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Modification of HVOF and cold spray deposited coatings via electron beam technology
Vacek, Petr ; Šiška, Filip (referee) ; Čížek, Jan (advisor)
The aim of this thesis was to modify microstructure and coating-substrate interface of CoNiCrAlY coatings deposited by HVOF and cold spray on Inconel 718 substrates. Electron beam remelting and annealing in a protective atmosphere were used to modify the coatings. Microstructure, chemical and phase composition were analyzed. The effect of beam current, transversal velocity and beam defocus on remelted depth was evaluated. As-sprayed microstructure and chemical composition of coatings were analyzed and compared with remelted samples. The effect of annealing of the as-sprayed and remelted samples was evaluated. Remelted layers exhibited dendritic structure. Chemical composition changed only after remelting of interface and part of a substrate. When only the coating was remelted, chemical composition remained the same. Phases coarsened after the annealing. Chemical composition changed after annealing due to the diffusion.
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Reaction synthesis of bulk intermetallic materials from cold spray deposits from binary powders containing iron
Dyčková, Lucie ; Krajňáková, Petra (referee) ; Jan, Vít (advisor)
This thesis deals with reaction synthesis of materials Fe–Al, Fe–Cu and Fe–Ni from cold spray. In literature analysis are introduced these systems and for each system there is brief description of binary equilibrium diagram. Furthermore here are some short explanations of diffusion, Kirkendall effect and other possible processing technologies of intermetallic materials. In experimental part, samples of sprayed materials were annealed and then microstructural changes were investigated. This thesis contains photographs of microstructure, results from scanning electron microscopy, X-ray, and measurements of microhardness.
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Determination of properties of as-sprayed and EB-deposited coatings prepared by thermal spray technologies using scratch test and nano-indentation methods
Cének, Lukáš ; Tkachenko, Serhii (referee) ; Čížek, Jan (advisor)
Properties of samples and their coatings may be affected by the electron beam. This paper deals with the analysis of the microstructure, phase and chemical composition and the determination of mechanical characteristics of inconel steel substrate and CoNiCrAlY coatings deposited via different types of thermal spraying (HVOF, cold spray), in combination with modifications by the electron beam technology. During the study it was found that the deposition did not change the chemical composition. Further it was found that the interaction of the electron beam with the material did not change the chemical composition, but there is a change in the structure and a reduction of porosity and surface roughness, resulting in a change of mechanical properties such as decreasing hardness or increase of the modulus of elasticity.
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Fatigue Properties of Materials with Protective Thermally Deposited Layers
Matějková, Michaela ; Kovářík,, Ondřej (referee) ; Čížek, Jan (advisor)
Titanium powder was deposited into low-carbon steel specimens using three thermal spray technologies: plasma spray, cold spray (USA, Singapore) and warm spray (denoted as PS, CSU, CS-S, and WS, respectively, in further text). The aim was to determine the influence of the coatings on the fatigue lives of the specimens. The experimental work was carried out in a symmetrical cantilever-beam bending setup using a computer-controlled SF-Test loading device. Further to that, the micro-morphology of coatings structure, their respective porosity content and the fracture surfaces of both coatings and substrate materials was carried out.
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Properties of Metallic Materials Prepared by Cold Spray Technology
Piňos, Jakub ; Šiška,, Filip (referee) ; Čížek, Jan (advisor)
Cold spray is a novel coating method. Due to its low-temperature character, it has a potential to replace the high-temperature thermal spray processes in some applications. The presented work analyzes the microstructure and the phase composition of pure metal coatings deposited by cold spraying and evaluates selected mechanical properties. Specimens prepared by readily used HVOF industrial technology were used for comparison purposes.
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Reaction synthesis of bulk intermetallic materials in Ti Ni system form kinetic spraying deposits
Dyčka, Martin ; Moravčík, Igor (referee) ; Jan, Vít (advisor)
Bachelor’s thesis deals with intermetallic compounds which are formed in nickel-titanium binary system. The theoretical part of this thesis deals with the best known titanium based intermetallics, diffusion and possible processing technologies of intermetallic materials. In experimental part, a nickel-titanium coating created by cold spray technique was used. The changes in microstructure depending on annealing temperature were analysed. The results contain photographs of microstructure and fractures, values of microhardness and results of chemical analyses.
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Reaction synthesis of bulk Fe-Al intermetallic materials
Dyčková, Lucie ; Hutařová, Simona (referee) ; Jan, Vít (advisor)
Bachelor’s thesis deals with iron aluminides. In literature analysis are the best known and the most widely used intermetallics materials, diffusion and other possible processing technologies of intermetallic materials. In experimental part was used sprayed coating. This sprayed coating was produced by cold gas-dynamic spray. In this thesis were analysed changes in microstructure of iron aluminides depending on annealing temperature. This thesis contains photographs of microstructure and analyses from electron microscopy and measurement of microhardness.
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