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Air contaminants separation process
Krištof, Ondřej ; Pekař, Miloslav (referee) ; Svěrák, Tomáš (advisor)
The Diploma thesis is focused on the separation of gaseous pollutants from contaminated mixtures of gases into liquids using absorbent device. The theoretical part is mainly concerned with describing the absorption process, the method expression and the factors influencing the rate of transfer of contaminants between phases. The experimental part deals with the dependence of transfer of carbon dioxide contained in an air mixture into an aqueous solution of sodium hydroxide on the process conditions of separation in pilot scrubber.
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Kinetics of the continual measurement of the actual fine particulates moisture content.
Mayerová, Kateřina ; Ing.Lukáš Brzobohatý (referee) ; Svěrák, Tomáš (advisor)
This thesis deals with the continual measurement of the hydrated lime moisture content on the principle of spectral measurements. The theoretical part describes the basic principles of the infrared spectroscopy, Fourier transformation and near infrared spectroscopy, which are used in the process of the spectroscopy measurement of fine particulates moisture content. The practical part of the work describes experiments and the evaluation of moisture hydrated lime measuring results, using gravimetric method and NIR spectroscopy in both the laboratory conditions and the conditions of operation production of hydrated lime as well. The part of the work monitors the spectroscopy measurement moisture values as the dependence on the optical quality of hydrate limes and the process conditions of the measurements.
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Genesis of new ultra-fine particles of milling stock in the course of the mill exposure.
Kejík, Pavel ; Pekař, Miloslav (referee) ; Svěrák, Tomáš (advisor)
This work deals with the study of limestone and corundum dry milling using attritor-type stirred mill in a batch mode. There were stearin and polyethylene glycol used as surfactants and spherical shaped steel grinding elements used for the experimental part of the work. The main idea was to examine behavior of the selected grinding stock type within a long-term grinding forces exposure in selected conditions of ultrafine dry milling leading up to the submicron area. Characterization of samples was performed by laser granulometry, X-ray powder diffraction analysis, flame atomic absorption spectroscopy, objective color determination and electrokinetic potential measurement. Experimetaly measured data implies that in all cases there was a re-agglomeration of the grinding stock particles occurring, although in different stages of the disintegration process and in mutually various degree. The analysis results denote that a larger erosion of the crystal structures with the associated increase of the amorphous phase in the submicron particle size took place in the grinding stock.
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Bulk properties of fine powders.
Zubek, Piotr ; Roman,, Fekete (referee) ; Svěrák, Tomáš (advisor)
The subject of this thesis is the measurement of flow properties of powder materials. The theoretical part deals with particulate substances in general and describes the basic principles of flow behavior of powder materials. In the theoretical part is a description of the Jenike Shear Tester and Ring Shear Tester. The following section summarizes the Standard Shear Testing Technique. Measurements were carried out on the new apparatus Laboratory of Chemical Engineering. The measurement was selected 5 samples of limestone Omyacarb ® from Omya CZ s.r.o. Individual samples varied in four different particle size distributions and one sample was surface-modified hydrophobic stearic acid. Tests were conducted at 3 levels of the preshear normal stress - 2.5 kPa, 5 kPa and 7.5 kPa. Distribution function of particle size in the material data sheets supplied by the manufacturer were verified using a laser particle size analyzer Sympatec Helos KR purchased in the Materials Research Centre at the Faculty of Chemistry at Brno University of Technology.
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Gaseous atmospheric contaminants stripping
Kalivoda, Josef ; Kotlík, Josef (referee) ; Svěrák, Tomáš (advisor)
The Diploma thesis is devoted to the absorption of gases by the experimental gas scrubber. The main attention of the theoretical part is focused on the description of absorption, kinetics and the equilibrium between gas and liquid phase. Experimental part is concentrated on the absorption of carbon dioxide to deionized water in the experimental scrubber. Finally, experimental data are discussed.
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Milling activators use in the very fine powder material practice.
Borguľová, Eva ; Kejík, Pavel (referee) ; Svěrák, Tomáš (advisor)
This work deals with the study of clinker dry milling using ball mill with the sferical shaped steel grinding elements in it. Grinding aids are surface active substances, wich separate particles of milled substance and prevent their reaglomeration and can active the proces of the grinding.There will be used PEG, TEA and HEAas a surfactans. Characterization of samples will be performed by granulometry.
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Preparation of WDXRF analysis cement tablets
Kozlová, Romana ; Lerch, Jiří (referee) ; Svěrák, Tomáš (advisor)
This bachelor's thesis is focused on the sample preparation for the X-ray fluorescent analysis (XRF) of cement. The thesis aims to contribute to finding optimal method of the sample preparation of cement in the form of tablets, which would then provide the most accurate XRF analysis. This activity is related with finding a method of the sample preparation with an appropriate granulometry and homogeneity of the powder material, and also is related with creating the conditions of pressing of this material in the form of compact tablets, which are not prone to fracture. Selected problem was solved by adjusting twenty possible parameters of the mill and press. The milling was evaluated by granulometric composition of the sample, which was determined by a laser diffraction. For the smallest sample the repeatability of measurement was performed. Sieve distribution was used to achieve a finer sample, followed by XRF analysis. Tests of strength of samples pressed into ringlets were performed using a three-point tensile strength in bending, for samples with the finest and most coarse composition. The chemical composition of the finest and most coarse sample, which was prepared by milling and also the sample after milling and sieve distribution, was verified with the XRF analysis. By combining the 20 parameters during the sample preparation, maximum accuracy of the XRF analysis was achieved. The final setting meet the granulometric requirements and also abrasive and strength tests of tablets after pressing the sample. The contribution of this work is an increase in accuracy of the XRF analysis to a better level than ever before. As a result the negative impacts, which directly affect he accuracy and reproducibility of the sample preparation for the XRF analysis, were minimized. The resulting sample preparation was applied to the laboratory of quality and quality control at Českomoravský cement a.s., Mokrá plant, for which this work has been performed.
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Mechatronics of classifying of microparticles by air separation
Adamčík, Martin ; Svěrák, Tomáš (referee) ; Pellant, Karel (advisor)
The aim of presentated bachelor’s thesis is exploration of the possibilities of classifying the microparticles according to the size of particles of the material and modelling the specific classifier and its parts in 3D system. This thesis describes in detail air separation method, its utilization and benefits. For this purpose, in thesis are solved those particular problems. a)Description of the classification process. Definition of the particle size distribution, discussion the influence of the classifier parameters to the particle size distribution. b)Analysis of particular devices used for classification of particles in the process. c)Engineering design of the classification system of the air classifier. d)Modelling out designed device in the 3D system.
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Continual actual moisture of fine particulates measurement possibilities.
Mayerová, Kateřina ; Ing.Lukáš Brzobohatý (referee) ; Svěrák, Tomáš (advisor)
This thesis describes the process of measuring a hydrated lime moisture, using gravimetric method and FT-NIR spectroscopy. The aim of the theretical part was to analyse and present the area of infrared spectroscopy (IR), gathering the general information about infrared spectroscopy, Fourier transformation and near infrared spectroscopy (NIR). Experimental part of the thesis was carried out in limekiln Carmeuse in Mokré town, where the FT-NIR spectroscopy was investigated for possible usage in on-line measuring of hydrated lime moisture.
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