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Multifunctional SNOM probes of new generation for correlative SEM/SPM measurements
Zezulka, Lukáš ; Kolíbal, Miroslav (referee) ; Spousta, Jiří (advisor)
Práce se věnuje návrhu multifunkční SNOM sondy pro korelativní SEM/SPM měření využívající dutého optického vlákna s plným jádrem. V rešerši jsou prozkoumány možné způsoby výroby SNOM hrotů na dutém optickém vlákně, využití dutých kapilár pro přívod pracovních tekutin ke vzorku a možnosti přívodu potenciálového rozdílu ke vzorku pomocí kapilár vyplněných vodivým materiálem. Dále je v práci prezentován vyvinutý způsob výroby unikátních SNOM hrotů a celý koncept je ověřen provedenými korelativními měřeními. Následně jsou diskutované problémy spojené s výrobou a měřeními.
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Tool for analysis of subject's movements in functional magnetic resonance measurements.
Šejnoha, Radim ; Lamoš, Martin (referee) ; Gajdoš, Martin (advisor)
This diploma thesis deals with an analysis of subject’s movement during measurements with funcional magnetic resonance imaging (fMRI). It focuses on methods of a movement artifacts detection and their removal in fMRI images. Thesis deals with metrics which are used for the movement rate of measured subjects evaluation. Metrics and a correction of movement are implemented into the programme in MATLAB. Comparison of subjects suffering from Parkinson’s disease with a group of healthy control was carried out. Tresholds of individual metrics were suggested and a criterion for the removal of subjects with high movement rate was determined.
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Mechanical excitation of self sensing SPM probes
Novotný, Ondřej ; Piastek, Jakub (referee) ; Pavera, Michal (advisor)
This bachelor thesis deals with the development of the SPM microscope probe holder which is designed for mechanical excitation of the probes. The first part of the thesis focuses on the description of physical theory, such as the principle of atomic force microscopy, the function of piezoceramics and the description of used quartz tunning fork based probes. The second part describes the gradual development and design of the new probe holder. Testing of the designed probe holder and comparison of mechanical and electric excitation is depicted at the end of this work. The designed probe holder was manufactured, the assembly procedure was described, and the drawings of the individual parts were created.
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Advanced SPM techniques for measuring electrical properties of materials
Kramář, Jan ; Konečný, Martin (referee) ; Pavera, Michal (advisor)
This bachelor thesis is concerned about development of local electric properties characterization technique of sample in contact mode of Atomic Force Microscopy. The research part describes the most expanded techniques of characterization of local electric properties using Scanning Probe Microscopy. For realization was chosen Scanning Spreading Resistance Microscopy. Important part of this technique is current amplifier. For that reason, operational amplifiers, circuits with them and implementation of new amplifier on microscop are described. Last chapter is dedicated to description of samples, which were used to test functionality of the amplifier and technique.
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Improvement of control and analysis techniques of a SPM model
Štefko, Marcel ; Nováček, Zdeněk (referee) ; Šulc, Dalibor (advisor)
Bakalářská práce se zabývá zdokonalováním výukového modelu mikroskopu atomárních sil (AFM). Součástí práce je rešerše stávajících analogii mezi makroskopickými jevy a fenomény spojenými s mikroskopii rastrovací sondou. Dále byla vybrána vhodná analogie, která byla následně implementována do již existujícího modelu mikroskopu atomárních sil. Do modelu byl integrován i jednodeskový počítač, který zajistí ovládání i bez nutnosti připojení externího počítače. Na závěr byly vyhodnoceny vlastnosti použité sondy a analogie mezi modelem a skutečnými mikroskopy atomárních sil.
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Correlated probe and electron microscopy for the study of modern magnetic nanomaterials
Novotný, Ondřej ; Flajšman, Lukáš (referee) ; Pavera, Michal (advisor)
High pressure on the development of new magnetic materials and their miniaturization also emphasizes the development of new analytical techniques. This diploma thesis deals with the development and demonstration of correlated magnetic force and electron microscopy, which is a promising tool for the characterization of magnetic nanomaterials. The first part of this thesis describes the fundamental physics of micromagnetism with a focus on cylindrical nanofibers. The following pages describe optic, probe, electron, and synchrotron methods for mapping the magnetic properties of materials. The next part describes magnetic domain wall motion in cylindrical nanowires performed as a part of a more extensive material study. The last part of the thesis describes the development of correlated magnetic force and electron microscopy on LiteScope device. A production of magnetic probes was designed and successfully tested. Probes were fabricated by focused electron beam-induced deposition from the Co2(CO)8 precursor. Further, the developed correlated microscopy is demonstrated on a multilayer PtCo sample, magnetic cylindrical nanofibers, NiFe vortex structures, and FeRh metamagnetic nano-islands.
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Software for patients and brain regions selection suitable for analysis of connectivity in fMRI
Slavíček, Tomáš ; Lamoš, Martin (referee) ; Jan, Jiří (advisor)
The aim of this thesis is to create an exploratory tool for functional magnetic resonance imaging data, which allows quickly and easily making a selection of persons and areas suitable for group analysis of connectivity. In the first chapters of this work is mentioned history of brain research and comparison of methods used in functional imaging. Next they are discussed the theoretical basis of fMRI methods, such as the formation of BOLD signal, acquisition parameters of MRI images and methods for designing experiments. The following chapter describes in detail the analysis of recorded data from the pre-processing to the interpretation of results. The last chapter of the first part describes problems of group analysis in SPM8 software. The second half of this work is dedicated to the description of developed program from data input to saving the results, including detailed descriptions of key features. In conclusion, there is a chapter characterizing the application of developed program on real data from clinical studies, including the results and evaluation of the usability of program. The program will mainly be used in neuroscience research.
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Visualization and export outputs from functional magnetic resonance imaging
Přibyl, Jakub ; Gajdoš, Martin (referee) ; Slavíček, Tomáš (advisor)
Thesis discusses the principles and methodology for measuring functional magnetic resonance imaging (fMRI), basically the origin and use of BOLD signal types used experiments. Further attention is paid fMRI data processing and statistical analysis. Subsequent chapters are devoted to a brief description of the most common software tools used to analyze data from fMRI. The main section was to create a program in MATLAB with a detailed graphic user interface for easy visualization and export output from analyzes of fMRI data. The second half is devoted to describing the program developer and graphic user interface, including key functionality. The final section describes the application program with real data from clinical studies of dynamic connectivity and use in an international project APGem.
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Local electrical conductivity measurements in AFM tapping mode
Dao, Radek ; Konečný, Martin (referee) ; Pavera, Michal (advisor)
This bachelor thesis is concerned about the development of a probe for local electrical conductivity measurements in tapping mode Atomic Force Microscopy. The teoretical part gives a short overview of Scanning Probe Microscopy techniques, with the focus being on Conductivity Atomic Force Microscopy. Furthermore, the measuring regime in which the probe operates is described here, as well as the basic component of the probe, the quartz tuning fork. The experimental part follows the iterative development process, and contains a chapter dedicated to making of very sharp tips. The final chapters describe the preparation of test samples, which were used to prove the functionality of the probe and the measurement of local electrical conductivity itself.
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Design of Low-Temperature Ultra High Vacuum Scanning Probe Microscopes
Pavera, Michal ; Klapetek, Petr (referee) ; Vetushka, Aliaksei (referee) ; Šikola, Tomáš (advisor)
This thesis deals with the development of scanning probe microscopes. Mechanical requirements for microscopes using measuring methods of scanning tunneling microscopy (STM) and atomic force microscopy (AFM) under enviroments of an ultrahigh vacuum (UHV) and variable temperatures are specified. Mechanical designs of two microscopes are discussed and their control electronics described. A special chapter is devoted to description of linear piezo manipulators and mechanical design of these prototypes.
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