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The magnetocrystalline anizotropy in the TbTX compounds
Klicpera, Milan
Title: The magnetocrystalline anizotropy in the TbTX compounds Author: Milan Klicpera Department: Department of Condensed Matter Physics Supervisor: doc. Mgr. Pavel Javorský, Dr. Supervisor's e-mail address: javor@mag.mff.cuni.cz Abstract: The subject of this work is the study of structural, magnetic and trans- port properties of the TbNi(Al,In) series to finding connections between magne- tocrystalline anisotropy and lattice parameters of the structure of the TbTX com- pounds. Polycrystalline TbNiAl1−xInx samples were prepared by melting. The phase and crystal structure analysis were provided on samples. We performed the measurements of the magnetization, susceptibility, specific heat, resistivity, low temperature X-ray diffraction and powder neutron diffraction. From the neutron diffraction data we refined lattice parameters and propagation vectors of the series. The main propagation is (000) and second weaker component has the propagation vector (1 2 0 1 2 ). The change of the magnetocrystalline anisotropy from uniaxial to planar type occurs for compounds with x between 0.4 and 0.5. Keywords: magnetization, X-ray and neutron diffraction, electrical resistivity.
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Measurement of tissue impedance during electroporation
Uher, Jakub ; Novotná, Veronika (referee) ; Červinka, Dalibor (advisor)
The Bachelor's thesis is devoted to the impedance of tissue in relation to the modern medical method electroporation. The Bachelor's thesis is divided into five chapters. The first three chapters describe the behaviour of the tissue and its impedance, whether during the passage of an electrical current or a phenomenon before and after the electroporation procedure. The fourth and fifth chapters examine those phenomena in the previous chapters on measurements made on animal and plant tissue.
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Microstructures fabrication for transport properties measurements of heavy fermion compounds
Volný, Jiří ; Uhlířová, Klára (advisor) ; Prchal, Jiří (referee)
In this thesis, we focus on preparation of micro-devices for resistivity measure- ment of CeCoIn5 using focused ion beam technique. Single crystal samples of ∼ 50 µm length were carved out by focused ion beam and transported on silicon sub- strates with prepared gold structures for electrical resistivity measurement. The samples were conductivily attached to gold contact pads by focused ion beam in- duced platinum deposition. Several steps and techniques were optimized: electron litography, golden pads electrical resitivity measurement and platinum structures electrical resitivity measurement and microstructure transport. Electrical resisti- vity measurement of CeCoIn5 single crystal showed superconductive transition at Tc = 2.27 K and H-T phase diagram was created from measurement in magnetic fields. The result obtained from bulk sample are in agreement with literature. On the other hand measurement of micro-devices showed no superconducting transition, suggesting unsufficient quality of samples. 1
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Effect of flexural loading on electrical properties of alkali-activated slag composites
Šimko, Lukáš ; Kusák, Ivo (referee) ; Rovnaník, Pavel (advisor)
Ordinary concrete is the most commonly used building material, but nowadays the requirements for low energy consumption, durability of structures together with their easy diagnostics as well as ecological production raises. This thesis deals with cement and aluminosilicate composites with content of conductive fillers, which allows to monitor the change in electrical properties, most commonly electrical resistance in dependence on mechanical stress. In the experimental part of the thesis, test beams were produced based on alkali-activated slag with content of carbon nanotubes, graphite powder, carbon black and carbon fibre. The beams were subjected to flexural loading in a three-point bending configuration and the shift in electrical resistance was monitored.
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Characterization of RCo2 singlecrystal
Latoňová, Věra ; Prchal, Jiří (advisor) ; Prokleška, Jan (referee)
The bachelor's thesis deals with the characterization of the cubic DyCo2 single crystal along three principal crystallographical orientations. Mea- surements which were so far performed mainly on polycrystals of the RCo2 group were carried out and evaluated. Measurements of electric resistivity, heat capa- city, magnetization and AC susceptibility showed the first-order magnetic phase transition at Curie temperature TC ≈ 142 K. From magnetization curves the easy [100] and the hard [110] axis was determined. Apart from the basic characterizati- on another interesting effects were found: stairlike development of magnetization curves along [100] at 2 K and an unknown anomaly in the phase component of the magnetic susceptibility at 70 K. Measurement of the AC susceptibility in the pa- ramagnetic area performed to check the presence of the so called parimagnetism did not show any anomaly that had been observed by polycrystalline samples - similar to other single crystals. 1
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The magnetocrystalline anizotropy in the TbTX compounds
Klicpera, Milan
Title: The magnetocrystalline anizotropy in the TbTX compounds Author: Milan Klicpera Department: Department of Condensed Matter Physics Supervisor: doc. Mgr. Pavel Javorský, Dr. Supervisor's e-mail address: javor@mag.mff.cuni.cz Abstract: The subject of this work is the study of structural, magnetic and trans- port properties of the TbNi(Al,In) series to finding connections between magne- tocrystalline anisotropy and lattice parameters of the structure of the TbTX com- pounds. Polycrystalline TbNiAl1−xInx samples were prepared by melting. The phase and crystal structure analysis were provided on samples. We performed the measurements of the magnetization, susceptibility, specific heat, resistivity, low temperature X-ray diffraction and powder neutron diffraction. From the neutron diffraction data we refined lattice parameters and propagation vectors of the series. The main propagation is (000) and second weaker component has the propagation vector (1 2 0 1 2 ). The change of the magnetocrystalline anisotropy from uniaxial to planar type occurs for compounds with x between 0.4 and 0.5. Keywords: magnetization, X-ray and neutron diffraction, electrical resistivity.
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Study of properties of Titanium prepared by SPD methods
Zháňal, Pavel ; Harcuba, Petr (advisor) ; Král, Robert (referee)
In present work the properties of comercially pure titanium fouth grade processed by equal channel angular pressing (ECAP) were studied. Experimental techniques such as Vickers microhardness, measurement of electrical resistivity, light and electron microscopy were used in this research. The dependence of the degree of the strain imposed by ECAP on microhardness of the material was measured. Microhardness measurement was used to indirectly investigate thermal stability of the prepared material, which is essential for ultra fine grained (UFG) materials. That was also the reason for establishing dependence of the electrical resistivity on the temperature. This method allows to detect changes in the material microstructure. Using scanning electron microscopy (SEM) the results obtained by previous methods were confirmed. It was found that the UFG titanium processed by ECAP is thermally stable aproximatelly up to 450řC. At this temperature begins recovery of the material which results in a decrease of the microhardness values and electrical resitivity. For the temperatures higher than 520řC material recrystalization begins.
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Magnetokrystalová anizotropie ve sloučeninách TbTX
Klicpera, Milan ; Javorský, Pavel (advisor) ; Prokleška, Jan (referee)
Title: The magnetocrystalline anizotropy in the TbTX compounds Author: Milan Klicpera Department: Department of Condensed Matter Physics Supervisor: doc. Mgr. Pavel Javorský, Dr. Supervisor's e-mail address: javor@mag.mff.cuni.cz Abstract: The subject of this work is the study of structural, magnetic and trans- port properties of the TbNi(Al,In) series to finding connections between magne- tocrystalline anisotropy and lattice parameters of the structure of the TbTX com- pounds. Polycrystalline TbNiAl1−xInx samples were prepared by melting. The phase and crystal structure analysis were provided on samples. We performed the measurements of the magnetization, susceptibility, specific heat, resistivity, low temperature X-ray diffraction and powder neutron diffraction. From the neutron diffraction data we refined lattice parameters and propagation vectors of the series. The main propagation is (000) and second weaker component has the propagation vector (1 2 0 1 2 ). The change of the magnetocrystalline anisotropy from uniaxial to planar type occurs for compounds with x between 0.4 and 0.5. Keywords: magnetization, X-ray and neutron diffraction, electrical resistivity.
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