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National Repository of Grey Literature 2 records found  Search took 0.00 seconds. 
Lanthanidocenes and their Precursors Synthesis
 Kašpárek, Vít ; Hermanová, Soňa (referee) ; Richtera, Lukáš (advisor)
The first section of this bachelor’s thesis aims on a theoretical basis used to characterize new preparation substances, especially x-ray diffraction, infrared spectroscopy, Raman spectroscopy and nuclear magnetic resonance spectroscopy. The next section deals with the basic structural types of lanthanidocenes according to the substituted ligands. The last theoretical section deals with work in the gloves box and the preparation of the laboratory glasses for the work in the inert atmosphere. The aim of the experimental section was the synthesis of methoxyethane, characterization of its purity using FT-IR and its next usage in the change of organic ligands in structure of (C5Me5)SmCl2Li(OEt2)2.
Detailed record
Lanthanidocenes and their Precursors Synthesis
 Kašpárek, Vít ; Hermanová, Soňa (referee) ; Richtera, Lukáš (advisor)
The first section of this bachelor’s thesis aims on a theoretical basis used to characterize new preparation substances, especially x-ray diffraction, infrared spectroscopy, Raman spectroscopy and nuclear magnetic resonance spectroscopy. The next section deals with the basic structural types of lanthanidocenes according to the substituted ligands. The last theoretical section deals with work in the gloves box and the preparation of the laboratory glasses for the work in the inert atmosphere. The aim of the experimental section was the synthesis of methoxyethane, characterization of its purity using FT-IR and its next usage in the change of organic ligands in structure of (C5Me5)SmCl2Li(OEt2)2.
Detailed record

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