| |
|
Supercritical Fluid Extraction of Sesquiterpene Lactones from Laserpitium archangelica.
Sajfrtová, Marie ; Kraus, V. ; Wimmer, Z. ; Cerhová, Marie ; Vlk, M.
The aim of the work was to describe the SFE of two STLs, archangelolide and trilobolide, from seeds of Laserpitium archangelica (Apiaceae). The objectives consisted in: (a) optimizing, investigating the SFE condition (pressure, temperature and concentration ofmodifier in scCO2) effect on the yield and concentration of STLs in extract, (b) \nDetermination of the SFE kinetics of major components in the extracts and (c) comparing the SFE with pressurised liquid extraction (PLE) and Soxhlet extraction.\n\n\n
Fulltext: content.csg - PDF Plný tet: SKMBT_C22018100509461 - PDF
|
| |
| |
| |
| |
| |
| |
| |
|
Hydrodesulfurization NiMo Catalysts over Mechanochemically Prepared Gamma-Alumina.
Kaluža, Luděk ; Jirátová, Květa ; Tyuliev, G. ; Palcheva, R. ; Koštejn, Martin ; Spojakina, A.
The aim of the present work is to explore optimum preparation route of NiMo catalysts for the novel mechanochemically prepared Al2O3 in order to achieve high HDS activity. Specifically, the goals are: i) to up-scale the support synthesis to provide sufficient amount ofAl2O3, ii) to deposit NiMo from solutions of highly soluble precursors by conventional impregnation techniques (I), i.e. sequential impregnation using Mo (first) and Ni (second), and by co-impregnation (Ni+Mo together), i.e. using chelating agent NTA or nickel heteropolyoxomolybdate (HPO), iii) to deposit NiMo from solutions ofslightly soluble precursors by slurry impregnation (SI).\n
Fulltext: content.csg - PDF Plný tet: SKMBT_C22018100509420 - PDF
|