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Use of the NMR spectroscopy for structural analysis of the plant metabolites
Maříková, Jana ; Kuneš, Jiří (advisor) ; Špulák, Marcel (referee)
Charles University in Prague Faculty of Pharmacy in Hradec Králové Department of Inorganic and Organic Chemistry Candidate: Jana Maříková Supervisor: doc. PharmDr. Jiří Kuneš, CSc. Title of Thesis:Use of the NMR spectroscopy for structural analysis of the plant metabolites This diploma thesis is based on the structure determination of unknown compounds. These compounds, plant alkaloids, have been carried out of Fumaria officinalis L. (Fumariaceae) and Nerine bowdenii (Amaryllidaceae) at the Department of Pharmaceutical Botany and Ecology of the Faculty of Pharmacy in Hradec Králové. After that, some of them were passed to the NMR laboratory, requesting a structure determination. The goal of this diploma thesis was the sample identification of three unknown substances by NMR analysis. The unknown compounds were identified on the basic of the NMR experiments (1 H NMR, 13 C NMR, gHSQC, gHMBC, gCOSY, NOESY). Then the structures were compared with the data provided in the subject publications.
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