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National Repository of Grey Literature 2 records found  Search took 0.00 seconds. 
Electrochemistry with Mass spectrometry as a Tool of Metal Complexes with Organic Ligand Studies
 Jaklová Dytrtová, Jana ; Jakl, M. ; Schröder, Detlef
Electrochemical and mass spectrometric approaches for the detection of metals species with organic ligands are compared. Advantages of the connection of electrochemistry with mass spectrometry are discussed.
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The study of cadmium - oxalic acid complexes using DPASV and ESI-MS
 Jakl, M. ; Jaklová Dytrtová, Jana ; Tlustoš, P.
The combination of DPASV with ESI-MS allows a reliable detection of metal complexes with small organic ligands. The request to exact molecular mass is essential to stoichiometry design simultaneously with low concentration of the analyte in most of biological matrixes. By the analysis of model solution consisting of Cd(NO3)(2) and oxalic acid (OAH(2)) these structures were identified: [Cd(OAH(2))(H2O)(2)](+), [Cd(OAH(2))(H2O)(3)](+), and [Cd(OAH(2))(H2O)(2)(CH3OH)](+). They were also found in soil solution.
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