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National Repository of Grey Literature

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	Preparation of Nanocrystalline Titania Thin Films and Aerogels by using Modified Supercritical Carbon Dioxide. Cerhová, Marie The purity and crystallinity of prepared TiO2 thin films and aerogels were estimated by Raman spectroscopy. The crystallite size and the phase composition were determined by X-ray diffraction. Textural properties of aerogels such as the surface area and the pore-size distribution were characterized by nitrogen physisorption and helium pycnometry measurements. Fulltext: content.csg - PDF Plný tet: SKMBT_C22016053109270 - PDF Detailed record
	Preparation of Nanostructured Titania Thin Films Using Supercritical Carbon Dioxide Cerhová, Marie ; Sajfrtová, Marie ; Matějová, L. ; Dřínek, Vladislav ; Daniš, S. ; Jandová, Věra Extrakce čistým a modifikovaným superkritickým oxidem uhličitým (SFE) a extrakce podkritickou vodou byla využita k získání krystalických a čistých nanostrukturních tenkých filmů TiO2 a současně k odstranění organických prekurzorů ze syntézy solu sol-gel metodou. Při SFE byl sledován vliv teploty a použitého modifikátoru (vody, metanolu, etanolu a acetonu) na čistotu a mikrostrukturu tenkých filmů TiO2. Byl testován i kombinovaný postup extrakce, kdy se střídaly kroky s CO2 modifikovaným vodou a s CO2 modifikovaným organickými rozpouštědly. Čistota a krystalinita tenkých filmů byla zjištěna pomocí Ramanovy spektroskopie. Fázová složení a velikosti krystalů anatasu, žádané krystalické struktury, byly vyhodnoceny rentgenovou difrakční analýzou (XRD). Fulltext: content.csg - PDF Plný tet: SKMBT_C22015111812130 - PDF Detailed record
	Progress in Helicene Stationary Phases Cerhová, Marie The motivation of this work is to utilize the SFE for the direct preparation of highly pure TiO2 thin films without any subsequent thermal processing. Extraction with pure and modified scCO2 was tested and compared with PLE. Different types of liquid solvents (water, ethanol, acetone etc.) were used as scCO2 modifiers at concentrations from 0 to 30 mass %. The effect of extraction temperature (40–150 °C), pressure (10–65 MPa) and the volume (50–200 g) and flow rate (0.3–1.8 g/min) of solvents passed through the extractor on microstructure and purity of TiO2 thin films were examined. Fulltext: content.csg - PDF Plný tet: SKMBT_C22015061709363 - PDF Detailed record

National Repository of Grey Literature : 13 records found   11 - 13  jump to record:

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1	Cerhová, Markéta

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