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Modification of HVOF and cold spray deposited coatings via electron beam technology
Vacek, Petr ; Šiška, Filip (referee) ; Čížek, Jan (advisor)
The aim of this thesis was to modify microstructure and coating-substrate interface of CoNiCrAlY coatings deposited by HVOF and cold spray on Inconel 718 substrates. Electron beam remelting and annealing in a protective atmosphere were used to modify the coatings. Microstructure, chemical and phase composition were analyzed. The effect of beam current, transversal velocity and beam defocus on remelted depth was evaluated. As-sprayed microstructure and chemical composition of coatings were analyzed and compared with remelted samples. The effect of annealing of the as-sprayed and remelted samples was evaluated. Remelted layers exhibited dendritic structure. Chemical composition changed only after remelting of interface and part of a substrate. When only the coating was remelted, chemical composition remained the same. Phases coarsened after the annealing. Chemical composition changed after annealing due to the diffusion.
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Microstructure and properties of YSZ thermal barier coatings deposited onto CoNiCrAlY bond coats remelted by electron beam
Slavíková, Barbora ; Jan, Vít (referee) ; Dlouhý, Ivo (advisor)
The master thesis is dealing with characterization of the structure and properties of the YSZ thermal barrier coating deposited by water hybrid plasma spray technology on the CoNiCrAlY bond coats modified by using electron beam and vacuum annealing. Deposition of the bond coats was performed via high velocity oxy-fuel technology and cold spray. In case of experimental evaluation, the microstructure and chemical composition of the ceramic top coat deposited with powder and suspension feedstock was analyzed. The same analysis procedure was used also for bond coats after electron beam remelting by using two sets of parameters. Furthermore, the changes in microstructure and chemical composition of the remelted and annealed bond coats was evaluated. Eventually, the micromechanical properties of the top coats and the bond coats were measured. The ceramic top coats deposited with powder feedstock exhibited the structure composed by splats, while the top coats deposited in form of suspension showed fine structure with columnar grains. The dendritic structure was observed on remelted bond coats. The annealing process had an influence on the structure in form of coarsened phases and the chemical composition was changed due to diffusion of the elements.
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Microstructure and properties of YSZ thermal barier coatings deposited onto CoNiCrAlY bond coats remelted by electron beam
Slavíková, Barbora ; Jan, Vít (referee) ; Dlouhý, Ivo (advisor)
The master thesis is dealing with characterization of the structure and properties of the YSZ thermal barrier coating deposited by water hybrid plasma spray technology on the CoNiCrAlY bond coats modified by using electron beam and vacuum annealing. Deposition of the bond coats was performed via high velocity oxy-fuel technology and cold spray. In case of experimental evaluation, the microstructure and chemical composition of the ceramic top coat deposited with powder and suspension feedstock was analyzed. The same analysis procedure was used also for bond coats after electron beam remelting by using two sets of parameters. Furthermore, the changes in microstructure and chemical composition of the remelted and annealed bond coats was evaluated. Eventually, the micromechanical properties of the top coats and the bond coats were measured. The ceramic top coats deposited with powder feedstock exhibited the structure composed by splats, while the top coats deposited in form of suspension showed fine structure with columnar grains. The dendritic structure was observed on remelted bond coats. The annealing process had an influence on the structure in form of coarsened phases and the chemical composition was changed due to diffusion of the elements.
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Modification of HVOF and cold spray deposited coatings via electron beam technology
Vacek, Petr ; Šiška, Filip (referee) ; Čížek, Jan (advisor)
The aim of this thesis was to modify microstructure and coating-substrate interface of CoNiCrAlY coatings deposited by HVOF and cold spray on Inconel 718 substrates. Electron beam remelting and annealing in a protective atmosphere were used to modify the coatings. Microstructure, chemical and phase composition were analyzed. The effect of beam current, transversal velocity and beam defocus on remelted depth was evaluated. As-sprayed microstructure and chemical composition of coatings were analyzed and compared with remelted samples. The effect of annealing of the as-sprayed and remelted samples was evaluated. Remelted layers exhibited dendritic structure. Chemical composition changed only after remelting of interface and part of a substrate. When only the coating was remelted, chemical composition remained the same. Phases coarsened after the annealing. Chemical composition changed after annealing due to the diffusion.
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