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National Repository of Grey Literature

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Synthetic studies towards substituted dendralenes Bíba, Ondřej ; Pour, Milan (advisor) ; Špulák, Marcel (referee) Charles University in Prague Faculty of Pharmacy in Hradec Králové Department of Inorganic and Organic Chemistry Candidate: Ondřej Bíba Consultant: Prof. RNDr. Milan Pour, PhD. Title of Thesis: Synthetic studies towards substituted dendralenes The aim of my thesis was to develop an efficient method to synthesize dendralenes with hydroxymethyl moiety attached to the double bonds. These hydroxyls can be protected by various groups (THP or silyl ether formation) during the building of target dendralene. Employed methodology for the formation of dendralene core was hydroalumination-iodation reaction followed by Sonogashira coupling. However, due to lower stability of some intermediates and the necessity of preparing more of them, the overall reaction sequence was not yet finished. Detailed record

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