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Machinable bioceramics prepared by gelcasting method
Kolář, Martin ; Částková, Klára (referee) ; Trunec, Martin (advisor)
In the diploma thesis, overviews of the existing literature focused on the gelcasting method and based on the findings were prepared aqueous slurries of zirconium oxide for gelcasting method. These suspensions were examined for the influence of the content ceramics powder, type and content of dispersants and volume of initiator on viscosity of aqueous suspensions and process of polymerization. Optimum ceramic suspension had 45 vol.% of ceramic powder which was stabilized by 0,5 weight % of dispersant Dolapix CE 64. Polymerization running at room temperature was initiated by 0,175 weight % of ammonium persufate without accelerator. Microstructure of prepared ceramic blanks and sintered bodies was compared with body prepared by isostatic pressing. For the machining tests were prepared blanks in disc-shaped.
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Milling optimization of ceramic blanks
Ráčková, Jana ; Pouchlý, Václav (referee) ; Trunec, Martin (advisor)
The master thesis deals mainly with the optimization of machining of ceramic semi-finished products from ZrO2 and Al2O3. The first part with literary research, which describes the steps of the technology of forming ceramic bodies, especially the gelcasting method. The thesis describes possibilities of milling of ceramic materials using CNC technology. The thesis describes the dependence of acquired roughness on bodies and used machining strategies. The best roughness parameters on ZrO2 samples were obtained after they were calcined at 900 ° C, while the lowest roughness was obtained on the samples in the unprotected state for the Al2O3 samples. Samples machined with a spherical milling cutter showed surface roughness Ra = 1 m for ZrO2 and Ra = 1.3 m for Al2O3. It also describes the possibility of machining sharp-edged shapes and fine details where the best results are achieved on ZrO2 samples engraved at 900 and 1100 °C. Tool wear was particularly important when machining samples of Al2O3 ignited at temperatures above 800 °C.
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Preparation of large and complex-shaped ceramics parts
Prehradná, Jana ; Pouchlý, Václav (referee) ; Trunec, Martin (advisor)
This bachelor’s thesis deals with research of ceramic materials in field of material engineering. The first part deals with biomaterials, especially bioceramics, its types, properties and its usage. The second part of this thesis deals with transparent ceramics and the third part includes the procedure and method of gel casting. The experimental part is dedicated to production of large and complex shaped components - knee joint, spherical cover and discs with transparent properties. The method of gelcasting was used for samples preparation of this type. The task was not only to produce these samples, but also to find suitable surrounding conditions for the proper course of the entire production process.
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Gelcasting of Advanced Ceramics
Veselý, Jan ; Maca, Karel (referee) ; Trunec, Martin (advisor)
In Bachelor thesis, a literary overview of gelcasting method was worked out and pursuant to this overview, composition of alumina suspension was optimised for fabrication of bulky and complex-shape ceramic part. Four variants of ceramic powder filling in suspensions were prepared. Based on the experiments, a suspension with powder loading of 47,5 vol. % was chosen. The ratio between linear and crosslinking monomers was investigated for this suspension. A suspension with monomer ratio of 4 : 1 (linear : crosslinking) was chosen for preparation of bulky and complex-shape ceramic part. Gelcasting was verified by fabrication of ceramic medal and a knee-joint.
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Milling optimization of ceramic blanks
Ráčková, Jana ; Pouchlý, Václav (referee) ; Trunec, Martin (advisor)
The master thesis deals mainly with the optimization of machining of ceramic semi-finished products from ZrO2 and Al2O3. The first part with literary research, which describes the steps of the technology of forming ceramic bodies, especially the gelcasting method. The thesis describes possibilities of milling of ceramic materials using CNC technology. The thesis describes the dependence of acquired roughness on bodies and used machining strategies. The best roughness parameters on ZrO2 samples were obtained after they were calcined at 900 ° C, while the lowest roughness was obtained on the samples in the unprotected state for the Al2O3 samples. Samples machined with a spherical milling cutter showed surface roughness Ra = 1 m for ZrO2 and Ra = 1.3 m for Al2O3. It also describes the possibility of machining sharp-edged shapes and fine details where the best results are achieved on ZrO2 samples engraved at 900 and 1100 °C. Tool wear was particularly important when machining samples of Al2O3 ignited at temperatures above 800 °C.
|
|
|
Machinable bioceramics prepared by gelcasting method
Kolář, Martin ; Částková, Klára (referee) ; Trunec, Martin (advisor)
In the diploma thesis, overviews of the existing literature focused on the gelcasting method and based on the findings were prepared aqueous slurries of zirconium oxide for gelcasting method. These suspensions were examined for the influence of the content ceramics powder, type and content of dispersants and volume of initiator on viscosity of aqueous suspensions and process of polymerization. Optimum ceramic suspension had 45 vol.% of ceramic powder which was stabilized by 0,5 weight % of dispersant Dolapix CE 64. Polymerization running at room temperature was initiated by 0,175 weight % of ammonium persufate without accelerator. Microstructure of prepared ceramic blanks and sintered bodies was compared with body prepared by isostatic pressing. For the machining tests were prepared blanks in disc-shaped.
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|
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Preparation of large and complex-shaped ceramics parts
Prehradná, Jana ; Pouchlý, Václav (referee) ; Trunec, Martin (advisor)
This bachelor’s thesis deals with research of ceramic materials in field of material engineering. The first part deals with biomaterials, especially bioceramics, its types, properties and its usage. The second part of this thesis deals with transparent ceramics and the third part includes the procedure and method of gel casting. The experimental part is dedicated to production of large and complex shaped components - knee joint, spherical cover and discs with transparent properties. The method of gelcasting was used for samples preparation of this type. The task was not only to produce these samples, but also to find suitable surrounding conditions for the proper course of the entire production process.
|
|
|
Gelcasting of Advanced Ceramics
Veselý, Jan ; Maca, Karel (referee) ; Trunec, Martin (advisor)
In Bachelor thesis, a literary overview of gelcasting method was worked out and pursuant to this overview, composition of alumina suspension was optimised for fabrication of bulky and complex-shape ceramic part. Four variants of ceramic powder filling in suspensions were prepared. Based on the experiments, a suspension with powder loading of 47,5 vol. % was chosen. The ratio between linear and crosslinking monomers was investigated for this suspension. A suspension with monomer ratio of 4 : 1 (linear : crosslinking) was chosen for preparation of bulky and complex-shape ceramic part. Gelcasting was verified by fabrication of ceramic medal and a knee-joint.
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