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Application of Technique of Oriented Foils in TEM
Buček, Petr ; Kruml, Tomáš (referee) ; Petrenec, Martin (advisor)
The master’s thesis is focused on the application of the technique of oriented foils in transmission electron microscopy. Dislocation structures were identified by this technique in both phases of polycrystalline austenitic-ferritic stainless steel SAF 2507 formed during low cycle fatigue at two plastic strain amplitudes ap. In individual grains the stress axis and the Schmid factors of active slip systems were determined. In austenitic grains, the planar structures were determined at both ap. In ferritic grains, the dislocation arrangement was different for the two observed ap. Individual screw dislocations and pile-up´s of edge dislocations were found at low ap = 1x10-4. Mixture of vein and wall dislocation structures were formed at high ap = 2x10-3. Observed dislocation structures were discussed in relation with the cyclic plastic response of the duplex stainless steel.
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Application of Technique of Oriented Foils in TEM
Buček, Petr ; Kruml, Tomáš (referee) ; Petrenec, Martin (advisor)
The master’s thesis is focused on the application of the technique of oriented foils in transmission electron microscopy. Dislocation structures were identified by this technique in both phases of polycrystalline austenitic-ferritic stainless steel SAF 2507 formed during low cycle fatigue at two plastic strain amplitudes ap. In individual grains the stress axis and the Schmid factors of active slip systems were determined. In austenitic grains, the planar structures were determined at both ap. In ferritic grains, the dislocation arrangement was different for the two observed ap. Individual screw dislocations and pile-up´s of edge dislocations were found at low ap = 1x10-4. Mixture of vein and wall dislocation structures were formed at high ap = 2x10-3. Observed dislocation structures were discussed in relation with the cyclic plastic response of the duplex stainless steel.
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Low cycle fatigue on Inconel 713L and Inconel 792-5A superalloys at 500 A 700 °C
Petrenec, Martin ; Obrtlík, Karel ; Polák, Jaroslav ; Hrbáček, K. ; Kruml, Tomáš
Cylindrical specimens of cast polycrystalline nickel base superalloys Inconel 713LC and 792-5A were cyclically strained under total strain control at500°C and at700°C.Structural characteristics and morphology of gama´ precipitates of both materials are documented. Dislocations structures were studied using transmission electron microscopy using technique of oriented foils in selected specimens cyclically strained up to failure. Cyclic hardening/softening curves, cyclic stress-strain curves, and fatigue life curves were obtained for both temperatures. Cyclic hardening/softening curves depend both on temperature and plastic strain amplitude. The cyclic stress-strain curves can be approximated by power law. Experimental points of fatigue life curves satisfy the Manson-Coffin and Basquin law. Stress-strain response and fatigue life characteristics are compared at both temperatures and discussed in relative to structural parameters and to dislocation structures of superalloys studied.
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