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Piezoelectric nanofiber materials for wearable electronics
Frolíková, Štěpánka ; Škarvada, Pavel (referee) ; Macků, Robert (advisor)
This thesis deals with the influence of production parameters on the morphology of PVDF nanofibers produced by electrospinning. Nanofibers are generally a widely used material, nanofibers are generally a widely used material, they can also have piezoelectric properties, which gives them a specific spectrum of use, eg in biosensors. The production of nanofibers was realized by electrospinning. A scanning electron microscope was used to examine the morphology and surface properties. The aim of this thesis is to compare the properties of PVDF nanofibers produced under different settings of production parameters.
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Study of intermetallic phases in cast duplex steel
Ponížil, Ondřej ; Foret, Rudolf (referee) ; Pacal, Bohumil (advisor)
This thesis deals with the study of intermetallic phases in cast duplex stainless steel ASTM A890 Grade 4A considering degradation of mechanical properties in the result of isothermal aging in the temperature of 700 °C and 595 °C. The period of aging in the temperature of 700 °C was ranging from 1 to 160 hours and in the temperature of 595 °C it was ranging from 24 to 245 hours. The study of microstructure after aging in the temperature of 700 °C has proved that the -phases, Laves phases, chromium carbides and chromium nitrides were excluded. The phase was observed after four hours of aging in the temperature of 700 °C in / interface for the first time. The transformation was performed by eutectoid mechanism according to the equation + 2. The Laves phase has been observed after 10 hours of aging in / interphase and later in the ferrite grain as well. Chromium carbides and nitrides have created a continuous contour along to the / and /2 interface. After the temperature of 595°C there have been observed a large amount of small precipitates in the structure. The precipitates have been extracted from some selected samples to carbon replica. Following analysis has confirmed the presence of chromium carbides, -phases and Laves phases. The deterioration of mechanical properties, caused by the influence of secondary phase exclusion, has been confirmed by the Vickers hardness test and impact test including fractography analysis of the fracture surface. The hardness has an increasing tendency while the impact strength has been significantly reduced.
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Piezoelectric nanofiber materials for wearable electronics
Frolíková, Štěpánka ; Škarvada, Pavel (referee) ; Macků, Robert (advisor)
This thesis deals with the influence of production parameters on the morphology of PVDF nanofibers produced by electrospinning. Nanofibers are generally a widely used material, nanofibers are generally a widely used material, they can also have piezoelectric properties, which gives them a specific spectrum of use, eg in biosensors. The production of nanofibers was realized by electrospinning. A scanning electron microscope was used to examine the morphology and surface properties. The aim of this thesis is to compare the properties of PVDF nanofibers produced under different settings of production parameters.
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Study of intermetallic phases in cast duplex steel
Ponížil, Ondřej ; Foret, Rudolf (referee) ; Pacal, Bohumil (advisor)
This thesis deals with the study of intermetallic phases in cast duplex stainless steel ASTM A890 Grade 4A considering degradation of mechanical properties in the result of isothermal aging in the temperature of 700 °C and 595 °C. The period of aging in the temperature of 700 °C was ranging from 1 to 160 hours and in the temperature of 595 °C it was ranging from 24 to 245 hours. The study of microstructure after aging in the temperature of 700 °C has proved that the -phases, Laves phases, chromium carbides and chromium nitrides were excluded. The phase was observed after four hours of aging in the temperature of 700 °C in / interface for the first time. The transformation was performed by eutectoid mechanism according to the equation + 2. The Laves phase has been observed after 10 hours of aging in / interphase and later in the ferrite grain as well. Chromium carbides and nitrides have created a continuous contour along to the / and /2 interface. After the temperature of 595°C there have been observed a large amount of small precipitates in the structure. The precipitates have been extracted from some selected samples to carbon replica. Following analysis has confirmed the presence of chromium carbides, -phases and Laves phases. The deterioration of mechanical properties, caused by the influence of secondary phase exclusion, has been confirmed by the Vickers hardness test and impact test including fractography analysis of the fracture surface. The hardness has an increasing tendency while the impact strength has been significantly reduced.
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