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Determination of inositol in medicinal products by HPLC
Rážová, Michaela ; Odehnalová,, Klára (referee) ; Pazourek,, Jiří (advisor)
This work focuses on the determination of inositol in drugs and food supplements using high-performance liquid chromatography in HILIC mode. The work is divided into several sections, it discusses the characteristics of analyzed myo-inositol including methods for saccharides determination. A chapter is detached for high-performance liquid chromatography. One of the work goals was also chromatography columns comparison. The experimental part includes measurement conditions, methods of sample preparation evaluated data and results including the discussion. Two real samples were analyzed, in both of them the content of myo-inositol was declared by the producer.
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Determination of inositol in medicinal products by HPLC
Rážová, Michaela ; Odehnalová,, Klára (referee) ; Pazourek,, Jiří (advisor)
This work focuses on the determination of inositol in drugs and food supplements using high-performance liquid chromatography in HILIC mode. The work is divided into several sections, it discusses the characteristics of analyzed myo-inositol including methods for saccharides determination. A chapter is detached for high-performance liquid chromatography. One of the work goals was also chromatography columns comparison. The experimental part includes measurement conditions, methods of sample preparation evaluated data and results including the discussion. Two real samples were analyzed, in both of them the content of myo-inositol was declared by the producer.
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Determination of palatinose in food supplements
Rážová, Michaela ; Ing.Robert Ulrich (referee) ; PharmDr.Věra Špačková (advisor)
This work focuses on the determination of palatinose in food supplements using HILIC method. The work is systematically divided into several sections. It contains a basic informations about saccharides including methods for their determination and discusses the characteristics of analyzed palatinose. A chapter s detached for high-performance liquid chromatogramy. The experimental part includes measurement conditions, methods of sample preparation evaluated data and results including the discussion. Four real samples were analysed, in two of them the content of palatinose was declared by producer. Other sugars that we identified were fructose, glucose and sucrose.
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