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Preparation of nanoforms of layered piezoelectric of systems BI2O3-TA(2)O(5)-AO (A=CA,SR,BA)
Štarman, S. ; Matz, V. ; Kváča, Z. ; Mohyla, M. ; Olšák, V. ; Plocek, Jiří ; Vaněk, Přemysl ; Tylš, B.
Based on the known Aurivillius phases types ABi2Ta2O9 and A2BiTaO6 ( A=Ca, Sr, Ba) were supplemented with new compositions of layered tantalates, which resulted the possibility of the existence of a new phase Sr2BiTaO6. Ternary compounds with piezoelectric structure were prepared as nanoforms by solgel reactions of homogeneous acetate Bi, Ta, A and subsequent annealing in a controlled atmosphere. Annealing temperature was determined from DSC curves based on the weight loss and phase transitions. Composition and structure of nanocrystals has been analyzed by X-ray diffraction (XRD), scanning nanomorphology (SEM) and acoustic measurements.
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