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Microscopic and structural characterization of high velocity oxygen-flue and atmospheric plasma sprayed coatings
Murafa, Nataliya
;
Štengl, Václav
;
Ctibor, Pavel
;
Houšková, Vendula
TiO2 nano-powders were agglomerated by a spray drying process for applying to thermal spraying High Velocity Oxygen-Fuel (HVOF) and Atmospheric Plasma Spraying (APS) were used to deposit porous partially nanostructured TiO2 coatings Steel substrate was used for a coatings spraying Scanning Electron Microscopy (SEM), and X-Ray diffraction were performed to study the morphology and the crystalline phases of the titania coatings
Detailed record
Photocatalytic niobium and tantallum doped monodispersed nanoparticles of titania for visible-ligt applications
Štengl, Václav
;
Houšková, Vendula
;
Bakardjieva, Snejana
;
Murafa, Nataliya
Niobium or tantalum doped anatase were prepared by thermal hydrolysis of peroxotitanium complex aqueous solutions dissolving niobium or tantalum peroxo-comples at 100 degrees C for 3 days The synthesized samples were characterized by X-ray diffraction (XRD), Scanning Electron Microscopy (SEM), High Resolution Transmission Electron Microscopy (HRTEM), surface area (BET) and porosity determination (BJH) The photocatalytic activity of doped titania samples was determined by decomposition of salicylic acid during irradiation at 365 nm and 400 nm Niobium-doping caused the increase of unit cell constants of anatase and the shape change of anatase crystallites from spindle-like to cubic-like structure. The niobium and tantalum doping increases the stability of anatase to above 1000 degrees C by inhibiting the growth of Mania crystallites.
Detailed record
Synthesis of Ru-doped titania and its photocatalytic properties
Houšková, Vendula
;
Štengl, Václav
;
Murafa, Nataliya
;
Bakardjieva, Snejana
rystalline Mania particles doped with ruthenium oxide have been prepared by homogenous hydrolysis of TiOSO4 in aqueous solutions in the presence of thioacetamide and RuCl3 at 80 degrees C After annealing at 600 degrees C in oxygen atmosphere for 2 hours the synthesis of the Ru-doped Mania powders was complete The effects of the Ru doping on the morphology and microstructure of TiO2 nanoparticles and their impacts on the photocatalytic activity were studied The synthesized particles were characterized by X-ray diffraction (XRD), Scanning Electron Microscopy (SEM) and Nitrogen adsorption-desorption was used for surface area (BET) and porosity determination (BM) The photocatalytic activity of Ru-doped mania samples was determined by photocatalytic decomposition of Orange II dye in an aqueous slurry during irradiation at 365 nm and 400 nm wavelength The Ru-doped Mania samples demonstrated enhanced photocatalytic activity under UV and visible light.
Detailed record
See also: similar author names
3
HOUŠKOVÁ, Veronika
1
Housková, Václava
1
Houšková, V.
3
Houšková, Veronika
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