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Surface and mechanical properties of a-CSi:H and a-CSiO:H films
Plichta, Tomáš ; Shukurov, Andrey (referee) ; Klapetek, Petr (referee) ; Čech, Vladimír (advisor)
The dissertation thesis deals with the preparation and characterisation of a-CSi:H and a CSiO:H thin films prepared using the process of plasma enhanced chemical vapour deposition (PECVD). Tetravinylsilane (TVS) and its mixtures with argon and oxygen were used to deposit films on both planar substrates and fibre bundles. Main characterisation techniques were employed to study the topography of films, namely atomic force microscopy (AFM). Their mechanical properties were studied through nanoindentation; the nanoscratch test was used to assess the film adhesion to the substrate. Other analysed properties were internal stress and friction coefficient. The particular attention was paid to the work of adhesion and its determination. This knowledge was further applied to the preparation of surface treatments of glass fibres and, subsequently, polymer composites. Those were tested using the push-out test and the short beam shear test. Based on the results, the effects of deposition conditions and the relationships between the studied properties and quantities were determined.
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Numerical support for description of behavior of cement based composite during fatigue test
Holušová, Táňa ; Padevět,, Pavel (referee) ; PhD, Ladislav Řoutil, (referee) ; Seitl, Stanislav (advisor)
The presented dissertation thesis is focused on analysis of alternative test method for determination of mechanical parameters of cement based composites. A disk shaped specimen with diameter 150 mm, thickness 60 mm was analysed and its modification for use on compact tension test (CT). Such a test is hereinafter referred to as modified compact tension (shortly MCT or MDCT)). This test configuration was chosen for testing the static and fatigue properties of cement based composites precisely because of its traditional use for fatigue testing of metallic materials. Specimens with a different cross-sections can also be used for MCT, but the work is exclusively focused on circular specimen, for example because it could be easily cut from drill core taken directly from the existing structure, on which the properties are more relevant to the age of the used concrete of the controlled structure. The modified compact tension test was firstly calibrated by numerical simulations involved the tuning of the shape of the numerical model and used material models of concrete and steel. Then the laboratory testing of modified compact tension on several levels were performed. The adequacy of the numerical model was verified against the pilot laboratory testing of the MCT test. Furthermore, the comparison of the modified compact tension test and its suitability for determining of fracture mechanical parameters of cement based composites with the three point bending test, which is the standardized test configuration for these purposes was performed. Another laboratory testing was focused of determining of fracture mechanical parameters of concrete mixture classified in strength class C30/37 and the pilot study of fatigue parameters of the same strength class of the concrete mix. The work was also presented numerical simulations of the push-out test, focused on the connection of concrete and steel with epoxy adhesive.
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Numerical support for description of behavior of cement based composite during fatigue test
Holušová, Táňa ; Padevět,, Pavel (referee) ; PhD, Ladislav Řoutil, (referee) ; Seitl, Stanislav (advisor)
The presented dissertation thesis is focused on analysis of alternative test method for determination of mechanical parameters of cement based composites. A disk shaped specimen with diameter 150 mm, thickness 60 mm was analysed and its modification for use on compact tension test (CT). Such a test is hereinafter referred to as modified compact tension (shortly MCT or MDCT)). This test configuration was chosen for testing the static and fatigue properties of cement based composites precisely because of its traditional use for fatigue testing of metallic materials. Specimens with a different cross-sections can also be used for MCT, but the work is exclusively focused on circular specimen, for example because it could be easily cut from drill core taken directly from the existing structure, on which the properties are more relevant to the age of the used concrete of the controlled structure. The modified compact tension test was firstly calibrated by numerical simulations involved the tuning of the shape of the numerical model and used material models of concrete and steel. Then the laboratory testing of modified compact tension on several levels were performed. The adequacy of the numerical model was verified against the pilot laboratory testing of the MCT test. Furthermore, the comparison of the modified compact tension test and its suitability for determining of fracture mechanical parameters of cement based composites with the three point bending test, which is the standardized test configuration for these purposes was performed. Another laboratory testing was focused of determining of fracture mechanical parameters of concrete mixture classified in strength class C30/37 and the pilot study of fatigue parameters of the same strength class of the concrete mix. The work was also presented numerical simulations of the push-out test, focused on the connection of concrete and steel with epoxy adhesive.
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Surface and mechanical properties of a-CSi:H and a-CSiO:H films
Plichta, Tomáš ; Shukurov, Andrey (referee) ; Klapetek, Petr (referee) ; Čech, Vladimír (advisor)
The dissertation thesis deals with the preparation and characterisation of a-CSi:H and a CSiO:H thin films prepared using the process of plasma enhanced chemical vapour deposition (PECVD). Tetravinylsilane (TVS) and its mixtures with argon and oxygen were used to deposit films on both planar substrates and fibre bundles. Main characterisation techniques were employed to study the topography of films, namely atomic force microscopy (AFM). Their mechanical properties were studied through nanoindentation; the nanoscratch test was used to assess the film adhesion to the substrate. Other analysed properties were internal stress and friction coefficient. The particular attention was paid to the work of adhesion and its determination. This knowledge was further applied to the preparation of surface treatments of glass fibres and, subsequently, polymer composites. Those were tested using the push-out test and the short beam shear test. Based on the results, the effects of deposition conditions and the relationships between the studied properties and quantities were determined.
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Push Out Test: Numerical Study of the Influence of Concrete Part Width on Load Test
Holušová, Táňa ; Klusák, Jan ; Seitl, Stanislav
The concrete and steel are often performed by mechanical connectors, which are resistant against shear load. These connectors can be subjected to adverse effect, which is high concentration level of tension in connectors or their tendency to corrosion. By using bonded joint such as an epoxy layer gritted by granulates it is possible to avoid these negative effects. The aim of the contribution is to show the influence of the various concrete block widths on values of the maximum load. The modelling was performed by 2D software ATENA (Červenka Consulting)
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