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Reaction synthesis of bulk Fe-Al intermetallic materials
Dyčková, Lucie ; Hutařová, Simona (referee) ; Jan, Vít (advisor)
Bachelor’s thesis deals with iron aluminides. In literature analysis are the best known and the most widely used intermetallics materials, diffusion and other possible processing technologies of intermetallic materials. In experimental part was used sprayed coating. This sprayed coating was produced by cold gas-dynamic spray. In this thesis were analysed changes in microstructure of iron aluminides depending on annealing temperature. This thesis contains photographs of microstructure and analyses from electron microscopy and measurement of microhardness.
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Reaction synthesis of bulk intermetallic materials from kinetic spraying deposits
Stejskal, Pavel ; Roupcová, Pavla (referee) ; Jan, Vít (advisor)
This work deals with issues of preparation of intermetallics based on iron, nickel and titanium aluminides. It works with an idea of preparation of bulk material by reaction synthe-sis from kinetic spraying deposits by cold spray. Theoretical part is concerned with phases and compounds of these aluminides for structural applications, their characteristics and present fabrication. In experimental part there are studied microstructures created by annealing of deposits.
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Reaction synthesis of bulk intermetallic materials from kinetic spraying deposits
Stejskal, Pavel ; Roupcová, Pavla (referee) ; Jan, Vít (advisor)
This work deals with issues of preparation of intermetallics based on iron, nickel and titanium aluminides. It works with an idea of preparation of bulk material by reaction synthe-sis from kinetic spraying deposits by cold spray. Theoretical part is concerned with phases and compounds of these aluminides for structural applications, their characteristics and present fabrication. In experimental part there are studied microstructures created by annealing of deposits.
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Reaction synthesis of bulk Fe-Al intermetallic materials
Dyčková, Lucie ; Hutařová, Simona (referee) ; Jan, Vít (advisor)
Bachelor’s thesis deals with iron aluminides. In literature analysis are the best known and the most widely used intermetallics materials, diffusion and other possible processing technologies of intermetallic materials. In experimental part was used sprayed coating. This sprayed coating was produced by cold gas-dynamic spray. In this thesis were analysed changes in microstructure of iron aluminides depending on annealing temperature. This thesis contains photographs of microstructure and analyses from electron microscopy and measurement of microhardness.
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Comparison of Al/Ni and Co/Ni Interdiffusion Coefficients in Pseudobinary Sections of Ni3Al-Co alloys
Gazda, Aleš ; Rothová, Věra ; Čermák, Jiří
Interdiffusion in Ni3Al intermetallic alloyed by 0 - 19 at % Co was studied in three pseudo-binary sections: c(Al) = 22, c(Co) = 3.5, and c(Co) = 16 (c in at. %). The experiments were carried out at temperatures between 900 and 1200°C. Since no detectable shift of tungsten inert markers was observed, it was concluded that the intrinsic diffusivities of element pairs with varying concentration (Al/Ni and Co/Ni) in respective pseudo-binary sections are approximately equal one to another. The interdiffusion in pseudo-binary alloys Al/Ni (c(Co) = const.) runs slightly faster than that in pseudo-binary alloys Ni/Co (c(Al) = const.). The relations between the measured interdiffusion coefficients in the Ni3Al-Co ordered gamma prime phase agree well with literature data for the interdiffusion coefficients in both pure gamma prime and Co alloyed gamma prime phases and also for the disordered Al-Ni and Co-Ni solid solutions. They are qualitatively explained by interaction between constituents and/or by their interaction with vacancies.
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