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National Repository of Grey Literature 2 records found  Search took 0.00 seconds. 
Kinetic determination of nitrites with spectrophotometric detection
 Vašíčková, Pavla ; Nesměrák, Karel (advisor) ; Rychlovský, Petr (referee)
Title: Kinetic determination of nitrites with spectrophotometric detection Annotation: The proposal and optimization of the kinetic determination of nitrites in water samples is the aim of this bachelor thesis. The method is based on the ability of nitrites to catalyze the oxidation of toluidine blue by bromate in acidic media. The course of the reaction is monitored by spectrophotometrically, using a decrease of the absorbance band at 653 nm in the constant period of time from the beginning of the reaction. The dual-chanel manifolds FIA apparatus was proposed and optimized. The calibration dependency in the range of 0,05-1,00 mg ml-1 was measured. The instrumental limit of detection of 0,038 mg ml-1 and limit of quantification of 0,125 mg ml-1 were calculated. The method was applied on real sample of river water. Key words: nitrites, flow-injection analysis, kinetic catalytic methods
Detailed record
Kinetic determination of nitrites with spectrophotometric detection
 Vašíčková, Pavla ; Nesměrák, Karel (advisor) ; Rychlovský, Petr (referee)
Title: Kinetic determination of nitrites with spectrophotometric detection Annotation: The proposal and optimization of the kinetic determination of nitrites in water samples is the aim of this bachelor thesis. The method is based on the ability of nitrites to catalyze the oxidation of toluidine blue by bromate in acidic media. The course of the reaction is monitored by spectrophotometrically, using a decrease of the absorbance band at 653 nm in the constant period of time from the beginning of the reaction. The dual-chanel manifolds FIA apparatus was proposed and optimized. The calibration dependency in the range of 0,05-1,00 mg ml-1 was measured. The instrumental limit of detection of 0,038 mg ml-1 and limit of quantification of 0,125 mg ml-1 were calculated. The method was applied on real sample of river water. Key words: nitrites, flow-injection analysis, kinetic catalytic methods
Detailed record

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