Home > Search Results: keywords:"mictrowave plasma"
Search:
Search Tips :: Advanced Search
Search collections:
Sort by: Display results: Output format:
National Repository of Grey Literature 1 records found  Search took 0.01 seconds. 
α-Fe nanočástice připravené rozkladem pentakarbonylu železa v mikrovlnném výboji
 David, Bohumil ; Pizúrová, Naděžda ; Schneeweiss, Oldřich ; Hoder, T. ; Kudrle, V. ; Janča, J.
The nanocrystalline iron powder has been prepared by the introducing of Fe(CO)5 vapor into the microwave induced argon discharge. A microwave 2.45 GHz source was operated at 430 W. The reaction was performed in a quartz tube passing through the microwave waveguide. The in-situ passivation using air was applied after synthesis. The powder was characterised by TEM, XRD, and Mössbauer spectroscopy. According to our TEM investigation, the produced passivated powder included aggregated core-shell nanoparticles. The cores consist of α-Fe and the shell is supposed to be iron oxide (indicated by TEM). The presence of α-Fe and iron oxides was confirmed by XRD and Mössbauer spectroscopy. The mean coherence domain size of α-Fe cores was estimated to be 30 nm. The synthesized nanopowder exhibits ferromagnetic behaviour.
Detailed record

Interested in being notified about new results for this query?
Subscribe to the RSS feed.
Digital Repository :: Search :: Submit :: Personalize :: Help
Powered by Invenio v1.1.2
Maintained by admin.invenio@techlib.cz
This site is also available in the following languages:
Česky  English