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Stability of aprotic electrolytes in lithium-ion batteries
Krištofík, František ; Máca, Josef (referee) ; Sedlaříková, Marie (advisor)
The Master thesis describe basic electrochemical processes in lithium-ion batteries and characteristic organic polar solvents for these articles. It focuses primarily on the aprotic liquid electrolytes for lithium-ion batteries and the subsequent use of gas chromatography to analyze the collected gas sample from the test article. For this experiment is, in this Master thesis, designed and described experimental arrangement in the form of a glass cell, which allows collection from the space above the working electrode. Finally, the work evaluates the effect of electrode potential on the stability of electrolytes in strongly positive potentials.
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Binders for supercapacitors electrodes
Gottwald, Tomáš ; Dvořák, Petr (referee) ; Sedlaříková, Marie (advisor)
This work deals with the issues of useing binders for supercapacitor electrodes and optimizing the technological process for their production. The work focuses on optimizing the amount of binder used in order to acheive the most capacity. The methodology consists of creating an appropriate experimental electrode and subsequent measuring its associated capacity with AutoLab. This aproach leads to creating grafs which show the dependencies of capacity on the amount of binder used.
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Using thermochromic systems for testing heat distribution
Klimeš, Jan ; Sedlaříková, Marie (referee) ; Zatloukal, Miroslav (advisor)
This thesis deals with principles of thermochromism and its possible applications in heat distribution testing. Theoretical part describes mechanisms which allow the thermochromic properties of the substances. Particular attention is paid to cholesteric liquid crystals. Ability to measure the heat for this type of liquid crystals was varified. Also long service life in high humidity environment, enviroment with intense UV radiation, cyclic changes in temperature or immersion in water was tested. A possibility of their practical use in diagnosis was verified as well. Specifically mapping of heat distribution on an assembled PCB. Conclusion contains comparison and evaluation of this method in terms of accuracy, user comfort and economic advantages compared to conventional infrared sensors.
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Aprotic electrolytes with fire retardant
Hlava, Kamil ; Máca, Josef (referee) ; Sedlaříková, Marie (advisor)
This thesis deals with liquid aprotic electrolytes based on sulfolane with added flame retardant. The theoretical part of the thesis explains concepts - mainly aprotic electrolytes, flame retardants, and their practical use. It also discusses lithium - ion accumulators and materials used in them while focusing on the electrolyte function. The practical part of the thesis aims to measure the properties of aprotic electrolytes: their conductivity, potential window and flashpoint. It also contains a review of the measurement results.
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Liquid Electrolytes for Lithium-Ion Batteries with Enhance Fire Safety
Máca, Josef ; Paidar,, Martin (referee) ; Studničková, Marie (referee) ; Sedlaříková, Marie (advisor)
Dissertation thesis is focused on study of liquid electrolytes for lithium ion batteries. The electrical and physical properties of aprotic electrolytes are observed. The main goal is to increase the fire safety of the batteries. An anhydrous solvents and there blends was investigated. The common used solvents mixtures and new low flammable solvents were used. The common used solvents were used propylene carbonate, ethylene carbonate and others. The new solvents were sulfolane and dimethyl sulfone. In the second part of the work the phosphor base flame retardants as additive in electrolytes was investigated. The last part deals with ionic liquids and there possible use as electrolyte in lithium ion batteries.
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Liquid electrolytes for supercapacitors
Bill, Jan ; Dvořák, Petr (referee) ; Sedlaříková, Marie (advisor)
This work deals with the preparation of liquid electrolytes from different types of aprotic solvents with the aim of their application as electrolytes in electrochemical supercapacitors. Different sorts of aprotic solvents have been chosen, in which the following forms of salts were used: LiBF4, LiClO4,LiPF6. In the next part of the work, the properties of these solvents were measured and the best electrolyte, according to the biggest possible capacity of the system, was chosen. In the theoretical part of this work, the physical principle of supercapacitors and their propeties are described. It deals with electrolytes, their division and with the properties that are appropriate for supercapacitors. The experimental part of the work describes the process of preparation of the samples of electrodes, electrolytes and the techniques of measuring their capacities.
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Thin layers TiO2 prepared by electrochemical way
Janov, Pavel ; Zatloukal, Miroslav (referee) ; Sedlaříková, Marie (advisor)
This work deals with issue of preparation active electrochromic film of titanium dioxide and intercalation properties. By electrodeposition was created active film on glass substrates covered with transparent conductive thin-film In2O3:Sn (ITO). The active films prepared by electrolytic way were compared with active films prepared by vacuum methods. Then has been studied theirs electrode properties in electrolytes containing lithium.
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Bones implants based on Fe and Mg
Košíček, Adam ; Zatloukal, Miroslav (referee) ; Sedlaříková, Marie (advisor)
This paper work deals with properties of metallic biomaterials in terms of their suitability for use as a temporary metal implants. The work focuses on biodegradable materials based on iron and suitable alloying elements, which would create a perfect implant. A part of this work describes procedure of creating biodegradable metallic samples with alloying element Magnesium and measuring the corrosion rates. There are a few theoretical chapters concerning permanent implants, function and composition of human bones, iron and magnesium in human body and biodegradable materials.
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