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Sample preparation and their measurement by EDS methods
Kostelník, Tomáš ; Jaššo, Kamil (referee) ; Čudek, Pavel (advisor)
This bachelor´s thesis is focused on preparation and analysis of samples by energy dispersive spectroscopy using scanning electron microscopy. In the theoretical the main differences between environmental scanning electron microscopy and scanning electron microscopy are described. There is also a description of basic knowledge regarding energy dispersive spectroscopy. The generation and detection of signals arising from the interaction of a beam of primary electrons with a sample is also explained, with emphasis on the description, generation and distribution of these signals. The experimental part is focused on sample preparation and analysis.
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Study of the electrode materials for Li-Ion accumulators by electron microscopy
Kaplenko, Oleksii ; Čudek, Pavel (referee) ; Kazda, Tomáš (advisor)
The aim of this work is to describe the influence of temperature on the structure and chemical composition of electrode materials for Li-ion accumulators. Theoretical part of this thesis contains described terminology and general issues of batteries and their division. Every kind of battery is provided with a closer description of a specific battery type. A separate chapter is dedicated to lithium cells, mainly Li-ion batteries. Considering various composition of Li-ion batteries, the next subchapters deeply analyzes the most used cathode (with an emphasis on the LiFePO4, LiMn1/3Ni1/3Co1/3O2) and anode materials (with an emphasis on the Li4Ti5O12). The next chapters describe the used analytical methods: electron microscopy, energy dispersion spectroscopy and thermomechanical analysis. The practical part is devoted to the description of the individual experiments and the achieved results.
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Sample preparation and their measurement by EDS methods
Kostelník, Tomáš ; Jaššo, Kamil (referee) ; Čudek, Pavel (advisor)
This bachelor´s thesis is focused on preparation and analysis of samples by energy dispersive spectroscopy using scanning electron microscopy. In the theoretical the main differences between environmental scanning electron microscopy and scanning electron microscopy are described. There is also a description of basic knowledge regarding energy dispersive spectroscopy. The generation and detection of signals arising from the interaction of a beam of primary electrons with a sample is also explained, with emphasis on the description, generation and distribution of these signals. The experimental part is focused on sample preparation and analysis.
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Study Of The Electrode Materials For Li-Ion
Accumulators By Electron Microscopy
Kaplenko, Oleksii
One of the biggest problems with current Li-Ion batteries is thermal stability. Some active materials are more stable than others, but usually high-capacity materials suffer from lower thermal stability. During heating, not only the decomposition of the cathode material, but also the decomposition of other parts of the accumulator, such as anode material, binders and electrolytes, occurs. One of the important advantages of LiFePO4 over other cathode materials is its thermal and chemical stability, which improves battery safety. For this reason, high temperature effects were monitored on individual parts of the complete electrode, and the results are described in this work.
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Study of the electrode materials for Li-Ion accumulators by electron microscopy
Kaplenko, Oleksii ; Čudek, Pavel (referee) ; Kazda, Tomáš (advisor)
The aim of this work is to describe the influence of temperature on the structure and chemical composition of electrode materials for Li-ion accumulators. Theoretical part of this thesis contains described terminology and general issues of batteries and their division. Every kind of battery is provided with a closer description of a specific battery type. A separate chapter is dedicated to lithium cells, mainly Li-ion batteries. Considering various composition of Li-ion batteries, the next subchapters deeply analyzes the most used cathode (with an emphasis on the LiFePO4, LiMn1/3Ni1/3Co1/3O2) and anode materials (with an emphasis on the Li4Ti5O12). The next chapters describe the used analytical methods: electron microscopy, energy dispersion spectroscopy and thermomechanical analysis. The practical part is devoted to the description of the individual experiments and the achieved results.
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