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Use of the NMR spectroscopy for structural analysis of the secondary metabolites isolated from Berberis vulgaris L.
Hordějčuková, Anežka ; Kuneš, Jiří (advisor) ; Špulák, Marcel (referee)
Charles Univeversity in Prague Faculty of Pharmacy in Hradec Králové Department of Inorganic and Organic Chenistry Candidate: Anežka Hordějčuková Supervisor: doc. PharmDr. Jiří Kuneš, CSc. Title of Thesis: The use of NMR spectroscopy for structural analysis of secondary metabolites isolated from Berberis vulgaris L. This diploma thesis deals with determination of unknown substances structure. A great many alkaloids from the plant Berberis vulgaris from the Berberidaceae family has been isolated in the Department of Pharmaceutical Botany and Ecology at the Faculty of Pharmacy in Hradec Králové. Some of them were passed to the NMR laboratory, requestig a structure determination. The aim of this thesis was to identify three unknown chemical formulas isolated from the plant Berberis vulgaris with the help of NMR analysis. The unknown compounds were determined on the basis of NMR experiments (1 H NMR, 13 C NMR, gHSQC, gHMBC, gCOSY, NOESY).
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Use of the NMR Spectroscopy for Stuctural Analysis of the Substances Isolated from Berberis vulgaris L and Narcissus poeticus cv. Pink Parasol
Hordějčuková, Anežka ; Kuneš, Jiří (advisor) ; Špulák, Marcel (referee)
Charles University in Prague Faculty od Pharmacy in Hradec Králové Department od Inorganic and Organic Chemistry Candidate: Anežka Hordějčuková Supervisor: doc. PharmDr. Jiří Kuneš, CSc. Title of Diploma Thesis: Use of the NMR Spectroscopy for Structural Analysis of the Substances Isolated from Berberis vulgaris L. and Narcissus poeticus cv. Pink Parasol This rigorous thesis deals with determination of three unknown substances structure isolated from natural sources. A great many alkaloids from the plant Berberis vulgaris from the Berberidaceae family and Narcissus poeticus from the Amarillidaceae family has been isolated in the Department of Pharmaceutical Botany and Ecology at the Faculty of Pharmacy in Hradec Králové. A lot of them were passed to the NMR laboratory, requestig a structure analysis. The aim of this thesis was to identify two unknown chemical formulas isolated from the plant Berberis vulgaris (with code B11 and HA2) and one chemical formula isolated from the plant Narcissus poeticus cv. Pink Parasol (code NP-D-4/3) with the help of NMR analysis. The unknown compounds were determined on the basis of NMR experiments (1 H NMR, 13 C NMR, gHSQC, gHMBC, gCOSY, NOESY).
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Use of the NMR Spectroscopy for Stuctural Analysis of the Substances Isolated from Berberis vulgaris L and Narcissus poeticus cv. Pink Parasol
Hordějčuková, Anežka ; Kuneš, Jiří (advisor) ; Špulák, Marcel (referee)
Charles University in Prague Faculty od Pharmacy in Hradec Králové Department od Inorganic and Organic Chemistry Candidate: Anežka Hordějčuková Supervisor: doc. PharmDr. Jiří Kuneš, CSc. Title of Diploma Thesis: Use of the NMR Spectroscopy for Structural Analysis of the Substances Isolated from Berberis vulgaris L. and Narcissus poeticus cv. Pink Parasol This rigorous thesis deals with determination of three unknown substances structure isolated from natural sources. A great many alkaloids from the plant Berberis vulgaris from the Berberidaceae family and Narcissus poeticus from the Amarillidaceae family has been isolated in the Department of Pharmaceutical Botany and Ecology at the Faculty of Pharmacy in Hradec Králové. A lot of them were passed to the NMR laboratory, requestig a structure analysis. The aim of this thesis was to identify two unknown chemical formulas isolated from the plant Berberis vulgaris (with code B11 and HA2) and one chemical formula isolated from the plant Narcissus poeticus cv. Pink Parasol (code NP-D-4/3) with the help of NMR analysis. The unknown compounds were determined on the basis of NMR experiments (1 H NMR, 13 C NMR, gHSQC, gHMBC, gCOSY, NOESY).
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Use of the NMR spectroscopy for structural analysis of the secondary metabolites isolated from Berberis vulgaris L.
Hordějčuková, Anežka ; Kuneš, Jiří (advisor) ; Špulák, Marcel (referee)
Charles Univeversity in Prague Faculty of Pharmacy in Hradec Králové Department of Inorganic and Organic Chenistry Candidate: Anežka Hordějčuková Supervisor: doc. PharmDr. Jiří Kuneš, CSc. Title of Thesis: The use of NMR spectroscopy for structural analysis of secondary metabolites isolated from Berberis vulgaris L. This diploma thesis deals with determination of unknown substances structure. A great many alkaloids from the plant Berberis vulgaris from the Berberidaceae family has been isolated in the Department of Pharmaceutical Botany and Ecology at the Faculty of Pharmacy in Hradec Králové. Some of them were passed to the NMR laboratory, requestig a structure determination. The aim of this thesis was to identify three unknown chemical formulas isolated from the plant Berberis vulgaris with the help of NMR analysis. The unknown compounds were determined on the basis of NMR experiments (1 H NMR, 13 C NMR, gHSQC, gHMBC, gCOSY, NOESY).
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