of carbon on possitive electrode of Ni-Cd accumulators
Janečka, Marek ; Dvořák, Petr (referee) ; Chladil, Ladislav (advisor)
Master’s thesis is deals with the effect of carbon additives on the positive electrode in the NiCd batteries. It examines whether the positive electrode material enrichment of carbon additives to achieve improved internal parameters of conductivity and better contact with the electrode materials in a discharged. Galvanostatic cycling and electro-chemical impedance spectroscopy (EIS) are used for evaluation of graphite aditives.
|
|
|
Liquid analysis sensor
Hanus, Martin ; Adámek, Martin (referee) ; Kosina, Petr (advisor)
This thesis deals with the mixing of liquids issues. The simulation of structure for mixing of liquids and evaluation of parametres which have most significant influence on mixing of liquids was made with help of COMSOL programm. In the next section of thesis the quality of electrodes used for cyclic voltammetry made on LTCC by thick layer technology was determined. In the end of this thesis the 3D structure for mixing of liquids was made. The quality of mixing was controlled by cyclic voltammetry.
|
|
| |
|
|
Composite electrode materials for lithium-ion batteries based on LiFePO4 prepared using GAC method
Vilhelm, Ondřej ; Neoral, Jiří (referee) ; Čech, Ondřej (advisor)
Presented work investigates the problem of secondary lithium-ion cells and the different available cathode materials. We have prepared samples of LiFePO4 with the addition of different kinds of carbon materials such as Super P, Vulcan and expanded graphite. We have always created the sample with and without surfactant. Developed samples were compared by measuring electrochemical methods (cyclic voltammetry, charge and discharge cycles and impedance spectroscopy). We also modeled the three-point cell for measuring electrochemical electrode materials.
|
guest ::
