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Optimization of thermal dissociation atomic hydrogen source for use SEM
Melichárek, Václav ; Polčák, Josef (referee) ; Mach, Jindřich (advisor)
The focus of this bachelor's thesis is the optimization of a thermal dissociation monoatomic hydrogen source. The project entailed the design and construction of a new control electronics for the thermal dissociation source, because the source has been powered using universal laboratory power supplies until now. The thesis begins with a brief introduction into the interaction of graphene with monoatomic hydrogen, the operational principle and construction of the monoatomic hydrogen source. Furthermore, the requirements on the design of the electronics are specified. A more detailed analysis of possible solutions, and the selection of the optimal solution were also conducted. The practical part discusses the conceptual designs in detail and describes the selection of the optimal solution. It follows by elaborating on the implementation of the control electronics in detail, its design and construction, and the electrical circuit in particular.
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Design of manipulator for TEM
Melichárek, Václav ; Doležel, Pavel (referee) ; Mach, Jindřich (advisor)
The topic of this master’s thesis is the design of a sample manipulator for TEM. Regarding which the segment of the sample manipulator used to move the sample in the direction of the x-axis (so-called x-stage) was designed. The introductory theoretical part is concerned with a brief description of transmission electron microscopy focused on the imaging methods used in TEM and the procedures of preparing and loading TEM samples. The theoretical part follows with the design of precise mechanisms, especially with respect to the inaccuracies of their operation and the technological aspect of the design. In the practical part, a detailed analysis of the design of the x-stage is presented. Kinematics and dynamics of the mechanism is analyzed in depth, following with the description of the overall design of the mechanism and some of its parts in detail.
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Design of manipulator for TEM
Melichárek, Václav ; Doležel, Pavel (referee) ; Mach, Jindřich (advisor)
The topic of this master’s thesis is the design of a sample manipulator for TEM. Regarding which the segment of the sample manipulator used to move the sample in the direction of the x-axis (so-called x-stage) was designed. The introductory theoretical part is concerned with a brief description of transmission electron microscopy focused on the imaging methods used in TEM and the procedures of preparing and loading TEM samples. The theoretical part follows with the design of precise mechanisms, especially with respect to the inaccuracies of their operation and the technological aspect of the design. In the practical part, a detailed analysis of the design of the x-stage is presented. Kinematics and dynamics of the mechanism is analyzed in depth, following with the description of the overall design of the mechanism and some of its parts in detail.
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Optimization of thermal dissociation atomic hydrogen source for use SEM
Melichárek, Václav ; Polčák, Josef (referee) ; Mach, Jindřich (advisor)
The focus of this bachelor's thesis is the optimization of a thermal dissociation monoatomic hydrogen source. The project entailed the design and construction of a new control electronics for the thermal dissociation source, because the source has been powered using universal laboratory power supplies until now. The thesis begins with a brief introduction into the interaction of graphene with monoatomic hydrogen, the operational principle and construction of the monoatomic hydrogen source. Furthermore, the requirements on the design of the electronics are specified. A more detailed analysis of possible solutions, and the selection of the optimal solution were also conducted. The practical part discusses the conceptual designs in detail and describes the selection of the optimal solution. It follows by elaborating on the implementation of the control electronics in detail, its design and construction, and the electrical circuit in particular.
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