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Influence of noble earth's elements on Bi based high temperature superconductors phase transition
 Snopek, Jan ; Havlica, Jaromír (referee) ; Ptáček, Petr (advisor)
The Bi2Sr2CaCu2O7+d, i.e. Bi2212 phase of bismuth derived high temperature superconductors (HTS), powder precursor were synthesized via sol – gel technique using ethylendiamintetraacetic acid (Chelaton II) as a chelating agent. Metal nitrate’s solutions were mixed with EDTA suspension. The pH value was adjusted to 9 by NH4OH by reason forming of stable metal’s complexes. The mixture was heated to 80 °C for gelation. Solution taken before solid gel was form is used for preparation of Bi2212 layer on to a-Al2O3 surface via spin coating deposition’s technique. Reactive powder used for bulk sample preparation was made by calcination (800 °C) of pyrolyzed xerogel (500 °C). Sintering in oxygen atmosphere was proceeding at temperature from 850 to 880 °C. Bulk sample properties were compared with sample prepared by common ceramic method. Simultaneous TG-DTA, IR spectroscopy and heating microscopy were used for sample characterization. Furthermore, construction of furnace for sintering in O2 atmosphere was described.
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