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Impact of soil samples treatment and used measurement methods on heavy metals concentrations.
Kejík, Marek ; Marko, Michal (referee) ; Hajzler, Jan (advisor)
This bachelor thesis aims to explore the possibilities of treatment of soil samples and compare the suitability of selected analytical methods of analysis for determining the concentration of heavy metals. 7 reference certified materials of various soil types and one soil sample from the recreational area located in Brno were selected. Each soil sample was subjected to three different treatments. It is a method of melting into a solution, decomposition in aqua regia and aqueous extract. All thus treated samples were subsequently subjected to analytical methods for determining the concentration, specifically the ICP-OES and GF-AAS methods were used. To assess the suitability of selected methods of treatment of soil samples and analytical methods of determination, the 4 most risky elements were selected, namely arsenic, cadmium, copper and lead. The measured concentrations were compared with reference values of soil samples. Finally, the suitability of combinations of different sample preparation procedures and selected methods of analytical determination of the content of determined elements from soil samples was assessed.
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The optimization of quarried limestone analysis and usage.
Sidelnicov, Vitalii ; Bednárek, Jan (referee) ; Šiler, Pavel (advisor)
Limestones are rocks formed predominantly from the mineral calcite. The Czech Republic is quite rich in this type of rock. Limestone may have a very diverse composition, properties and uses. For this reason, it is beneficial to study and analyze this material, to better utilize it to its full potential. This bachelor thesis deals with the possible uses of limestone from Lesní lom in Líšna in the city of Brno, which consists of two limestones - Hádsko-Ričský and Vilemovický. Limestone analyses were performed using by the following analytical methods: XRF, XRD and ICP-OES. Furthermore, the thesis deals with the preparation of samples for individual analytical methods and the differences of the results obtained by individual methods. Part of the thesis is also an overview of the possible uses of analysed limestones.
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Impact of soil samples treatment and used measurement methods on heavy metals concentrations.
Kejík, Marek ; Marko, Michal (referee) ; Hajzler, Jan (advisor)
This bachelor thesis aims to explore the possibilities of treatment of soil samples and compare the suitability of selected analytical methods of analysis for determining the concentration of heavy metals. 7 reference certified materials of various soil types and one soil sample from the recreational area located in Brno were selected. Each soil sample was subjected to three different treatments. It is a method of melting into a solution, decomposition in aqua regia and aqueous extract. All thus treated samples were subsequently subjected to analytical methods for determining the concentration, specifically the ICP-OES and GF-AAS methods were used. To assess the suitability of selected methods of treatment of soil samples and analytical methods of determination, the 4 most risky elements were selected, namely arsenic, cadmium, copper and lead. The measured concentrations were compared with reference values of soil samples. Finally, the suitability of combinations of different sample preparation procedures and selected methods of analytical determination of the content of determined elements from soil samples was assessed.
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The optimization of quarried limestone analysis and usage.
Sidelnicov, Vitalii ; Bednárek, Jan (referee) ; Šiler, Pavel (advisor)
Limestones are rocks formed predominantly from the mineral calcite. The Czech Republic is quite rich in this type of rock. Limestone may have a very diverse composition, properties and uses. For this reason, it is beneficial to study and analyze this material, to better utilize it to its full potential. This bachelor thesis deals with the possible uses of limestone from Lesní lom in Líšna in the city of Brno, which consists of two limestones - Hádsko-Ričský and Vilemovický. Limestone analyses were performed using by the following analytical methods: XRF, XRD and ICP-OES. Furthermore, the thesis deals with the preparation of samples for individual analytical methods and the differences of the results obtained by individual methods. Part of the thesis is also an overview of the possible uses of analysed limestones.
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