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Mechanical Properties of Plastics
Pavlíková, Petra ; Nezbedová, Eva (referee) ; Molliková, Eva (advisor)
Diploma paper deals with fracture toughtness of pipe type HDPE. The influence of material structure on its fracture toughness at temperature 0°C and 23°C measured by PSI test was determined. Experimental results were compared with gained results of S4 test and the conclusions about usage of PSI test in screening of impact properties of polymeric materials were formulated.
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Influence of Residual Stress on Lifetime Prediction of Polymer Pipelines
Poduška, Jan ; Nezbedová, Eva (referee) ; Malíková, Lucie (referee) ; Hutař, Pavel (advisor)
The lifetime of plastic pipes for water supply and other applications is demanded to exceed at least 50 years. Such a long lifetime is difficult to prove by standard testing methods like the hydrostatic pres-sure test. However, it is possible to calculate an estimation of the lifetime, as the most frequently oc-curring mechanism of failure of plastic pipes is the creep crack propagation and subsequent failure. The method is based on describing the crack propagation by parameters of the linear-elastic fracture mechanics. An important part of this method is a finite element simulation of crack propagation in a pipe loaded by various types of loads. Residual stress, a side product of solidification after extrusion, is one of these loads. This thesis begins with an introductory part and literature review of the relevant topics – most of all the typical material properties of the pipe materials, mechanisms of failure, methods of residual stress determination suitable for plastic pipes and their results, methods of testing the materials and calculating lifetime. After the introduction, the problems to be solved are defined. The description of the residual stress state in the wall of various plastic pipes is the main topic. Both tangential (hoop) and axial residual stress in pipes of different dimensions and materials are determined using a combination of experiments and numerical simulations. Also, a simplified method of tangential residual stress is designed that can provide a sufficiently precise description of the tangential resid-ual stress state and is not difficult to carry out. A method to include the residual stress in the lifetime calculations and its influence on the lifetime is also dealt with. Apart from residual stress, the influence of soil loads in case of a buried pipe is studied. The residual stress can also influence the experimental determination of crack growth rate. If the CRB (cracked round bar) test is used to measure the crack growth rate, the crack can propagate asymmetrically due to the presence of residual stress in the specimens, which affects the results. Based on a finite element simulation of crack propagation in a CRB specimen, the severity of the influence is assessed.
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Targeted Preparation of Composite Based on PP with Inorganic Micro-, or Nanofiller with Different Adhesive Interlayer
Dombková, Julie ; Krčma, František (referee) ; Nezbedová, Eva (advisor)
The diploma thesis studies composite of PP and filler particle. As a particle filler was used commercially available CaCO3 (SOCAL 31). The submitted thesis had a goal to find new approaches and technologies of filler surface treatment in order to improve properties of composite materials. The plasma discharge behind static pressure was used for the surface treatment of the fillers. These fillers were afterwards analyzed by using of sedimentation analysis, turbidimetry, infra-red spectroscopy (FT-IR), X-ray diffraction analysis (XRD), scan electron microscopy (SEM), transmission electron microscopy and particle size distribution by laser diffraction. The composites with various volume parts of the fillers were prepared in PIB and studied by short-time tests. Furthermore, the influence of an adhesive layer on fracture mechanical properties of prepared composite was study. Regarding to experimental demand, there was not possible to realize long-term mechanical properties.
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DEFORMATION BEHAVIOR OF NANO/MICRO REINFORCED PMMA
Recman, Lukáš ; Nezbedová, Eva (referee) ; Kučera, Jaroslav (referee) ; Jančář, Josef (advisor)
Práce sleduje vliv velikosti částic na elastický modul a deformační chování za mezí kluzu. Bylo pozorováno, že jak elastická oblast, tak oblast za mezí kluzu ukazuje silnou závislost chování na velikosti částic. Cílem této práce je korelovat experimentální data a teoretické předpoklady které bylo odvozeny pro deformační chování v elastické oblasti a v oblasti za mezí kluzu pro amorfní polymery a konkrétně pro PMMA. Vše je motivováno propojit zatím oddělené oblasti kontinuální mikromechaniky a diskrétní nanomechaniky. Deformační chovaní PMMA plněného nano a mikro plnivem bylo pozorováno v elastické a plastické oblasti. Byl zkoumán vliv velikosti částic na velikost modulu a deformačního zpevnění. Mechanizmus vyztužení je interpretován s použitím teorie imobilizace řetězců, nanočástice mají silný vliv na molekulární dynamiku a kinetiku zapletenin. Mým příspěvkem k tomuto tématu je ukázat výraznou závislost na mechanizmu vyztužení v závislosti na velikosti částic. A to jak pod teplotou skelného přechodu tak nad teplotou skelného přechodu. Ačkoli pro velikost modulu byla publikována značná množství dat, která byla následně i interpretována, vliv částic na deformační zpevnění je poskrovnu. Během elastické deformace je primární struktura materiálu neměnná, jedná se o elastickou deformaci, za mezí kluzu již toto neplatí a primární struktura je zde nevratně poškozena. Bylo ukázáno, že obsah nano částic vede ke zvýšení meze kluzu a vyššímu deformačnímu zpevnění. Tento nárůst deformačního zpevnění je v korelaci s Guth-Gold rovnicí. Je předpokládáno, že nanočástice slouží jako další fyzikální zapleteniny a vedou k fyzikálně více zapletenému systému. Stejný efekt jako v elastické oblast tj. vliv velikosti částic na modul, byla pozorována i během deformačního zpevnění.
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Influence of adhesive layer on the mechanical behavior of PP+ inorganic filler composite.
Švestková, Dana ; Krčma, František (referee) ; Nezbedová, Eva (advisor)
The diploma thesis was dealt with the study of system PP and particular filler, specifically PPH and like a filler was used commercially available CaCO3 (SOCAL P3). This type of filler is declared by the producer as a filler without surface treatment. The submitted thesis had a goal to find and testing the suitable method and methodology for defined surface treatment of the filler. This is the first step for systematic study of influence the various types of adhesive layer on mechanical properties of declared composite. The plasma discharge behind static pressure was used for the surface treatment of the fillers. These fillers were afterwards analyzed by using of sedimentation analysis, infra - red spectroscopy (FT-IR) and scan electron microscopy (SEM). The composites with various volume part of the fillers were prepared in PIB and studied by short-time tests. Regarding to experimental demand there wasn't possible to realize the whole originally intended program i. e. study of influence the different types of adhesive layer, including to form the model for FEM approach. Nevertheless finding and testing the suitable method of surface treatment is completely basic for the others study. The above mentioned method was used in this application for the first time and it is possible to consider this process like an original approach.
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Influence of physical treatment of precipitated CaCO3 on the properties of PP composites
Huczala, Vít ; Ing.Vendula Balgová ,Ph.D. (referee) ; Nezbedová, Eva (advisor)
The diploma thesis deals with study of system of polypropylene and inorganic filler. As filler was used commercially available particulate filler CaCO3 termed NPCC 201. The objective of the study was a surface plasma treatment of filler in order to obtain composite based on polypropylene. Mechanical properties of this composite will show significantly greater value than basic matrix. The filler was treated in dielectric barrier plasma discharge by atmospheric pressure. The characterization of filler was performed before and after plasma treatment by x-ray photoelectron spectroscopy (XPS), electron microscope (SEM) and sedimentation analysis. The distribution of particle size was measured by laser diffraction and by dynamic light scattering. The composite materials with various weight concentration of filler were prepared in POLYMER INSTITUTE BRNO by using the twin-screw extruder and the test specimens were prepared by the injection molding technology. Their mechanical properties was studied by using of short and long-term tests. The uniaxial creep testing in tension was used for study of long-term behavior of composites.
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Analysis of mechanical properties of polymers and polymer compsites from video record of tensile test
Ščudlová, Jolana ; Nezbedová, Eva (referee) ; Žídek, Jan (advisor)
This thesis described mechanical tests with monitoring of camera. The aim of this work is to obtain additional information about material behavior during the test. The mechanical tests were monitored high-definition (HD) digital video-camera and camera with high resolution. The method was applied to the tensile test and Pennsylvania notch test (PENT test). The videorecordings were processed with the assistance image analysis method. The marks were placed on both of these specimens, mutual movement these marks were used to obtain following characteristics. It was Poisson’s ratio and true stress by tensile test. By PENT test it was rate growth crack. The investigated material was elastomeric polyurethane filled by biodegradable polyhydroxybutyrate for tensile test. Second material was polypropylene for PENT test. The camera is adding to the test gives extended information about the material and better interpretation results.
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Influence of detergents on the accelarated lifetime tests of PE pipes grades.
Štolfová, Kristýna ; Přikryl, Zdeněk (referee) ; Nezbedová, Eva (advisor)
This thesis studies the lifetime of the PE pipes materials. For determination of the lifetime one of the standard accelerated tests (Full Notch Creep test) was used. The main goal is to assess the influence of different types of detergents on lifetime. Specimen preparation and measurement procedure corresponding to the relevant ISO standard (ISO 16770: Plastics - Determination of environmental stress cracking (ESC) of Polyethylene (PE) - Full Notch Creep Test (FNCT)). Air, distilled water, Arkopal N 090 and Arkopal N 110 were used as detergents.
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