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Application of Technique of Oriented Foils in TEM
Buček, Petr ; Kruml, Tomáš (referee) ; Petrenec, Martin (advisor)
The master’s thesis is focused on the application of the technique of oriented foils in transmission electron microscopy. Dislocation structures were identified by this technique in both phases of polycrystalline austenitic-ferritic stainless steel SAF 2507 formed during low cycle fatigue at two plastic strain amplitudes ap. In individual grains the stress axis and the Schmid factors of active slip systems were determined. In austenitic grains, the planar structures were determined at both ap. In ferritic grains, the dislocation arrangement was different for the two observed ap. Individual screw dislocations and pile-up´s of edge dislocations were found at low ap = 1x10-4. Mixture of vein and wall dislocation structures were formed at high ap = 2x10-3. Observed dislocation structures were discussed in relation with the cyclic plastic response of the duplex stainless steel.
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Measurement of oxygen activity in ferro-alloys
Žák, Štěpán ; Čamek, Libor (referee) ; Záděra, Antonín (advisor)
The thesis deals with determination of the oxygen content in ferro-alloys with emphasis on direct oxygen activity measurement in the meltage. The practical part of the thesis contains statistical analysis of oxygen activity values measured in austenitic and duplex stainless steel meltages. The measurements were done in vacuum furnace before vacuuming and afterwards. Statistically significant dependency of oxygen activity on the temperature of meltage was discovered among the values measured after the vacuuming. Therefore, its value can be predicted based just on the temperature of the meltage. No statistically significant dependency was found among the values measured before vacuuming (except for the low Chromium austenitic stainless steel meltages). Hence, other factors need to be considered when predicting oxygen activity before vacuuming.
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Manufacturing, use and properties of duplex austenitic-ferritic steels
Klapetek, Václav ; Blažík, Petr (referee) ; Myška, Martin (advisor)
This bachelor thesis focuses on stainless duplex austenitic-feritic steels. The first chapter is focused on mechanical and technological properties, microstructure and chemical proposition with its impact on corrosion resistance, following the introduction to the issue. Intermetallic phases and their effect on properties are also described. Second chapter deals with their usage in several industry spheres, such as petrochemical industry, paper-producing, transport and storage of chemicals etc.
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Measurement of oxygen activity in ferro-alloys
Žák, Štěpán ; Čamek, Libor (referee) ; Záděra, Antonín (advisor)
The thesis deals with determination of the oxygen content in ferro-alloys with emphasis on direct oxygen activity measurement in the meltage. The practical part of the thesis contains statistical analysis of oxygen activity values measured in austenitic and duplex stainless steel meltages. The measurements were done in vacuum furnace before vacuuming and afterwards. Statistically significant dependency of oxygen activity on the temperature of meltage was discovered among the values measured after the vacuuming. Therefore, its value can be predicted based just on the temperature of the meltage. No statistically significant dependency was found among the values measured before vacuuming (except for the low Chromium austenitic stainless steel meltages). Hence, other factors need to be considered when predicting oxygen activity before vacuuming.
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Manufacturing, use and properties of duplex austenitic-ferritic steels
Klapetek, Václav ; Blažík, Petr (referee) ; Myška, Martin (advisor)
This bachelor thesis focuses on stainless duplex austenitic-feritic steels. The first chapter is focused on mechanical and technological properties, microstructure and chemical proposition with its impact on corrosion resistance, following the introduction to the issue. Intermetallic phases and their effect on properties are also described. Second chapter deals with their usage in several industry spheres, such as petrochemical industry, paper-producing, transport and storage of chemicals etc.
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|
|
Application of Technique of Oriented Foils in TEM
Buček, Petr ; Kruml, Tomáš (referee) ; Petrenec, Martin (advisor)
The master’s thesis is focused on the application of the technique of oriented foils in transmission electron microscopy. Dislocation structures were identified by this technique in both phases of polycrystalline austenitic-ferritic stainless steel SAF 2507 formed during low cycle fatigue at two plastic strain amplitudes ap. In individual grains the stress axis and the Schmid factors of active slip systems were determined. In austenitic grains, the planar structures were determined at both ap. In ferritic grains, the dislocation arrangement was different for the two observed ap. Individual screw dislocations and pile-up´s of edge dislocations were found at low ap = 1x10-4. Mixture of vein and wall dislocation structures were formed at high ap = 2x10-3. Observed dislocation structures were discussed in relation with the cyclic plastic response of the duplex stainless steel.
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