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Determination of Camphor Content in the Ointment Using Monolithic Column
Voříšková, Michaela ; Kastner, Petr (advisor) ; Mokrý, Milan (referee)
Determination of Camphor content in the ointment using monolithic column Thesis Mgr. Michaela Voříšková Charles University in Prague, Faculty of Pharmacy in Hradec Králové, Department of Pharmaceutical Chemistry and Drug Control The HPLC method for determination of camphor content in pharmaceutical preparation Unguentum camphoratum vaselinatum 10% using monolithic column was developed. The time of analysis was shorted on 1,3 min. The chromatographic column Chromolith Speed rod, RP-18e 50-4,6 mm and chromatographic precolumn Chromolith, RP-18e 10-4,6 mm with mobile phase water : methanol 35 : 65 were used. UV detector for the determination with the setting wave lenght 289 nm was used. The metod was validated for accuracy (recovery = 99,03 %), precision (RSD = 0,83 %), linearity (R = 0,9995) and for specificity. The metod was also tested in other pharmaceutical preparations containing camphor.
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Determination of the Active Substance in Pharmaceutical Preparation II
Voříšková, Michaela ; Kastner, Petr (advisor) ; Pilařová, Pavla (referee)
Determination of the Active Substance in Pharmaceutical Preparation II (Determination of Camphor using HPLC) Thesis Michaela Voříšková Charles University in Prague, Faculty of Pharmacy in Hradec Králové, Department of Pharmaceutical Chemistry and Drug Control The method for determination of camphor content in pharmaceutical preparation Unguentum camphoratum vaselinatum 10% using High Performance Liquid Chromatography was optimalised. The suitable method for sample preparation was found. The chromatographic column Tessek Ltd, SGX C 8 7 µm, CGC 3×150 mm with mobile phase water : methanol 35 : 65 was used. UV detector for the determination with the setting wave lenght 289 nm was used. The method was tested in other pharmaceutical preparations containing camphor.
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Determination of the Active Substance in Pharmaceutical Preparation II
Voříšková, Michaela ; Pilařová, Pavla (referee) ; Kastner, Petr (advisor)
Determination of the Active Substance in Pharmaceutical Preparation II (Determination of Camphor using HPLC) Thesis Michaela Voříšková Charles University in Prague, Faculty of Pharmacy in Hradec Králové, Department of Pharmaceutical Chemistry and Drug Control The method for determination of camphor content in pharmaceutical preparation Unguentum camphoratum vaselinatum 10% using High Performance Liquid Chromatography was optimalised. The suitable method for sample preparation was found. The chromatographic column Tessek Ltd, SGX C 8 7 µm, CGC 3×150 mm with mobile phase water : methanol 35 : 65 was used. UV detector for the determination with the setting wave lenght 289 nm was used. The method was tested in other pharmaceutical preparations containing camphor.
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Determination of Camphor Content in the Ointment Using Monolithic Column
Voříšková, Michaela ; Kastner, Petr (advisor) ; Mokrý, Milan (referee)
Determination of Camphor content in the ointment using monolithic column Thesis Mgr. Michaela Voříšková Charles University in Prague, Faculty of Pharmacy in Hradec Králové, Department of Pharmaceutical Chemistry and Drug Control The HPLC method for determination of camphor content in pharmaceutical preparation Unguentum camphoratum vaselinatum 10% using monolithic column was developed. The time of analysis was shorted on 1,3 min. The chromatographic column Chromolith Speed rod, RP-18e 50-4,6 mm and chromatographic precolumn Chromolith, RP-18e 10-4,6 mm with mobile phase water : methanol 35 : 65 were used. UV detector for the determination with the setting wave lenght 289 nm was used. The metod was validated for accuracy (recovery = 99,03 %), precision (RSD = 0,83 %), linearity (R = 0,9995) and for specificity. The metod was also tested in other pharmaceutical preparations containing camphor.
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