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National Repository of Grey Literature 1 records found  Search took 0.00 seconds. 
Spectroelectrochemical cell with CD-trode
 Hladík, Martin ; Nesměrák, Karel (advisor) ; Rychlovský, Petr (referee)
This bachelor thesis was aimed on the optimisation of preparation of gold electrodes (CDtrodes) from commercially available DVDs by treatment of concentrated nitric acid. The duration of the treatment was set on 20 minutes, based on study of voltammetric responses of fabricated CDtrodes. The CDtrodes were employed in spectroelectrochemical cells in two arrangements (i) with beam perpendicular to the area of electrode, and (ii) with beam collinear to the area of electrode. The formation and extinction of phenothiazine radicals during cyclic voltammetry were followed spectrophotometrically. Key words: spectroelectrochemistry, CDtrode, phenothiazine
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