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Detection of Signed Homonuclear Couplings between Low Abundant Nuclei
Blechta, Vratislav ; Schraml, Jan
The subject of this lecture is a modification of CSEc method for detection of signed homonuclear couplings. The new sequence is neither trivial nor simple application of the CSEc but some tricks are used to design broadband pulse sequence without selective pulses. The sequence was proved on a few samples by measuring carbon-carbon two- and three-bond couplings. For the first time signs of 2J(Si-O-Si) couplings were measured on a set of siloxane oligomers with different bond maps. The results will be presented.
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Měření relativních znamének 29Si-13C kaplingu
Blechta, Vratislav ; Schraml, Jan
This article deals with measurement of relative signs of 29Si-13 C couplings.

National Repository of Grey Literature : 22 records found   previous11 - 20next  jump to record:
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1 Blechta, Václav
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