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Application of Conductive Inks and Low Temperature Sintered Pastes in PCB Production
Kolek, Andrej ; Špinka, Jiří (referee) ; Starý, Jiří (advisor)
The present masters's thesis informs about the development and application of low-temperature sintering pastes in the manufacture and assembly of PCB components of the enclosing lead-free using nanoparticles of metals and their compounds. Lead-free brazing technology which s using in the present time, which has its drawbacks, however, and thus gaining other appropriate alternatives that seek to replace or further refined lead brazing. The introduction of the theoretical part inform about retrieval method of the type, composition and properties of low-temperature sintering pastes consisting of metal nanoparticles and their compounds. This section describes and explains the reaction mechanisms taking place during the sintering process. The end of the first chapter is dedicated to nanotechnology and production of nanoparticles and their compounds for the needs of the low-temperature sintering and possible related problems. Folowing section is devoted to examples of practitioners of the application and use of low-temperature sintering pastes and tests with which to assess the characteristics and quality of the related sintering conection. At the end of the thesis is a summary perspective and the use of low-temperature sintering technology nanoparticle past into the future. The experimental part is devoted to the application of conductive ink on the base of graphite for the production of 1V, 2V and 4V structures and their electroplated by the copper. There were created technological processes of 2V and 4V structures and test proposed methodologies resistance conductive theme to environmental influences. Filling pasta was tested in implementing 4V structure. There were made microsections various technological applications and their results were processed and evaluated.
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Thermal source with tuneable temperature gradient
Masár, Pavol ; Drexler, Petr (referee) ; Steinbauer, Miloslav (advisor)
This work deals with design of thermal source of panel shape for scientific biological application. Panel has adjustable surface temperature and thermal gradient. The first part of this work concern with design and numerical modeling of the thermal system, application of materials and arrangement of thermal and cooling devices – Peltier elements. Second part of this work is about construction of the panel and experimental measurement.
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Computation of thermal network of switchgear type UniGear and comparison with the real temperature rise test
Rybka, Michal ; Tůma, Drahomír (referee) ; Orságová, Jaroslava (advisor)
The Master’s thesis deals with thermal network computation of UniGear type switchgear and it compares the calculated results with the real temperature rise test. The thesis describes both electrical and non-electrical characteristics of such a switchgear as well as its application in variol fields of industry. Description of switchgear auxiliary equipment is obvious part of the thesis. Modelling of current carrying track in software environment of Autodesk Inventor and preparing of this current carrying track for thermal network calculation in software environment of ANSYS follows. Main part of this thesis is presentation of thermal analysis results and their comparison with the real temperature rise test.
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Thermal conductive plate with controlled thermal field
Masár, Pavol ; Král, Bohumil (referee) ; Steinbauer, Miloslav (advisor)
This work deals with design of thermal source of panel shape for scientific biological application. Panel has adjustable surface temperature and thermal gradient. The first part of this work concern with design and numerical modeling of the thermal system, application of materials and arrangement of thermal and cooling devices – Peltier elements. Second part of this work is about construction of the panel and experimental measurement.
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Utilization of ANSYS Workbench program at power electrical engineering
Partl, Tomáš ; Aubrecht, Vladimír (referee) ; Kuchyňková, Hana (advisor)
In its first part this Master´s thesis describes creation of electronic database design in Raster Design 2009 program as an effective form of storage only for paper documentation. The second part of my thesis provides calculation of primary and secondary winding of current instrument transformer of over-current conduit through the winding and influence on other parts of transformer i.e. error of transformer or increasing magnetic induction core and others. The last third part is focusing on usage of ANSYS Workbench in power electrical engineering. The thesis shows specific example of warming of current instrument transformer (thermal analysis) and comparing the results with theoretical (calculated) values.
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Stability of complexes of humic acids with heavy metals
Nováčková, Kristýna ; Šmejkalová, Daniela (referee) ; Klučáková, Martina (advisor)
Tato diplomová práce je zaměřena na porovnání termo-oxidační a chemické stability kovových komplexů huminových kyselin. Pro tyto experimenty byly vybrány tři prvky reprezentující skupinu těžkých kovů (kobalt, měď a nikl). Použitá huminová kyselina byla extrahována z Jihomoravského lignitu. Pro přípravu komplexů byly využito různě koncentrovaných roztoků kovů, aby bylo možné pozorovat vliv jejich počáteční koncentrace na obě studované stability připravených komplexů. Chemická stabilita kovových komplexů byla posuzována z hlediska uvolňování kovových iontů ze struktury huminové kyseliny do dvou různých extrakčních činidel (HCl, MgCl2). Termo-oxidační chování bylo zkoumáno pomocí technik termické analýzy: diferenční kompenzační kalorimetrie (DSC) a zejména termogravimetrické analýzy (TGA). Výsledky této práce přinášejí hlubší poznatky o problematice interakce kovů s humifikovanou částí půdní organické hmoty, využitelné k osvětlení problematiky kovových polutantů v životním prostředí a prohloubení žádoucích znalostí procedur jako jsou dekontaminace půdy a remediace.
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Ageing of cotton fabric as determined from polymerization degree change
Flimelová, Miroslava ; Nasadil, Petr (referee) ; Kučerík, Jiří (advisor)
The degree of polymerization (DP) is the main factor which plays a role in cellulose aging. The adverse consequence of cellulose fibers aging is the deterioration of mechanical and optical properties. Viscometry is a technique which is frequently used for determination of degree of polymerization of cellulose fibers. The aim of the work was to determine the degree of polymerization of cotton fabrics and to investigate the dependence of DP on number of washing and dying. Next task was to investigate if there exists a corellation between DP and results from thermal and thermo-oxidative degradation studied by methods of thermal analysis. First, the traditional viscometry was employed to determine DP of cellulose fibers. It has been demonstrated that number of washing and dying decreases the DP. In the second part the differential scanning calorimetry (DSC) and thermogravimetry (TG) were used. DSC provided values of combustion heat and TG allowed the detail evaluation of degradation steps; obtained results were further used for correlation with DP. Methods of thermal analysis revealed differences between cotton wool and treated fabrics. Combustion heat did not show any correlation with DP. In contrast, results from TG suggested some promising correlations which could be used for the prediction of cotton fabrics DP using thermal analysis in the future.
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