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Design of aparature for RF plasma etching
Bárdy, Stanislav ; Bábor, Petr (referee) ; Mach, Jindřich (advisor)
This bachelor's thesis deals with a design of an ICP (Inductively Coupled Plasma) apparatus. The theoretical part consists of a research of a plasmatic graphene surface cleaning. Next are described plasma generation methods and an RF circuit design. The experimental part deals with a construction of the ICP apparatus and the impedance matching box, an optical diagnostics of a plasma discharge and a measurement of PMMA etching parameters (etch rate, roughness) by a spectroscopic reflectometry and an atomic force microscopy.
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The preparation of Grafen by method CVD
Procházka, Pavel ; Kromka,, Alexander (referee) ; Mach, Jindřich (advisor)
This diploma thesis is mainly focused on the fabrication of graphene layers on the copper foil by the Chemical Vapor Deposition (CVD). For this purpose the high-temperature chamber for the production of the graphene was completed and fully automated. The production of the high area graphene on the copper foil was experimentally achieved. The Raman microscopy and X-ray photoelectron spectroscopy measurements proved that the produced graphene is mostly a monolayer. Graphene layer was transferred on non-conductive substrate.
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Selective growth of GaN layers on substrate modificated by method FIB
Mareš, Petr ; Voborný, Stanislav (referee) ; Mach, Jindřich (advisor)
The thesis deals with the selective growth of GaN crystals on the SiO2 layer. The theoretical part discusses the type of growth of ultrathin layers with focus on gallium nitride and its manufacturing. Moreover the text deals with principles of the focused ion beam and basic principles of other further methods which were used for analyzing the samples (AFM, XPS, photoluminescence spectroscopy). Experimental part consists of depositions of GaN. The silicon wafer Si(111) with native oxide SiO2 (1-2 nm) was used as a substrate. Focused ion beam was utilized to manufacture suitable structures on the substrate. Selective growth was acomplished with the use of the postnitridation method. Method of the pulse deposition was introduced with focus on increasing the volume of crystals.
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The hydrogen modification of the graphene structures for field effect transistors
Kurfürstová, Markéta ; Čermák,, Jan (referee) ; Mach, Jindřich (advisor)
This master’s thesis is focused on the subject of graphene modified with atomic hydrogen and its electronic transport properties. Structural and electronic properties of graphene and hydrogenated graphene are compared in the theoretical part of the thesis. The Raman spectroscopy technique is described, including characterization of typical Raman spectra of both unmodified and modified graphene. Samples used during experimental part of the thesis are prepared via laser and electron lithography, and are set to be measured in a vacuum chamber. Subsequently, electronic transport properties are measured before and after hydrogen modification of graphene. Finally, hydrogenated graphene is irradiated using electron beam and changes in its structure are analyzed with Raman spectroscopy techniques.
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Deposition of Ga and GaN ultrathin layers on graphene substrate
Dvořák, Martin ; Nebojsa, Alois (referee) ; Mach, Jindřich (advisor)
This diploma thesis deals with preparation of graphene samples for depositions of ultrathin layers of gallium and gallium nitride. Graphene substrates were prepared by chemical vapour deposition in home-build high temperature reactor. After graphene transfer to silicon wafers, a series of chemical and thermal treatments were performed. Obtained samples were suitable for the study of growth of ultrathin layers of Ga and GaN. The growth of Ga and GaN was realized in ultra high vacuum conditions. Molecular beam epitaxy technique was used for gallium depositions together with ion source for nitridation. Obtained ultrathin layers were studied with X-ray photoelectron spectroscopy, atomic force microscopy and with scanning electron microscopy.
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Design and Construction of an Effusion Cell for Growth of Ultrathin Layers
Křápek, Ondřej ; Voborný, Stanislav (referee) ; Mach, Jindřich (advisor)
This Bachelor's work deals with the design, documentation and construction of effusion cell for deposition of ultrathin layers of various materials in conditions of ultrahigh vacuum. After fabrication and assemblage the effusion cell was placed to an ultrahigh vacuum chamber (p ~ 10-5 Pa) where the first testing deposition of a silver ultrathin film on Si (111) substrate was performed. This sample was studied by X-ray photoelectron spectroscopy and atomic force microscopy.
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Sequential growth of GaN nanocrystals on SiO2 substrate modified by FIB method
Flajšmanová, Jana ; Voborný, Stanislav (referee) ; Mach, Jindřich (advisor)
This bachelor's thesis deals with the selective growth of gallium (Ga) and gallium nitride (GaN). In theoretical part, there is a brief description of growth of ultrathin films with respect to GaN and their manufacturing. Experimental part is aimed to the deposition of Ga and GaN on silicon substrates Si(1 1 1). Substrates with the native silicon dioxide layer (SiO2) were modified by focused ion beam (FIB). GaN was deposited by pulsed deposition followed by postnitridation. Prepared samples were studied by atomic force microscope (AFM), X-ray photoelectron spectroscopy (XPS) and scanning electron microscope (SEM).
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Growth ultrathin of layers Au
Beránek, Jiří ; Kolíbal, Miroslav (referee) ; Mach, Jindřich (advisor)
The aim of this thesis is to study growth of ultrathin gold layers prepared by MBE (Molecular beam epitaxy) in UHV conditions. Differently modified sillicon served as a substrate and depositions were done at different temperatures of a substrate. Samples were analyzed by ToF LEIS for thickness, morfology was examined by SEM and AFM. X-ray photoelectron spectra were taken for chemical analysis. Gathered data together with their evaluation contribute to description and understanding of some processes during deposition and subsequent exposure of the sample to high temperatures. Experimental data and conslusions also prowide basis for further experiments and development of potential applications.
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